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Erschienen in: Journal of Material Cycles and Waste Management 1/2018

17.03.2017 | ORIGINAL ARTICLE

Synthesis and characterization of zeolites NaA and NaX from coal gangue

verfasst von: Jianlong Chen, Xinwei Lu

Erschienen in: Journal of Material Cycles and Waste Management | Ausgabe 1/2018

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Abstract

Zeolites NaA and NaX were synthesized from initial coal gangue (milled sample) and pretreated coal gangue (calcinated and acid immersed sample) by an alkali fusion method prior to hydrothermal treatment, which started by mixing NaOH with coal gangue at an optimal weight ratio of nearly 1.2:1. Results show that zeolite NaA was successfully synthesized by alkali fusion at 650 and 950 °C from initial coal gangue, while zeolite NaX was synthesized by alkali fusion at 600 °C from pretreated coal gangue. Zeolites NaX with different specific surface area, external surface area, surface area of micropore and crystallinity were synthesized when the molar ratio of SiO2/Al2O3 in raw materials ranges from 3.46 to 10.0.

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Literatur
1.
Zurück zum Zitat Mandal A, Sengupta D (2003) Radioelemental study of Kolaghat, thermal power plant, West Bengal, India: possible environmental hazards. Environ Geol 44:180–186 Mandal A, Sengupta D (2003) Radioelemental study of Kolaghat, thermal power plant, West Bengal, India: possible environmental hazards. Environ Geol 44:180–186
2.
Zurück zum Zitat Bhuiyan MAH, Parvez L, Islam MA, Dampare SB, Suzuki S (2010) Heavy metal pollution of coal mine-affected agricultural soils in the northern part of Bangladesh. J Hazard Mater 173:384–392CrossRef Bhuiyan MAH, Parvez L, Islam MA, Dampare SB, Suzuki S (2010) Heavy metal pollution of coal mine-affected agricultural soils in the northern part of Bangladesh. J Hazard Mater 173:384–392CrossRef
3.
Zurück zum Zitat Lu X, Jia X, Wang L (2006) Natural radioactivity of coal and its by-productions in the Baoji coal-fired power plant, China. Currt Sci 91:1508–1511 Lu X, Jia X, Wang L (2006) Natural radioactivity of coal and its by-productions in the Baoji coal-fired power plant, China. Currt Sci 91:1508–1511
4.
Zurück zum Zitat Cao J, Liu Y, Guo G (2004) The current situation in comprehensive utilization of gangue. Tech Equi Environ Pollut Contr 5(1):19–22 (in Chinese) Cao J, Liu Y, Guo G (2004) The current situation in comprehensive utilization of gangue. Tech Equi Environ Pollut Contr 5(1):19–22 (in Chinese)
5.
Zurück zum Zitat Liang A, Kuang S, Ding H (2004) The discussion of comprehensive utilization of coal gangue. Chine Resour Compre Utiliz 2:11–14 (in Chinese) Liang A, Kuang S, Ding H (2004) The discussion of comprehensive utilization of coal gangue. Chine Resour Compre Utiliz 2:11–14 (in Chinese)
6.
Zurück zum Zitat Xu H, Song W, Cao W, Shao G, Lu H, Yang D, Chen D, Zhang R (2016) Utilization of coal gangue for the production of brick. J Mater Cycles Waste Manag. doi:10.1007/s10163-016-0521-0 Xu H, Song W, Cao W, Shao G, Lu H, Yang D, Chen D, Zhang R (2016) Utilization of coal gangue for the production of brick. J Mater Cycles Waste Manag. doi:10.​1007/​s10163-016-0521-0
7.
Zurück zum Zitat Li D, Song X, Gong C, Pan Z (2006) Research on cementitious behavior and mechanism of pozzolanic cement with coal gangue. Cem Concr Res 36:1752–1759CrossRef Li D, Song X, Gong C, Pan Z (2006) Research on cementitious behavior and mechanism of pozzolanic cement with coal gangue. Cem Concr Res 36:1752–1759CrossRef
8.
Zurück zum Zitat Jameson CJ, Jameson AK, Lim HM (1997) Competitive adsorption of xenon and krypton in zeolite NaA: 129Xe nuclear magnetic resonance studies and grand canonical Monte Carlo simulations. J Chem Phys 107:4364–4372CrossRef Jameson CJ, Jameson AK, Lim HM (1997) Competitive adsorption of xenon and krypton in zeolite NaA: 129Xe nuclear magnetic resonance studies and grand canonical Monte Carlo simulations. J Chem Phys 107:4364–4372CrossRef
9.
Zurück zum Zitat Darkrim F, Aoufi A, Malbrunot P, Levesque D (2000) Hydrogen adsorption in the NaA zeolite: a comparison between numerical simulations and experiments. J Chem Phys 112:5991–5999CrossRef Darkrim F, Aoufi A, Malbrunot P, Levesque D (2000) Hydrogen adsorption in the NaA zeolite: a comparison between numerical simulations and experiments. J Chem Phys 112:5991–5999CrossRef
10.
Zurück zum Zitat Huang Y, Wang K, Dong D, Li D, Hill MR, Hill AJ, Wang H (2010) Synthesis of hierarchical porous zeolite NaY particles with controllable particle sizes. Micropor Mesopor Mater 127:167–175CrossRef Huang Y, Wang K, Dong D, Li D, Hill MR, Hill AJ, Wang H (2010) Synthesis of hierarchical porous zeolite NaY particles with controllable particle sizes. Micropor Mesopor Mater 127:167–175CrossRef
11.
Zurück zum Zitat Ojha K, Pradhan NC, Samanta AN (2004) Zeolite from fly ash: synthesis and characterization. Bull Mater Sci 27:555–564CrossRef Ojha K, Pradhan NC, Samanta AN (2004) Zeolite from fly ash: synthesis and characterization. Bull Mater Sci 27:555–564CrossRef
12.
Zurück zum Zitat Chandrasekhar S, Pramada PN (1999) Investigation on the synthesis of zeolite NaX from Kerala kaolin. J Poro Mater 6:283–297CrossRef Chandrasekhar S, Pramada PN (1999) Investigation on the synthesis of zeolite NaX from Kerala kaolin. J Poro Mater 6:283–297CrossRef
13.
Zurück zum Zitat Zhan BZ, White MA, Lumsden M, Mueller-Neuhaus J, Robertson KN, Cameron TS, Gharghouri M (2002) Control of particle size and surface properties of crystals of NaX zeolite. Chem Mater 14:3636–3642CrossRef Zhan BZ, White MA, Lumsden M, Mueller-Neuhaus J, Robertson KN, Cameron TS, Gharghouri M (2002) Control of particle size and surface properties of crystals of NaX zeolite. Chem Mater 14:3636–3642CrossRef
14.
Zurück zum Zitat Ghorai PK, Sluiter M, Yashonath S, Kawazoe Y (2006) Intermolecular potential for methane in zeolite A and Y: adsorption isotherm and related properties. Solid State Sci 8:248–258CrossRef Ghorai PK, Sluiter M, Yashonath S, Kawazoe Y (2006) Intermolecular potential for methane in zeolite A and Y: adsorption isotherm and related properties. Solid State Sci 8:248–258CrossRef
15.
Zurück zum Zitat Nibou D, Mekatel H, Amokrane S, Barkat M, Trari M (2010) Adsorption of Zn2+ ions onto NaA and NaX zeolites: kinetic, equilibrium and thermodynamic studies. J Hazard Mater 173:637–646CrossRef Nibou D, Mekatel H, Amokrane S, Barkat M, Trari M (2010) Adsorption of Zn2+ ions onto NaA and NaX zeolites: kinetic, equilibrium and thermodynamic studies. J Hazard Mater 173:637–646CrossRef
16.
Zurück zum Zitat Zhao Y, Zhang B, Zhang X, Wang J, Liu J, Chen R (2010) Preparation of highly ordered cubic NaA zeolite from halloysite mineral for adsorption of ammonium ions. J Hazard Mater 178:658–664CrossRef Zhao Y, Zhang B, Zhang X, Wang J, Liu J, Chen R (2010) Preparation of highly ordered cubic NaA zeolite from halloysite mineral for adsorption of ammonium ions. J Hazard Mater 178:658–664CrossRef
17.
Zurück zum Zitat Bouizi Y, Paillaud JL, Simon L, Valtchev V (2007) Seeded synthesis of very high silica zeolite A. Chem Mater 19:652–654CrossRef Bouizi Y, Paillaud JL, Simon L, Valtchev V (2007) Seeded synthesis of very high silica zeolite A. Chem Mater 19:652–654CrossRef
18.
Zurück zum Zitat Sasaki H, Oumi Y, Sadakane M, Sano T (2010) Synthesis of single phase Ca-α-SiAlON using Y-type zeolite. J Eur Ceram Soc 30:1537–1541CrossRef Sasaki H, Oumi Y, Sadakane M, Sano T (2010) Synthesis of single phase Ca-α-SiAlON using Y-type zeolite. J Eur Ceram Soc 30:1537–1541CrossRef
19.
Zurück zum Zitat Braschi I, Blasioli S, Gigli L, Gessa CE, Alberti A, Martucci A (2010) Removal of sulfonamide antibiotics from water: evidence of adsorption into an organophilic zeolite Y by its structural modifications. J Hazard Mater 178:218–225CrossRef Braschi I, Blasioli S, Gigli L, Gessa CE, Alberti A, Martucci A (2010) Removal of sulfonamide antibiotics from water: evidence of adsorption into an organophilic zeolite Y by its structural modifications. J Hazard Mater 178:218–225CrossRef
20.
Zurück zum Zitat Inada M, Eguchi Y, Enomoto N, Hojo J (2005) Synthesis of zeolite from coal fly ash with different silica-alumina composition. Fuel 84:299–304CrossRef Inada M, Eguchi Y, Enomoto N, Hojo J (2005) Synthesis of zeolite from coal fly ash with different silica-alumina composition. Fuel 84:299–304CrossRef
21.
Zurück zum Zitat Tanaka H, Furusawa S, Hino R (2002) Synthesis, characterization, and formation process of NaX zeolite from coal fly ash. J Mater Synth Proc 10:143–148CrossRef Tanaka H, Furusawa S, Hino R (2002) Synthesis, characterization, and formation process of NaX zeolite from coal fly ash. J Mater Synth Proc 10:143–148CrossRef
22.
Zurück zum Zitat Tanaka H, Miyagawa A, Eguchi H, Hino R (2004) Synthesis of a single-phase Na-A zeolite from coal fly ash by dialysis. Ind Eng Chem Res 43:6090–6094CrossRef Tanaka H, Miyagawa A, Eguchi H, Hino R (2004) Synthesis of a single-phase Na-A zeolite from coal fly ash by dialysis. Ind Eng Chem Res 43:6090–6094CrossRef
23.
Zurück zum Zitat Zhang X, Tang D, Zhang M, Yang R (2013) Synthesis of NaX zeolite: Influence of crystallization time, temperature and batch molar ratio SiO2/Al2O3 on the particulate properties of zeolite crystals. Pow Tech 235:322–328CrossRef Zhang X, Tang D, Zhang M, Yang R (2013) Synthesis of NaX zeolite: Influence of crystallization time, temperature and batch molar ratio SiO2/Al2O3 on the particulate properties of zeolite crystals. Pow Tech 235:322–328CrossRef
24.
Zurück zum Zitat Fotovat F, Kazemian H, Kazemeini M (2009) Synthesis of Na-A and faujasitic zeolites from high silicon fly ash. Mater Res Bull 44:913–917CrossRef Fotovat F, Kazemian H, Kazemeini M (2009) Synthesis of Na-A and faujasitic zeolites from high silicon fly ash. Mater Res Bull 44:913–917CrossRef
25.
Zurück zum Zitat Wang MR, Jia DC, He PG, Zhou Y (2010) Influence of calcination temperature of kaolin on the structure and properties of final geopolymer. Mater Lett 64:2551–2554CrossRef Wang MR, Jia DC, He PG, Zhou Y (2010) Influence of calcination temperature of kaolin on the structure and properties of final geopolymer. Mater Lett 64:2551–2554CrossRef
26.
Zurück zum Zitat Hollman GG, Steenbruggen G, Janssen JM (1999) A two-step process for the synthesis of zeolites from coal fly ash. Fuel 78:1225–1230CrossRef Hollman GG, Steenbruggen G, Janssen JM (1999) A two-step process for the synthesis of zeolites from coal fly ash. Fuel 78:1225–1230CrossRef
27.
Zurück zum Zitat Shigemoto N, Hayashi H, Miyaura K (1993) Selective formation of Na-X zeolite from coal fly ash by fusion with sodium hydroxide prior to hydrothermal reaction. J Mater Sci 28:4781–4786CrossRef Shigemoto N, Hayashi H, Miyaura K (1993) Selective formation of Na-X zeolite from coal fly ash by fusion with sodium hydroxide prior to hydrothermal reaction. J Mater Sci 28:4781–4786CrossRef
28.
Zurück zum Zitat Tan WC, Yap SY, Matsumoto A, Othman R, Yeoh FY (2011) Synthesis and characterization of zeolites NaA and NaY from rice husk ash. Adsorption 17:863–868CrossRef Tan WC, Yap SY, Matsumoto A, Othman R, Yeoh FY (2011) Synthesis and characterization of zeolites NaA and NaY from rice husk ash. Adsorption 17:863–868CrossRef
29.
Zurück zum Zitat Szostak R (1997) Molecular sieves: principles of synthesis and identification. Springer, New York Szostak R (1997) Molecular sieves: principles of synthesis and identification. Springer, New York
30.
Zurück zum Zitat Ríos CA, Williams CD, Fullen MA (2009) Nucleation and growth history of zeolite LTA synthesized from kaolinite by two different methods. Appl Clay Sci 42:446–454CrossRef Ríos CA, Williams CD, Fullen MA (2009) Nucleation and growth history of zeolite LTA synthesized from kaolinite by two different methods. Appl Clay Sci 42:446–454CrossRef
31.
Zurück zum Zitat Belver C, Bañares Muñoz MA, Vicente MA (2002) Chemical activation of a kaolinite under acid and alkaline conditions. Chem Mater 14:2033–2043CrossRef Belver C, Bañares Muñoz MA, Vicente MA (2002) Chemical activation of a kaolinite under acid and alkaline conditions. Chem Mater 14:2033–2043CrossRef
32.
Zurück zum Zitat Qiu L, Laws PA, Zhan BZ, White MA (2006) Thermodynamic investigations of zeolites NaX and NaY. Can J Chem 84:134–139CrossRef Qiu L, Laws PA, Zhan BZ, White MA (2006) Thermodynamic investigations of zeolites NaX and NaY. Can J Chem 84:134–139CrossRef
Metadaten
Titel
Synthesis and characterization of zeolites NaA and NaX from coal gangue
verfasst von
Jianlong Chen
Xinwei Lu
Publikationsdatum
17.03.2017
Verlag
Springer Japan
Erschienen in
Journal of Material Cycles and Waste Management / Ausgabe 1/2018
Print ISSN: 1438-4957
Elektronische ISSN: 1611-8227
DOI
https://doi.org/10.1007/s10163-017-0605-5

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