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Journal of Materials Science
Erschienen in: Journal of Materials Science 23/2018

02.08.2018 | Chemical routes to materials

Suzuki–Miyaura reaction and solventfree oxidation of benzyl alcohol by Pd/nitrogen-doped CNTs catalyst

verfasst von: Ayomide H. Labulo, Bernard Omondi, Vincent O. Nyamori

Erschienen in: Journal of Materials Science | Ausgabe 23/2018

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Abstract

Suzuki–Miyaura C–C coupling reactions were investigated with Pd/nitrogen-doped carbon nanotubes (Pd/N-CNTs) as a catalyst. Also, the same catalyst was examined for the solventfree oxidation of benzyl alcohol to benzaldehyde. Nitrogen-doped carbon nanotubes (N-CNTs) were synthesized from 1-ferrocenylmethyl(2-methylimidazole) and benzophenone via a chemical vapour deposition technique. Acetonitrile was used as a solvent and source of both carbon and nitrogen constituents of N-CNTs. Pd nanoparticles (Pd NPs) were successfully dispersed on N-CNTs via a metal organic chemical vapour deposition method. SEM, TEM, XRD, elemental analysis and ICP-OES measurements were used to characterize the nanomaterials. From the TEM analysis, it was observed that Pd NPs were spherical and with particle sizes ranging from 3 to 8 nm. For Suzuki C–C coupling reactions, phenylboronic acid, aryl halide, Pd/N-CNTs catalyst and a base (NaOAc, K2PO4, K2CO3, NaOH, Et3N and Na2CO3) were used. The optimized experiments indicate that K2CO3, as the base, and ethanol/water (1:1 v/v, 10 mL) mixture, as a solvent, are the best reaction conditions. The solventfree oxidation reactions of benzyl alcohol were also done with Pd/N-CNTs catalyst and benzyl alcohol as a substrate. In both sets of reactions, C–C coupling and oxidation, the increase in pyrrolic nitrogen species was found to be responsible for higher catalytic activities of Pd/N-CNT catalysts, and this was attributed to the ease of Pd NP dispersion on N-CNTs, relative to pristine CNTs. Also, the higher catalytic activity of Pd/N-CNTs could be ascribed not only to the smaller Pd NP size or surface area, but to also the surface properties and the nature of the support when compared with the undoped counterpart, Pd/CNTs.
Vorheriger Artikel Assembly of WO3 nanosheets/Bi24O31Br10 nanosheets composites with superior photocatalytic activity for degradation of tetracycline hydrochloride
Nächster Artikel Fast-dissolving carvacrol/cyclodextrin inclusion complex electrospun fibers with enhanced thermal stability, water solubility, and antioxidant activity

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Metadaten
Titel
Suzuki–Miyaura reaction and solventfree oxidation of benzyl alcohol by Pd/nitrogen-doped CNTs catalyst
verfasst von
Ayomide H. Labulo
Bernard Omondi
Vincent O. Nyamori
Publikationsdatum
02.08.2018
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 23/2018
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-018-2748-8

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