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Journal of Materials Science
Erschienen in: Journal of Materials Science 2/2017

19.09.2016 | Original Paper

Synthesis and characterization of BiOI microspheres under standardized conditions

verfasst von: Adriana C. Mera, C. A. Rodríguez, M. F. Meléndrez, Héctor Valdés

Erschienen in: Journal of Materials Science | Ausgabe 2/2017

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Abstract

Bismuth oxyiodide (BiOI) has received much attention in the design of materials, because this material has proved its potential application in heterogeneous photocatalysis for environmental decontamination processes using visible light or simulated solar radiation. In this study, standard conditions and a reproducible method of solvothermal synthesis are established in order to obtain BiOI microspheres with higher photocatalytic activity in the degradation of gallic acid. Standard conditions of reaction temperature and reaction time turn out to be 126 °C and 18 h, respectively. In addition, results show that reaction temperature has a stronger influence on different properties of the BiOI, affecting the photocatalytic efficiency. BiOI materials were synthesized by solvothermal process using different ranges of reaction temperature (120–200 °C) and reaction time (12–24 h). Eleven experiments were designed, applying response surface methodology. The morphological, optical, and chemical properties of the best and worst material were determined using several techniques.
Vorheriger Artikel Concentration- and temperature-dependent fluorescent quenching and Judd–Ofelt analysis of Eu3+ in NaLaTi2O6 phosphors
Nächster Artikel Dopamine-modified poly(amino acid): an efficient near-infrared photothermal therapeutic agent for cancer therapy

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Metadaten
Titel
Synthesis and characterization of BiOI microspheres under standardized conditions
verfasst von
Adriana C. Mera
C. A. Rodríguez
M. F. Meléndrez
Héctor Valdés
Publikationsdatum
19.09.2016
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 2/2017
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-016-0390-x

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