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Erschienen in: Journal of Nanoparticle Research 3/2024

01.03.2024 | Research

Porous silicon layer decorated with PbS nanoparticles by SILAR method for enhanced photocatalytic degradation of amido black dye

verfasst von: Ameni Rebhi, Chohdi Amri, Ines Khemissi, Rabia Benabderrahmane Zaghouani, Mounir Gaidi, Anouar Hajjaji, Karim Choubani, Mohammed A. Almeshaal, Murugesan Palaniappan Papathi, Mohamed Ben Rabha

Erschienen in: Journal of Nanoparticle Research | Ausgabe 3/2024

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Abstract

The effect of lead sulfide (PbS) decoration on the photocatalytic properties of porous silicon (PS) was investigated. The PbS nanoparticles (PbS-NPs) are prepared by the successive ionic layer adsorption and reaction method (SILAR). The microstructure, surface morphology, phase composition, and optical properties of the prepared structure were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM and high-resolution mode HRTEM), and UV–Vis spectroscopy respectively. The PbS nanoparticle properties were altered by changing the SILAR cycles number (10 to 60 cycles) permitting a well-control of PbS-NP size and density. The synthesized nanohybrid system photocatalytic activity was investigated via the degradation of amido black dye (AB) as a pollutant model. The tested structures showed that the best enhancement of the photocatalytic removal of AB was reached with PbS-NPs deposited during 60 SILAR cycles with a reaction rate of 0.01096 min−1, exceeding that of pure PS layer.

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Literatur
1.
Zurück zum Zitat Canham LT (1990) Silicon quantum wire array fabrication by electrochemical and chemical dissolution of wafers. Appl Phys Lett 57:1046–1048CrossRef Canham LT (1990) Silicon quantum wire array fabrication by electrochemical and chemical dissolution of wafers. Appl Phys Lett 57:1046–1048CrossRef
2.
Zurück zum Zitat Zaghouani RB, Alaya M, Nouri H, Lazzari JL, Dimassi W (2018) Study of WO3 decorated porous silicon and Al2O3-ALD encapsulation. J Mater Sci: Mater Electron 29:17731–17736 Zaghouani RB, Alaya M, Nouri H, Lazzari JL, Dimassi W (2018) Study of WO3 decorated porous silicon and Al2O3-ALD encapsulation. J Mater Sci: Mater Electron 29:17731–17736
3.
Zurück zum Zitat Herino R, Bomchil G, Barla K, Bertrand C, Ginoux JL (1994) Porosity and pore size distributions of porous silicon layers. J Electrochem Soc 1987:134 Herino R, Bomchil G, Barla K, Bertrand C, Ginoux JL (1994) Porosity and pore size distributions of porous silicon layers. J Electrochem Soc 1987:134
4.
Zurück zum Zitat Mhamdi H, Azaiez K, Fiorido T, Zaghouani RB, Lazzari JL, Bendahan M, Dimassi W (2022) Room temperature NO2 gas sensor based on stain-etched porous silicon: towards a low-cost gas sensor integrated on silicon. Inorg Chem Commun 139:109325CrossRef Mhamdi H, Azaiez K, Fiorido T, Zaghouani RB, Lazzari JL, Bendahan M, Dimassi W (2022) Room temperature NO2 gas sensor based on stain-etched porous silicon: towards a low-cost gas sensor integrated on silicon. Inorg Chem Commun 139:109325CrossRef
5.
Zurück zum Zitat Mhamdi H, Zaghouani RB, Fiorido T, Lazzari JL, Bendahan M, Dimassi W (2020) Study of n-WO3/p-porous silicon structures for gas-sensing applications. J Mater Sci Mater Electron 31:7862–7870CrossRef Mhamdi H, Zaghouani RB, Fiorido T, Lazzari JL, Bendahan M, Dimassi W (2020) Study of n-WO3/p-porous silicon structures for gas-sensing applications. J Mater Sci Mater Electron 31:7862–7870CrossRef
6.
Zurück zum Zitat Syshchyk O, Skryshevsky VA, Soldatkin OO, Soldatkin AP (2015) Enzyme biosensor systems based on porous silicon photoluminescence for detection of glucose, urea and heavy metals. Biosens Bioelectron 66:89–94CrossRefPubMed Syshchyk O, Skryshevsky VA, Soldatkin OO, Soldatkin AP (2015) Enzyme biosensor systems based on porous silicon photoluminescence for detection of glucose, urea and heavy metals. Biosens Bioelectron 66:89–94CrossRefPubMed
7.
Zurück zum Zitat Kopani M, Mikula M, Kosnac D, Vojtek P, Gregus J, Vavrinsky E, Pincik E (2018) Effect of etching time on structure of p-type porous silicon. Appl Surf Sci 461:44–47CrossRef Kopani M, Mikula M, Kosnac D, Vojtek P, Gregus J, Vavrinsky E, Pincik E (2018) Effect of etching time on structure of p-type porous silicon. Appl Surf Sci 461:44–47CrossRef
8.
Zurück zum Zitat Mauckner G, Thonke K, Sauer R (1993) Dynamics of the degradation by photo-oxidation of porous silicon: FTPL and FTIR absorption study. J Phys Condens Matter 5:L9 Mauckner G, Thonke K, Sauer R (1993) Dynamics of the degradation by photo-oxidation of porous silicon: FTPL and FTIR absorption study. J Phys Condens Matter 5:L9
9.
Zurück zum Zitat Kilian KA, Böcking T, Gooding JJ (2009) The importance of surface chemistry in mesoporous materials: lessons from porous silicon biosensors. Chem Commun 6:630–640CrossRef Kilian KA, Böcking T, Gooding JJ (2009) The importance of surface chemistry in mesoporous materials: lessons from porous silicon biosensors. Chem Commun 6:630–640CrossRef
10.
Zurück zum Zitat Hajjaji A, Rebhi A, Ka I, Trabelsi K, Gaidi M, Bessais B, El Khakani MA (2020) Pulsed-laser-deposited lead sulfide nanoparticles based decoration of porous silicon layer as an effective passivation treatment for multicrystalline silicon. Appl Surf Sci 505:144590CrossRef Hajjaji A, Rebhi A, Ka I, Trabelsi K, Gaidi M, Bessais B, El Khakani MA (2020) Pulsed-laser-deposited lead sulfide nanoparticles based decoration of porous silicon layer as an effective passivation treatment for multicrystalline silicon. Appl Surf Sci 505:144590CrossRef
11.
Zurück zum Zitat Hamdi A, Boussekey L, Roussel P, Addad A, Ezzaouia H, Boukherroub R, Coffinier Y (2016) Hydrothermal preparation of MoS2/TiO2/Si nanowires composite with enhanced photocatalytic performance under visible light. Mater Des 109:634–643CrossRef Hamdi A, Boussekey L, Roussel P, Addad A, Ezzaouia H, Boukherroub R, Coffinier Y (2016) Hydrothermal preparation of MoS2/TiO2/Si nanowires composite with enhanced photocatalytic performance under visible light. Mater Des 109:634–643CrossRef
12.
13.
Zurück zum Zitat Garcia-Valenzuela JA, Baez-Gaxiola MR, Sotelo-Lerma M (2013) Chemical bath deposition of PbS thin films on float glass substrates using a Pb (CH3COO)2–NaOH–(NH2) 2CS–N (CH2CH2OH)3–CH3CH2OH definite aqueous system and their structural, optical, and electrical/photoelectrical characterization. Thin Solid Films 534:126–131 Garcia-Valenzuela JA, Baez-Gaxiola MR, Sotelo-Lerma M (2013) Chemical bath deposition of PbS thin films on float glass substrates using a Pb (CH3COO)2–NaOH–(NH2) 2CS–N (CH2CH2OH)3–CH3CH2OH definite aqueous system and their structural, optical, and electrical/photoelectrical characterization. Thin Solid Films 534:126–131
14.
Zurück zum Zitat Ka I, Le Borgne V, Fujisawa K, Hayashi T, Kim YA, Endo M, El Khakani MA (2020) PbS-quantum-dots/double-wall-carbon-nanotubes nanohybrid based photodetectors with extremely fast response and high responsivity. Mater Today Energy 16:100378CrossRef Ka I, Le Borgne V, Fujisawa K, Hayashi T, Kim YA, Endo M, El Khakani MA (2020) PbS-quantum-dots/double-wall-carbon-nanotubes nanohybrid based photodetectors with extremely fast response and high responsivity. Mater Today Energy 16:100378CrossRef
15.
Zurück zum Zitat Gonfa BA, Kim MR, Zheng P, Cushing S, Qiao Q, Wu N, Ma D (2016) Investigation of the plasmonic effect in air-processed PbS/CdS core–shell quantum dot based solar cells. J Mater Chem A 4:13071–13080CrossRef Gonfa BA, Kim MR, Zheng P, Cushing S, Qiao Q, Wu N, Ma D (2016) Investigation of the plasmonic effect in air-processed PbS/CdS core–shell quantum dot based solar cells. J Mater Chem A 4:13071–13080CrossRef
16.
Zurück zum Zitat Ka I, Le Borgne V, Ma D, El Khakani MA (2012) Pulsed laser ablation based direct synthesis of single-wall carbon nanotube/PbS quantum dot nanohybrids exhibiting strong, spectrally wide and fast photoresponse. Adv Mater 24:6289–6294CrossRefPubMed Ka I, Le Borgne V, Ma D, El Khakani MA (2012) Pulsed laser ablation based direct synthesis of single-wall carbon nanotube/PbS quantum dot nanohybrids exhibiting strong, spectrally wide and fast photoresponse. Adv Mater 24:6289–6294CrossRefPubMed
17.
Zurück zum Zitat Yang P, Song CF, Lü MK, Yin X, Zhou GJ, Xu D, Yuan DR (2001) The luminescence of PbS nanoparticles embedded in sol–gel silica glass. Chem Phys Lett 345:429–434CrossRef Yang P, Song CF, Lü MK, Yin X, Zhou GJ, Xu D, Yuan DR (2001) The luminescence of PbS nanoparticles embedded in sol–gel silica glass. Chem Phys Lett 345:429–434CrossRef
18.
Zurück zum Zitat Pan X, Dong Y, Jia M, Wen J, Su C, Shang Y, Wang T (2021) Temperature-induced PbS quantum dots with tunable broadband wavelength grown by atomic layer deposition. Appl Surf Sci 546:149086 Pan X, Dong Y, Jia M, Wen J, Su C, Shang Y, Wang T (2021) Temperature-induced PbS quantum dots with tunable broadband wavelength grown by atomic layer deposition. Appl Surf Sci 546:149086
19.
Zurück zum Zitat da Silva Filho JMC, Marques FC (2019) Structural and optical temperature-dependent properties of PbS thin films deposited by radio frequency sputtering. Mater Sci Semicond Process 91:188–193CrossRef da Silva Filho JMC, Marques FC (2019) Structural and optical temperature-dependent properties of PbS thin films deposited by radio frequency sputtering. Mater Sci Semicond Process 91:188–193CrossRef
20.
Zurück zum Zitat Islam MA, Misran H, Akhtaruzzaman M, Amin N (2020) Influence of oxygen on structural and optoelectronic properties of CdS thin film deposited by magnetron sputtering technique. Chin J Phys 67:170–179CrossRef Islam MA, Misran H, Akhtaruzzaman M, Amin N (2020) Influence of oxygen on structural and optoelectronic properties of CdS thin film deposited by magnetron sputtering technique. Chin J Phys 67:170–179CrossRef
21.
Zurück zum Zitat Yang YJ, Hu S (2008) The deposition of highly uniform and adhesive nanocrystalline PbS film from solution. Thin Solid Films 516:6048–6051CrossRef Yang YJ, Hu S (2008) The deposition of highly uniform and adhesive nanocrystalline PbS film from solution. Thin Solid Films 516:6048–6051CrossRef
22.
Zurück zum Zitat Chandekar KV, Kant KM (2018) Size-strain analysis and elastic properties of CoFe2O4 nanoplatelets by hydrothermal method. J Mol Struct 1154:418–427CrossRef Chandekar KV, Kant KM (2018) Size-strain analysis and elastic properties of CoFe2O4 nanoplatelets by hydrothermal method. J Mol Struct 1154:418–427CrossRef
23.
Zurück zum Zitat Suganya M, Anitha S, Prabha D, Balamurugan S, Srivind J, Balu AR (2017) Enhanced photocatalytic and antifungal properties of Sr-doped PbS nanopowders. Mater Technol 33:1–6 Suganya M, Anitha S, Prabha D, Balamurugan S, Srivind J, Balu AR (2017) Enhanced photocatalytic and antifungal properties of Sr-doped PbS nanopowders. Mater Technol 33:1–6
24.
Zurück zum Zitat Zhang X, Tang Y, Li Y, Wang Y, Liu X, Liu C, Luo S (2013) Reduced graphene oxide and PbS nanoparticles co-modified TiO2 nanotube arrays as a recyclable and stable photocatalyst for efficient degradation of pentachlorophenol. Appl Catal A 457:78–84CrossRef Zhang X, Tang Y, Li Y, Wang Y, Liu X, Liu C, Luo S (2013) Reduced graphene oxide and PbS nanoparticles co-modified TiO2 nanotube arrays as a recyclable and stable photocatalyst for efficient degradation of pentachlorophenol. Appl Catal A 457:78–84CrossRef
25.
Zurück zum Zitat Hajjaji A, Jemai S, Rebhi A, Trabelsi K, Gaidi M, Alhazaa AN, Al-Gawati MA, El Khakani MA, Bessais B (2020) Enhancement of photocatalytic and photoelectrochemical properties of TiO2 nanotubes sensitized by SILAR-Deposited PbS nanoparticles. J Materiomics 6:62–69CrossRef Hajjaji A, Jemai S, Rebhi A, Trabelsi K, Gaidi M, Alhazaa AN, Al-Gawati MA, El Khakani MA, Bessais B (2020) Enhancement of photocatalytic and photoelectrochemical properties of TiO2 nanotubes sensitized by SILAR-Deposited PbS nanoparticles. J Materiomics 6:62–69CrossRef
26.
Zurück zum Zitat Zhang H, Gao Y, Zhu G, Li B, Gou J, Cheng X (2019) Synthesis of PbS/TiO2 nano-tubes photoelectrode and its enhanced visible light driven photocatalytic performance and mechanism for purification of 4-chlorobenzoic acid. Sep Purif Technol 227:115697CrossRef Zhang H, Gao Y, Zhu G, Li B, Gou J, Cheng X (2019) Synthesis of PbS/TiO2 nano-tubes photoelectrode and its enhanced visible light driven photocatalytic performance and mechanism for purification of 4-chlorobenzoic acid. Sep Purif Technol 227:115697CrossRef
27.
Zurück zum Zitat Khemissi I, Khezami L, Trabelsi K, Guesmi A, Kouki A, Kiwi J, Bessais B, Rtimi S, Hajjaji A (2023) Stable Ta2O5 nanotubes decorated by PbS by the SILAR method for photocatalytic dye degradation. J Photochem Photobiol, A 444:114937CrossRef Khemissi I, Khezami L, Trabelsi K, Guesmi A, Kouki A, Kiwi J, Bessais B, Rtimi S, Hajjaji A (2023) Stable Ta2O5 nanotubes decorated by PbS by the SILAR method for photocatalytic dye degradation. J Photochem Photobiol, A 444:114937CrossRef
28.
Zurück zum Zitat Kar A, Sain S, Rossouw D, Knappett BR, Pradhan SK, Wheatley AEH (2016) Facile synthesis of SnO2–PbS nanocomposites with controlled structure for applications in photocatalysis. Nanoscale 8:1–30CrossRef Kar A, Sain S, Rossouw D, Knappett BR, Pradhan SK, Wheatley AEH (2016) Facile synthesis of SnO2–PbS nanocomposites with controlled structure for applications in photocatalysis. Nanoscale 8:1–30CrossRef
29.
Zurück zum Zitat Algethami FK, Trabelsi K, Hajjaji A, Rabha MB, Khezami L, Elamin MR, Bessais B, El Khakani MA (2022) Photocatalytic activity of silicon nanowires decorated with PbS nanoparticles deposited by pulsed laser deposition for efficient wastewater treatment. Materials (Basel) 15:4970CrossRefPubMed Algethami FK, Trabelsi K, Hajjaji A, Rabha MB, Khezami L, Elamin MR, Bessais B, El Khakani MA (2022) Photocatalytic activity of silicon nanowires decorated with PbS nanoparticles deposited by pulsed laser deposition for efficient wastewater treatment. Materials (Basel) 15:4970CrossRefPubMed
30.
Zurück zum Zitat Sabri NS, Deni MS, Zakaria A, Talari MK (2012) Effect of Mn doping on structural and optical properties of SnO2 nanoparticles prepared by mechanochemical processing. Phys Procedia 25(233):239 Sabri NS, Deni MS, Zakaria A, Talari MK (2012) Effect of Mn doping on structural and optical properties of SnO2 nanoparticles prepared by mechanochemical processing. Phys Procedia 25(233):239
31.
Zurück zum Zitat Ahmadi A, Wu T (2017) Inactivation of E. coli using a novel TiO2 nanotube electrode. Environ Sci Water Res Technol 3:534–545CrossRef Ahmadi A, Wu T (2017) Inactivation of E. coli using a novel TiO2 nanotube electrode. Environ Sci Water Res Technol 3:534–545CrossRef
32.
Zurück zum Zitat Bai W, Tian X, Yao R, Chen Y, Lin H, Zheng J, Xu Y, Lin J (2020) Preparation of nano-TiO2@polyfluorene composite particles for the photocatalytic degradation of organic pollutants under sunlight. Solar Energy 196:616–624 Bai W, Tian X, Yao R, Chen Y, Lin H, Zheng J, Xu Y, Lin J (2020) Preparation of nano-TiO2@polyfluorene composite particles for the photocatalytic degradation of organic pollutants under sunlight. Solar Energy 196:616–624
Metadaten
Titel
Porous silicon layer decorated with PbS nanoparticles by SILAR method for enhanced photocatalytic degradation of amido black dye
verfasst von
Ameni Rebhi
Chohdi Amri
Ines Khemissi
Rabia Benabderrahmane Zaghouani
Mounir Gaidi
Anouar Hajjaji
Karim Choubani
Mohammed A. Almeshaal
Murugesan Palaniappan Papathi
Mohamed Ben Rabha
Publikationsdatum
01.03.2024
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 3/2024
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-024-05957-w

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