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2017 | OriginalPaper | Buchkapitel

Real-Time Observation of AZ91 Solidification by Synchrotron Radiography

verfasst von : G. Zeng, K. Nogita, S. Belyakov, J. W. Xian, S. D. McDonald, K. V. Yang, H. Yasuda, C. M. Gourlay

Erschienen in: Magnesium Technology 2017

Verlag: Springer International Publishing

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Abstract

The equiaxed solidification of AZ91 has been studied by time-resolved synchrotron radiography of 150 µm thick samples. Primary Al8Mn5 and α-Mg dendrite growth has been observed and analysed during solidification at a cooling rate of 5 K/min. Morphological, compositional and kinetic information of AZ91 solidification has been extracted from quantitative image analysis on synchrotron radiographs combined with thermodynamic calculations. α-Mg dendrites appeared to grow largely independently of the surrounding Al8Mn5 particles. Solute partitioning mainly occurred during the dendrite coarsening stage and Zn/Al solute build-up was studied in a region that remains a liquid channel until a late stage of AZ91 solidification.

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Literatur
1.
Zurück zum Zitat B.L. Mordike, T. Ebert, Magnesium properties—applications—potential. Mater. Sci. Eng. A 302, 37–45 (2001)CrossRef B.L. Mordike, T. Ebert, Magnesium properties—applications—potential. Mater. Sci. Eng. A 302, 37–45 (2001)CrossRef
2.
Zurück zum Zitat E.F. Emley, Principles of Magnesium Technology (Elsevier Science & Technology, Oxford, 1966), pp. 157–159 E.F. Emley, Principles of Magnesium Technology (Elsevier Science & Technology, Oxford, 1966), pp. 157–159
3.
Zurück zum Zitat M. Liu, P.J. Uggowitzer, A.V. Nagasekhar, P. Schmutz, M. Easton, G.L. Song, A. Atrens, Calculated phase diagrams and the corrosion of die-cast Mg-Al alloys. Corros. Sci. 51, 602–619 (2009)CrossRef M. Liu, P.J. Uggowitzer, A.V. Nagasekhar, P. Schmutz, M. Easton, G.L. Song, A. Atrens, Calculated phase diagrams and the corrosion of die-cast Mg-Al alloys. Corros. Sci. 51, 602–619 (2009)CrossRef
4.
Zurück zum Zitat M. Ohno, D. Mirkovic, R. Schmid-Fetzer, Phase equilibria and solidification of Mg-rich Mg-Al-Zn alloys. Mater. Sci. Eng. A 421, 328–337 (2006)CrossRef M. Ohno, D. Mirkovic, R. Schmid-Fetzer, Phase equilibria and solidification of Mg-rich Mg-Al-Zn alloys. Mater. Sci. Eng. A 421, 328–337 (2006)CrossRef
5.
Zurück zum Zitat M. Ohno, D. Mirkovic, R. Schmid-Fetzer, Liquidus and solidus temperatures of Mg-rich Mg-Al-Mn-Zn alloys. Acta Mater. 54, 3883–3891 (2006)CrossRef M. Ohno, D. Mirkovic, R. Schmid-Fetzer, Liquidus and solidus temperatures of Mg-rich Mg-Al-Mn-Zn alloys. Acta Mater. 54, 3883–3891 (2006)CrossRef
6.
Zurück zum Zitat S. Biswas, F. Sket, M. Chiumenti, I. Gutiérrez-Urrutia, J.M. Molina-Aldareguía, M.T. Pérez-Prado, Relationship between the 3D porosity and β-phase distributions and the mechanical properties of a high pressure die cast AZ91 Mg alloy. Metall. Mater. Trans. A 44, 4391–4403 (2013) S. Biswas, F. Sket, M. Chiumenti, I. Gutiérrez-Urrutia, J.M. Molina-Aldareguía, M.T. Pérez-Prado, Relationship between the 3D porosity and β-phase distributions and the mechanical properties of a high pressure die cast AZ91 Mg alloy. Metall. Mater. Trans. A 44, 4391–4403 (2013)
7.
Zurück zum Zitat A.V. Nagasekhar, C.H. Cáceres, C. Kong, 3D characterization of intermetallics in a high pressure die cast Mg alloy using focused ion beam tomography. Mater. Charact. 61, 1035–1042 (2010)CrossRef A.V. Nagasekhar, C.H. Cáceres, C. Kong, 3D characterization of intermetallics in a high pressure die cast Mg alloy using focused ion beam tomography. Mater. Charact. 61, 1035–1042 (2010)CrossRef
8.
Zurück zum Zitat M. Yang, S.M. Xiong, Z. Guo, Characterisation of the 3-D dendrite morphology of magnesium alloys using synchrotron X-ray tomography and 3-D phase-field modelling. Acta Mater. 92, 8–17 (2015)CrossRef M. Yang, S.M. Xiong, Z. Guo, Characterisation of the 3-D dendrite morphology of magnesium alloys using synchrotron X-ray tomography and 3-D phase-field modelling. Acta Mater. 92, 8–17 (2015)CrossRef
9.
Zurück zum Zitat A.K. Dahle, Y.C. Lee, M.D. Nave, P.L. Schaffer, D.H. StJohn, Development of the as-cast microstructure in magnesium-aluminium alloys. J. Light Met. 1, 61–72 (2001)CrossRef A.K. Dahle, Y.C. Lee, M.D. Nave, P.L. Schaffer, D.H. StJohn, Development of the as-cast microstructure in magnesium-aluminium alloys. J. Light Met. 1, 61–72 (2001)CrossRef
10.
Zurück zum Zitat L. Lu, A.K. Dahle, D.H. StJohn, Heterogeneous nucleation of Mg-Al alloys. Scripta Mater. 54, 2197–2201 (2006)CrossRef L. Lu, A.K. Dahle, D.H. StJohn, Heterogeneous nucleation of Mg-Al alloys. Scripta Mater. 54, 2197–2201 (2006)CrossRef
11.
Zurück zum Zitat Y. Wang, M. Xia, Z. Fan, X. Zhou, G.E. Thompson, The effect of Al8Mn5 intermetallic particles on grain size of as-cast Mg-Al-Zn AZ91D alloy. Intermetallics 18, 1683–1689 (2010)CrossRef Y. Wang, M. Xia, Z. Fan, X. Zhou, G.E. Thompson, The effect of Al8Mn5 intermetallic particles on grain size of as-cast Mg-Al-Zn AZ91D alloy. Intermetallics 18, 1683–1689 (2010)CrossRef
12.
Zurück zum Zitat C. Simensen, N. Hansen, The effect of silicon upon alloys of Mg-2. 2 wt%Al-Mn. Z. Metallkd. 79, 541–543 (1988) C. Simensen, N. Hansen, The effect of silicon upon alloys of Mg-2. 2 wt%Al-Mn. Z. Metallkd. 79, 541–543 (1988)
13.
Zurück zum Zitat B.C. Oberlander, C.J. Simensen, J. Svalestuen, A. Thorvaldsen, Phase diagram of liquid magnesium–aluminium–manganese alloys, in Magnesium Technology (1986), pp. 133–137 B.C. Oberlander, C.J. Simensen, J. Svalestuen, A. Thorvaldsen, Phase diagram of liquid magnesium–aluminium–manganese alloys, in Magnesium Technology (1986), pp. 133–137
14.
Zurück zum Zitat C.J. Simensen, B.C. Oberlander, J. Svalestuen, A. Thorvaldsen, Phase diagram for magnesium-aluminium-manganese above 650 °C. Z. Metallkd. 79, 696–699 (1988) C.J. Simensen, B.C. Oberlander, J. Svalestuen, A. Thorvaldsen, Phase diagram for magnesium-aluminium-manganese above 650 °C. Z. Metallkd. 79, 696–699 (1988)
15.
Zurück zum Zitat C.J. Simensen, B.C. Oberlander, J. Svalestuen, A. Thorvaldsen, The Effect of Iron on Mg-4 wt.% Al-Mn Alloys. Z. Metallkd. 80, 101–103 (1989) C.J. Simensen, B.C. Oberlander, J. Svalestuen, A. Thorvaldsen, The Effect of Iron on Mg-4 wt.% Al-Mn Alloys. Z. Metallkd. 80, 101–103 (1989)
16.
Zurück zum Zitat G. Han, X. Liu, Phase control and formation mechanism of Al–Mn(–Fe) intermetallic particles in Mg–Al-based alloys with FeCl3 addition or melt superheating. Acta Mater. 114, 54–66 (2016)CrossRef G. Han, X. Liu, Phase control and formation mechanism of Al–Mn(–Fe) intermetallic particles in Mg–Al-based alloys with FeCl3 addition or melt superheating. Acta Mater. 114, 54–66 (2016)CrossRef
17.
Zurück zum Zitat F. Pan, Z. Feng, X. Zhang, A. Tang, The types and distribution characterization of Al-Mn phases in the AZ61 magnesium alloy. Procedia Eng. 27, 833–839 (2012)CrossRef F. Pan, Z. Feng, X. Zhang, A. Tang, The types and distribution characterization of Al-Mn phases in the AZ61 magnesium alloy. Procedia Eng. 27, 833–839 (2012)CrossRef
18.
Zurück zum Zitat B. Sundman, B. Jansson, J.-O. Andersson, The thermo-calc databank system. Calphad 9, 153–190 (1985)CrossRef B. Sundman, B. Jansson, J.-O. Andersson, The thermo-calc databank system. Calphad 9, 153–190 (1985)CrossRef
19.
Zurück zum Zitat Y.W. Riddle, M.M. Makhlouf, Characterizing solidification by non-equilibrium thermal analysis, in Magnesium Technology (2003), pp. 101–106 Y.W. Riddle, M.M. Makhlouf, Characterizing solidification by non-equilibrium thermal analysis, in Magnesium Technology (2003), pp. 101–106
20.
Zurück zum Zitat R.H. Mathiesen, L. Arnberg, X-ray radiography observations of columnar dendritic growth and constitutional undercooling in an Al-30 wt%Cu alloy. Acta Mater. 53, 947–956 (2005)CrossRef R.H. Mathiesen, L. Arnberg, X-ray radiography observations of columnar dendritic growth and constitutional undercooling in an Al-30 wt%Cu alloy. Acta Mater. 53, 947–956 (2005)CrossRef
21.
Zurück zum Zitat W.U. Mirihanage, K.V. Falch, I. Snigireva, A. Snigirev, Y.J. Li, L. Arnberg, R.H. Mathiesen, Retrieval of three-dimensional spatial information from fast in situ two-dimensional synchrotron radiography of solidification microstructure evolution. Acta Mater. 81, 241–247 (2014)CrossRef W.U. Mirihanage, K.V. Falch, I. Snigireva, A. Snigirev, Y.J. Li, L. Arnberg, R.H. Mathiesen, Retrieval of three-dimensional spatial information from fast in situ two-dimensional synchrotron radiography of solidification microstructure evolution. Acta Mater. 81, 241–247 (2014)CrossRef
22.
Zurück zum Zitat L. Arnberg, R.H. Mathiesen, The real-time, high-resolution X-ray video microscopy of solidification in aluminum alloys. JOM 59, 20–26 (2007)CrossRef L. Arnberg, R.H. Mathiesen, The real-time, high-resolution X-ray video microscopy of solidification in aluminum alloys. JOM 59, 20–26 (2007)CrossRef
23.
Zurück zum Zitat T. Nagira, C.M. Gourlay, A. Sugiyama, M. Uesugi, Y. Kanzawa, M. Yoshiya, K. Uesugi, K. Umetani, H. Yasuda, Direct observation of deformation in semi-solid carbon steel. Scripta Mater. 64, 1129–1132 (2011)CrossRef T. Nagira, C.M. Gourlay, A. Sugiyama, M. Uesugi, Y. Kanzawa, M. Yoshiya, K. Uesugi, K. Umetani, H. Yasuda, Direct observation of deformation in semi-solid carbon steel. Scripta Mater. 64, 1129–1132 (2011)CrossRef
24.
Zurück zum Zitat A.B. Phillion, R.W. Hamilton, D. Fuloria, A.C.L. Leung, P. Rockett, T. Connolley, P.D. Lee, In situ X-ray observation of semi-solid deformation and failure in Al-Cu alloys. Acta Mater. 59, 1436–1444 (2011)CrossRef A.B. Phillion, R.W. Hamilton, D. Fuloria, A.C.L. Leung, P. Rockett, T. Connolley, P.D. Lee, In situ X-ray observation of semi-solid deformation and failure in Al-Cu alloys. Acta Mater. 59, 1436–1444 (2011)CrossRef
25.
Zurück zum Zitat G. Reinhart, N. Mangelinck-Noël, H. Nguyen-Thi, T. Schenk, J. Gastaldi, B. Billia, P. Pino, J. Härtwig, J. Baruchel, Investigation of columnar-equiaxed transition and equiaxed growth of aluminium based alloys by X-ray radiography. Mater. Sci. Eng. A 413–414, 384–388 (2005)CrossRef G. Reinhart, N. Mangelinck-Noël, H. Nguyen-Thi, T. Schenk, J. Gastaldi, B. Billia, P. Pino, J. Härtwig, J. Baruchel, Investigation of columnar-equiaxed transition and equiaxed growth of aluminium based alloys by X-ray radiography. Mater. Sci. Eng. A 413–414, 384–388 (2005)CrossRef
26.
Zurück zum Zitat H. Yasuda, I. Ohnaka, K. Kawasaki, A. Sugiyama, T. Ohmichi, J. Iwane, K. Umetani, Direct observation of stray crystal formation in unidirectional solidification of Sn-Bi alloy by X-ray imaging. J. Cryst. Growth 262, 645–652 (2004)CrossRef H. Yasuda, I. Ohnaka, K. Kawasaki, A. Sugiyama, T. Ohmichi, J. Iwane, K. Umetani, Direct observation of stray crystal formation in unidirectional solidification of Sn-Bi alloy by X-ray imaging. J. Cryst. Growth 262, 645–652 (2004)CrossRef
27.
Zurück zum Zitat C.M. Gourlay, K. Nogita, A.K. Dahle, Y. Yamamoto, K. Uesugi, T. Nagira, M. Yoshiya, H. Yasuda, In situ investigation of unidirectional solidification in Sn-0.7Cu and Sn-0.7Cu-0.06Ni. Acta Mater. 59, 4043–4054 (2011)CrossRef C.M. Gourlay, K. Nogita, A.K. Dahle, Y. Yamamoto, K. Uesugi, T. Nagira, M. Yoshiya, H. Yasuda, In situ investigation of unidirectional solidification in Sn-0.7Cu and Sn-0.7Cu-0.06Ni. Acta Mater. 59, 4043–4054 (2011)CrossRef
28.
Zurück zum Zitat G. Zeng, S.D. McDonald, C.M. Gourlay, K. Uesugi, Y. Terada, H. Yasuda, K. Nogita, Solidification of Sn-0.7Cu-0.15Zn solder: in situ observation. Metall. Mater. Trans. A 45, 918–926 (2014)CrossRef G. Zeng, S.D. McDonald, C.M. Gourlay, K. Uesugi, Y. Terada, H. Yasuda, K. Nogita, Solidification of Sn-0.7Cu-0.15Zn solder: in situ observation. Metall. Mater. Trans. A 45, 918–926 (2014)CrossRef
29.
Zurück zum Zitat H. Yasuda, T. Nagira, M. Yoshiya, N. Nakatsuka, A. Sugiyama, K. Uesugi, K. Umetani, Development of X-ray Imaging for Observing Solidification of Carbon Steels. ISIJ Int. 51, 402–408 (2011)CrossRef H. Yasuda, T. Nagira, M. Yoshiya, N. Nakatsuka, A. Sugiyama, K. Uesugi, K. Umetani, Development of X-ray Imaging for Observing Solidification of Carbon Steels. ISIJ Int. 51, 402–408 (2011)CrossRef
30.
Zurück zum Zitat S. Shuai, E. Guo, A.B. Phillion, M.D. Callaghan, T. Jing, P.D. Lee, Fast synchrotron X-ray tomographic quantification of dendrite evolution during the solidification of MgSn alloys. Acta Mater. 118, 260–269 (2016)CrossRef S. Shuai, E. Guo, A.B. Phillion, M.D. Callaghan, T. Jing, P.D. Lee, Fast synchrotron X-ray tomographic quantification of dendrite evolution during the solidification of MgSn alloys. Acta Mater. 118, 260–269 (2016)CrossRef
31.
Zurück zum Zitat D. Casari, W.U. Mirihanage, K.V. Falch, I.G. Ringdalen, J. Friis, R. Schmid-Fetzer, D. Zhao, Y. Li, W.H. Sillekens, R.H. Mathiesen, α-Mg primary phase formation and dendritic morphology transition in solidification of a Mg-Nd-Gd-Zn-Zr casting alloy. Acta Mater. 116, 177–187 (2016)CrossRef D. Casari, W.U. Mirihanage, K.V. Falch, I.G. Ringdalen, J. Friis, R. Schmid-Fetzer, D. Zhao, Y. Li, W.H. Sillekens, R.H. Mathiesen, α-Mg primary phase formation and dendritic morphology transition in solidification of a Mg-Nd-Gd-Zn-Zr casting alloy. Acta Mater. 116, 177–187 (2016)CrossRef
32.
Zurück zum Zitat N. Otsu, A threshold selection method from gray-level histograms. Automatica 11, 23–27 (1975) N. Otsu, A threshold selection method from gray-level histograms. Automatica 11, 23–27 (1975)
Metadaten
Titel
Real-Time Observation of AZ91 Solidification by Synchrotron Radiography
verfasst von
G. Zeng
K. Nogita
S. Belyakov
J. W. Xian
S. D. McDonald
K. V. Yang
H. Yasuda
C. M. Gourlay
Copyright-Jahr
2017
DOI
https://doi.org/10.1007/978-3-319-52392-7_82

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