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Journal of Electroceramics

Erschienen in:

09.03.2018

Structural, dielectric and magnetic properties of particulate composites of relaxor (BaTi_0.85Sn_0.15O₃) and ferrite (NiFe₂O₄) synthesized by gel-combustion method

verfasst von: Md. Jawed Ansaree, Upendra Kumar, Shail Upadhyay

Erschienen in: Journal of Electroceramics | Ausgabe 3/2018

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Abstract

Particulate composites of (1-x) BaTi_0.85Sn_0.15O₃ – x NiFe₂O₄ (with x = 5, 10,15 and 20 wt%) were synthesized using the solid-state reaction method by sintering at 1350 °C for 4 h. Formation of the diphase composites was confirmed by X-ray diffraction (XRD) and Fourier Transform Infra-red (FTIR) techniques. Temperature (RT-200 °C) and frequency (20 Hz- 1 MHz) dependent of AC conductivity, dielectric constant and dissipation have been studied. The dielectric constant exhibits strong frequency dispersion in the range 20 Hz-1 kHz which is attributed to Maxwell-Wagner interfacial polarization occurring at grain-grain-boundaries interface/interface of grains of BTS-NF. The M-H curve of all the composites exhibited a hysteresis loops typical charcateistic of a ferromagnetic material. The ferromagnetic ordering in the composites on account of NiFe₂O₄ as a constituent is explained using bound magnetic polarons (BMPs) model. The experimental magnetic data have been fitted to BMP model. Value of M_s is smaller, whereas of H_c and M_r are higher of the composites compared to value for NiFe₂O₄. The temperature at which divergence in the M vs. T plot in ZFC and FC starts is higher for the composites than for NiFe₂O₄.

Vorheriger Artikel Improved magnetic properties of bismuth ferrite ceramics by La and Gd co-substitution

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Titel: Structural, dielectric and magnetic properties of particulate composites of relaxor (BaTi0.85Sn0.15O3) and ferrite (NiFe2O4) synthesized by gel-combustion method
verfasst von: Md. Jawed Ansaree
Upendra Kumar
Shail Upadhyay
Publikationsdatum: 09.03.2018
Verlag: Springer US
Erschienen in: Journal of Electroceramics / Ausgabe 3/2018
Print ISSN: 1385-3449
Elektronische ISSN: 1573-8663
DOI: https://doi.org/10.1007/s10832-018-0127-0

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