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Optical and Quantum Electronics
Erschienen in: Optical and Quantum Electronics 14/2023

01.12.2023

Study of structural, surface morphology, Raman spectroscopy, and electrochemical properties of Bi1+xFeO3 nanoparticles for usage in supercapacitors

verfasst von: Garima Srivastava, Shalendra Kumar, S. Z. Hashmi, Ravina, A. M. Quraishi, Saurabh Dalela, Faheem Ahmed, Kavita Kumari, B. H. Koo, P. A. Alvi

Erschienen in: Optical and Quantum Electronics | Ausgabe 14/2023

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Abstract

This article reports the synthesis of Bi1+xFeO3 (with x = 0, 0.05, 0.10) nanoparticles and their characterizing results for seeking the appropriate utility in making energy storage devices like supercapacitors. The BFO nanoparticles were synthesized via the sol–gel route and characterized by different techniques. The structural analysis was carried out by XRD along with Rietveld refinement, which gives information about the particle size, micro-strain and rhombohedral picture with the R3c space group. This study has confirmed that the BFO5 in single phase is the most optimized phase with the most stoichiometry as compared to pure BFO and BFO10. For surface morphology, FESEM along with EDAX technique was used. The Raman spectrometer with a 532 nm laser was used to study the vibrational modes available in the samples. To understand the super-capacitive behaviour of the synthesized samples, a detailed electrochemical analysis was performed with the help of cyclic-voltammetry. According to the recording of cyclic-voltammetry data for the samples BFO, BFO5, and BFO10 with the scan frequencies 10, 20, 50, and 100 mV/s, it was found that the BFO5 (i.e. Bi1+xFeO3 with x = 0.05) electrode has displayed the highest capacitive reaction in comparison to the pure BFO and BFO10 electrodes. In addition, the BFO5 has shown the highest specific capacitance. The impedance analysis was also performed to study the grain properties of the samples via Nyquist plots considering the equivalent ac circuit, which confirmed that the BFO5 nanoparticles display the greatest grain resistance. Further, the justified Nyquist plots with the fitted data have confirmed the best performance of BFO5. According to the GCD (galvanostatic charge–discharge) study, the BFO5 electrode has demonstrated impressive cycle stability. As evaluated at 1Ag−1, the BFO5 electrode has demonstrated outstanding cyclic stability, with > 94% capacitance retention over 2000 cycles. Thus, in conclusion, all these characterization results suggest that the Bi1+xFeO3 with x = 0.05 is a very suitable composition for supercapacitors application.
Vorheriger Artikel Optimization of BaSnO3 as a compact layer for enhancement of DSSC performance using response surface methodology/Box–Behnken design
Nächster Artikel First principles study of nonlinear optical, electronic properties and absorption spectra of some anti-HIV drugs: a comparative approach

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Metadaten
Titel
Study of structural, surface morphology, Raman spectroscopy, and electrochemical properties of Bi1+xFeO3 nanoparticles for usage in supercapacitors
verfasst von
Garima Srivastava
Shalendra Kumar
S. Z. Hashmi
Ravina
A. M. Quraishi
Saurabh Dalela
Faheem Ahmed
Kavita Kumari
B. H. Koo
P. A. Alvi
Publikationsdatum
01.12.2023
Verlag
Springer US
Erschienen in
Optical and Quantum Electronics / Ausgabe 14/2023
Print ISSN: 0306-8919
Elektronische ISSN: 1572-817X
DOI
https://doi.org/10.1007/s11082-023-05517-x

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