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01.12.2018 | Research Paper

The self-assembly of DyF₃ nanoparticles synthesized by chloride-based route

verfasst von: E. M. Alakshin, E. I. Kondratyeva, D. S. Nuzhina, M. F. Iakovleva, V. V. Kuzmin, K. R. Safiullin, A. T. Gubaidullin, T. Kikitsu, K. Kono, A. V. Klochkov, M. S. Tagirov

Erschienen in: Journal of Nanoparticle Research | Ausgabe 12/2018

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Abstract

The series of DyF₃ nanoparticles was synthesized for the first time by a chloride-based route, using the water-soluble dysprosium chloride hexahydrate as a precursor. The synthesized nanoparticles have sizes of 3 to 7 nm, which is the smallest reported size for DyF₃ nanoparticles. The influence of precursor concentration in an aqueous solution prior to the chemical reaction on the size of nanoparticles was studied. The influence of microwave-assisted hydrothermal treatment was also studied. The analysis of transmission electron microscopy (TEM) data revealed no correlation between the size of synthesized nanoparticles and the concentration of the aqueous solution. The AC/DC magnetic susceptibility of DyF₃ nanoparticles was measured. The dipolar ferromagnetic transition for this sample was not observed down to 1.8 K that can be possibly explained by onset of superparamagnetism. The self-assembly of DyF₃ nanoparticles was observed for the first time by analysis of XRD and TEM data and the evidence of superlattice formation along (020) and (210) lattice planes over the size of 20–30 nm (4–5 nanoparticles) was obtained.

Vorheriger Artikel Exposure media a critical factor for controlling dissolution of CuO nanoparticles

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Titel: The self-assembly of DyF3 nanoparticles synthesized by chloride-based route
verfasst von: E. M. Alakshin
E. I. Kondratyeva
D. S. Nuzhina
M. F. Iakovleva
V. V. Kuzmin
K. R. Safiullin
A. T. Gubaidullin
T. Kikitsu
K. Kono
A. V. Klochkov
M. S. Tagirov
Publikationsdatum: 01.12.2018
Verlag: Springer Netherlands
Erschienen in: Journal of Nanoparticle Research / Ausgabe 12/2018
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-018-4426-9

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