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Polymer Bulletin
Erschienen in: Polymer Bulletin 6/2020

23.08.2019 | Original Paper

Preparation and characterization of biodegradable polyurethane composites containing oyster shell powder

verfasst von: Chia-Hung Liu, Hsun-Tsing Lee, Chi-Hui Tsou, Chyung-Chyung Wang, Jia-Hao Gu, Maw-Cherng Suen

Erschienen in: Polymer Bulletin | Ausgabe 6/2020

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Abstract

In this study, natural oyster shell (OS) powder was used to reinforce polyurethane (PU) to fabricate OS powder/PU (OS/PU) composites. First, polycaprolactone diol, 4,4′-diphenylmethane diisocyanate, and 1,4-butanediol (1,4-BD) were utilized, respectively, as a soft segment, hard segment, and chain extender for PU. Next, the aforementioned chemicals were placed in the solvent N,N-dimethylacetamide (DMAc) to react with each other and form PU. Finally, OSP was added to the PU to form biodegradable OS/PUs. FTIR analysis showed that –NCO functional groups underwent a complete reaction, and X-ray diffraction analysis showed that OS characteristic crystallization peaks emerged when 2θ = 17.9°, 29.3°, and 34.0°. The TGA, DSC, and DMA showed that increases in OS content elevated PU decomposition temperature, glass transition temperature, and dynamic glass transition temperature. Antibacterial tests showed that increases in the OS content enhanced the antibacterial properties of OS/PUs against Staphylococcus aureus and Escherichia coli.
Vorheriger Artikel Electrosynthesized conducting poly(1,5-diaminonaphthalene) as a corrosion inhibitor for copper

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Metadaten
Titel
Preparation and characterization of biodegradable polyurethane composites containing oyster shell powder
verfasst von
Chia-Hung Liu
Hsun-Tsing Lee
Chi-Hui Tsou
Chyung-Chyung Wang
Jia-Hao Gu
Maw-Cherng Suen
Publikationsdatum
23.08.2019
Verlag
Springer Berlin Heidelberg
Erschienen in
Polymer Bulletin / Ausgabe 6/2020
Print ISSN: 0170-0839
Elektronische ISSN: 1436-2449
DOI
https://doi.org/10.1007/s00289-019-02906-9

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