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Optical and Quantum Electronics

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01.03.2024

Spectroscopic and TL properties of Sm₂O₃ doped lead silicate glasses containing alumina and antimony oxides

verfasst von: Padala Ashok, Ravi Kumar Guntu, S. Shashi Devi, Ch. Ramesh, N. Rama Krishna Chand

Erschienen in: Optical and Quantum Electronics | Ausgabe 3/2024

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Abstract

The present investigation, aimed to prepare lead silicate glasses doped with samarium ions and to study it’s structure, elastic, spectroscopic and thermoluminiscence properties with Al_(10−x)Sb_x composite influence. The objective of the investigation is to develop TL sustained good laser active resource by means of studying photo and thermoluminiscence properties. In this direction, we have prepared the glass series of Al_(10−x)Sb_xSm_0.1Pb₃₀Si_59.9 materials (where, 0 ≤ x ≤ 10, with steps of 0, 2, 4, 6, 8 and 10 mol%) after that planned for structural (XRD, FT-IR, DTA, EDS & SEM), Optical (UV & PL) and thermoluminescence characterization. The XRD and SEM studies reveal the glassy behavior of test samples. The EDX analysis signifies the chemical constitutes with atomic weight %. The physical properties such as density and molar volume of glasses were evaluated. The DTA studies of glasses reveal the glass transition and crystallization temperature points. The values of thermal stabilities of glasses found to be purely function of Sb³⁺ ions. Various structural vibrations of test glass conformed using FT-IR studies. Using ultrasonic velocities of the test glasses, the glasses' micro-hardness was evaluated. From the absorption spectra, the Judd–Ofelt intensity parameters (Ω₂, Ω₄, Ω₆) have been calculated. The PL spectra under stimulation at 402 nm show a prominent reddish–orange emission at 602 nm. The experimental lifetimes (τ_r) of the ⁴G_5/2 → ⁶H_7/2 (602 nm) luminescence transition were measured using the decay spectral profiles of this transition. The evaluated emission cross-sections (σ_se), branching ratios (β_r), and quantum efficiency (η) allow us to speculate that the lead silicate glasses doped with Sm³⁺ ions are ideally suitable as potential gain mediums for visible reddish orange lasers pumped directly by readily available 405 nm laser diodes. Quantum efficiencies of the produced glasses are obtained using a decay curve analysis. The emission spectra used to establish the developed glasses' reddish orange emission are used to compute the CIE chromaticity coordinates. It is evident from the stated fluorescent properties that the developed glasses are suited for reddish–orange laser applications, particularly in opto-electronic devices. From all of the values obtained, it can be observed that SAS₆ glass code is ideally suited for reddish–orange laser applications. The TL properties are studied at 30 kGy gamma irradiation dose range. The frequency factor and A.E. of glasses were evaluated. This reveals that the TL behavior of glasses is a purely function of Sb³⁺ ions. Overall, the Al_(10−x)Sb_xSm_0.1Pb₃₀Si_59.9 glasses prepared are mechanical hard, TL effective, and optically useful resources.

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Titel: Spectroscopic and TL properties of Sm2O3 doped lead silicate glasses containing alumina and antimony oxides
verfasst von: Padala Ashok
Ravi Kumar Guntu
S. Shashi Devi
Ch. Ramesh
N. Rama Krishna Chand
Publikationsdatum: 01.03.2024
Verlag: Springer US
Erschienen in: Optical and Quantum Electronics / Ausgabe 3/2024
Print ISSN: 0306-8919
Elektronische ISSN: 1572-817X
DOI: https://doi.org/10.1007/s11082-023-06093-w

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Weitere Artikel der Ausgabe 3/2024

New analytic wave solutions to (2 + 1)-dimensional Kadomtsev–Petviashvili–Benjamin–Bona–Mahony equation using the modified extended mapping method

Optical quantum conformable recursional electroosmotic optimistic energy

A theoretical investigation of the Ba2CePtO6 double perovskite for optoelectronic and thermoelectric applications

Probing the influence of ZnFe2O4 doping on the optical and dielectric characteristics of PMMA/PANi

On the Van der Waals model on granular matters with truncated M-fractional derivative

Some optical soliton solution with bifurcation analysis of the paraxial nonlinear Schrödinger equation

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