Skip to main content
Fachgebiete
Automobil + Motoren Bauwesen + Immobilien Business IT + Informatik Elektrotechnik + Elektronik Energie + Nachhaltigkeit Finance + Banking Management + Führung Marketing + Vertrieb Maschinenbau + Werkstoffe Versicherung + Risiko
DE
EN
Themenseiten
Organisationspsychologie Projektmanagement Marketing Smart Manufacturing
Bücher
Zeitschriften
Weitere Formate
Podcasts Webinare Technik Webinare Wirtschaft Kongresse Veranstaltungskalender Awards
Jetzt Einzelzugang starten
Zugang für Unternehmen
Referenzkunden
MTZ-Fachkongress

Antriebe und Energiesysteme von morgen


Austausch von Automobil- und Energiewirtschaft

Am 14./15. Mai geht es in Chemnitz um die Mobilitätswende durch Elektro- und Wasserstofffahrzeuge.
Erweiterte Suche
Anmelden
nach oben
Journal of Nanoparticle Research
Erschienen in: Journal of Nanoparticle Research 10/2015

01.10.2015 | Research Paper

Two-dimensional FeS nanoflakes: synthesis and application to electrochemical sensor for mercury(II) ions

verfasst von: Ligang Wang, Yizhe Zhao, Yang Tian

Erschienen in: Journal of Nanoparticle Research | Ausgabe 10/2015

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

We report a facile solvothermal method to prepare troilite FeS two-dimensional nanoflakes. The morphology and size were observed by transmission electron microscopy (TEM), the intrinsic crystallography of the obtained FeS nanoflakes was characterized by powder X-ray diffraction and high-resolution TEM, and the composition was analyzed by X-ray photoelectron spectroscopy. Furthermore, the prepared FeS nanoflakes were successfully modified on an electrode to fabricate a sensor for Hg2+ detection. The electrochemical detection mechanism was expected that Hg2+ ions interact with FeS to form stable HgS in the nanoflakes, which provided a sensitive approach for electrochemical detection of Hg2+ selectively. The detection limit for Hg2+ was 4 nM in a PBS solution. The prepared sensor based on the FeS nanoflakes shows the better performance than that with bulk-FeS materials for the Hg2+ detection. The proposed FeS nanoflakes also exhibit good applicability for monitoring Hg2+ in real water specimens.

Graphical Abstract

Vorheriger Artikel Scalable fractionation of iron oxide nanoparticles using a CO2 gas-expanded liquid system
Nächster Artikel Impact of environmental conditions on aggregation kinetics of hematite and goethite nanoparticles

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Jetzt informieren
Anhänge
Nur mit Berechtigung zugänglich
Literatur
Abollino O, Giacomino A, Malandrino M, Piscionieri G, Mentasti E (2008) Determination of mercury by anodic stripping voltammetry with a gold nanoparticle-modified glassy carbon electrode. Electroanalysis 20:75–83CrossRef
An JH, Park SJ, Kwon OS, Bae J, Jang J (2013) High-performance flexible graphene aptasensor for mercury detection in mussels. ACS Nano 7:10563–10571CrossRef
Arulraj AD, Vijayan M, Samseya J, Vasantha V (2014) A simple and highly sensitive electrochemically reduced p-nitrobenzoic acid film modified sensor for determination of mercury. Electroanalysis 26:2773–2782CrossRef
Behra P, Bonnissel-Gissinger P, Alnot M, Revel R, Ehrhardt JJ (2001) XPS and XAS study of the sorption of Hg(II) onto pyrite. Langmuir 17:3970–3979CrossRef
Bian P, Xing L, Liu Z, Ma Z (2014) Functionalized-tryptophan stabilized fluorescent Ag nanoclusters: synthesis and its application as Hg2+ ions sensor. Sens Actuators B 203:252–257CrossRef
Bone SE, Bargar JR, Sposito G (2014) Mackinawite (FeS) reduces mercury (II) under sulfidic conditions. Environ Sci Technol 48:10681–10689CrossRef
Boudouh H, Guessasma S, Essehli R, Aissat A (2012) Monte carlo simulation of ion-exchange response of copper sulfide ion selective electrode for metal pollutant detection. J Electrochem Soc 159:D148–D154CrossRef
Cabán-Acevedo M, Liang D, Chew KS, DeGrave JP, Kaiser NS, Jin S (2013) Synthesis, characterization, and variable range hopping transport of pyrite (FeS2) nanorods, nanobelts, and nanoplates. ACS Nano 7:1731–1739CrossRef
Cummins DR, Russell HB, Jasinski JB, Menon M, Sunkara MK (2013) Iron sulfide (FeS) nanotubes using sulfurization of hematite nanowires. Nano Lett 13:2423–2430CrossRef
Dai X, Wildgoose GG, Salter C, Crossley A, Compton RG (2006) Electroanalysis using macro-, micro-, and nanochemical architectures on electrode surfaces. Bulk surface modification of glassy carbon microspheres with gold nanoparticles and their electrical wiring using carbon nanotubes. Anal Chem 78:6102–6108CrossRef
Duan J, Yang M, Lai Y, Yuan J, Zhan J (2012) A colorimetric and surface-enhanced Raman scattering dual-signal sensor for Hg2+ based on Bismuthiol II-capped gold nanoparticles. Anal Chim Acta 723:88–93CrossRef
Dutta AK, Maji SK, Srivastava DN, Mondal A, Biswas P, Paul P, Adhikary B (2012) Synthesis of FeS and FeSe nanoparticles from a single source precursor: a study of their photocatalytic activity, peroxidase-like behavior, and electrochemical sensing of H2O2. ACS Appl Mater Interfaces 4:1919–1927CrossRef
Feng J, Sun X, Wu C, Peng L, Lin C, Hu S, Yang J, Xie Y (2011) Metallic few-layered VS2 ultrathin nanosheets: high two-dimensional conductivity for in-plane supercapacitors. J Am Chem Soc 133:17832–17838CrossRef
Fu X-C, Chen X, Guo Z, Kong L-T, Wang J, Liu J-H, Huang X-J (2010) Three-dimensional gold micro-/nanopore arrays containing 2-mercaptobenzothiazole molecular adapters allow sensitive and selective stripping voltammetric determination of trace mercury (II). Electrochim Acta 56:463–469CrossRef
Gao C, Wang Q, Gao F, Gao F (2014) A high-performance aptasensor for mercury (II) based on the formation of a unique ternary structure of aptamer–Hg2+–neutral red. Chem Commun 50:9397–9400CrossRef
Han DS, Orillano M, Khodary A, Duan Y, Batchelor B, Abdel-Wahab A (2014) Reactive iron sulfide (FeS)-supported ultrafiltration for removal of mercury (Hg(II)) from water. Water Res 53:310–321CrossRef
Hyun SP, Davis JA, Sun K, Hayes KF (2012) Uranium (VI) reduction by iron (II) monosulfide mackinawite. Environ Sci Technol 46:3369–3376CrossRef
Janegitz BC, Figueiredo-Filho LCS, Marcolino-Junior LH, Souza SPN, Pereira-Filho ER, Fatibello-Filho O (2011) Development of a carbon nanotubes paste electrode modified with crosslinked chitosan for cadmium(II) and mercury(II) determination. J Electroanal Chem 660:209–216CrossRef
Jorn C, Lai EP, Sadeghi S (2004) Surface plasmon resonance sensor for Hg(II) detection by binding interactions with polypyrrole and 2-mercaptobenzothiazole. Sens Actuators B 101:236–241CrossRef
Kaiser H (1973) Guiding concepts relating to trace analysis. Pure Appl Chem 34:35–62CrossRef
Khan MR, Khoo SB (2001) Optimization of the simultaneous batch determinations of Bi(III), Hg(II) and Cu (II) at an epoxy–graphite electrode bulk modified with 2-mercaptobenzothiazole. Analyst 126:2172–2177CrossRef
Kirsch R, Fellhauer D, Altmaier M, Neck V, Rossberg A, Fanghänel T, Charlet L, Scheinost AC (2011) Oxidation state and local structure of plutonium reacted with magnetite, mackinawite, and chukanovite. Environ Sci Technol 45:7267–7274CrossRef
Kumar Jena B, Retna Raj C (2008) Gold nanoelectrode ensembles for the simultaneous electrochemical detection of ultratrace arsenic, mercury, and copper. Anal Chem 80:4836–4844CrossRef
Liu J, Valsaraj KT, Delaune R (2009) Inhibition of mercury methylation by iron sulfides in an anoxic sediment. Environ Eng Sci 26:833–840CrossRef
Lou X, Zhao T, Liu R, Ma J, Xiao Y (2013) Self-assembled DNA monolayer buffered dynamic ranges of mercuric electrochemical sensor. Anal Chem 85:7574–7580CrossRef
Macpherson HA, Stoldt CR (2012) Iron Pyrite Nanocubes: size and Shape Considerations for Photovoltaic Application. ACS Nano 6:8940–8949CrossRef
Miao P, Liu L, Li Y, Li G (2009) A novel electrochemical method to detect mercury (II) ions. Electrochem Commun 11:1904–1907CrossRef
Pan D, Wang Y, Chen Z, Lou T, Qin W (2009) Nanomaterial/ionophore-based electrode for anodic stripping voltammetric determination of lead: an electrochemical sensing platform toward heavy metals. Anal Chem 81:5088–5094CrossRef
Rui X, Tan H, Yan Q (2014) Nanostructured metal sulfides for energy storage. Nanoscale 6:9889–9924CrossRef
Safavi A, Farjami E (2011) Construction of a carbon nanocomposite electrode based on amino acids functionalized gold nanoparticles for trace electrochemical detection of mercury. Anal Chim Acta 688:43–48CrossRef
Shi W, Ma H (2008) Rhodamine B thiolactone: a simple chemosensor for Hg2+ in aqueous media. Chem Commun 16:1856–1858CrossRef
Song Y, Swain GM (2007) Development of a method for total inorganic arsenic analysis using anodic stripping voltammetry and a Au-coated, diamond thin-film electrode. Anal Chem 79:2412–2420CrossRef
Sun Y, Sun Z, Gao S, Cheng H, Liu Q, Piao J, Yao T, Wu C, Hu S, Wei S (2012) Fabrication of flexible and freestanding zinc chalcogenide single layers. Nat Commun 3:1057CrossRef
Tian Y, Yu B, Li X, Li K (2011) Facile solvothermal synthesis of monodisperse Fe3 O4 nanocrystals with precise size control of one nanometre as potential MRI contrast agents. J Mater Chem 21:2476–2481CrossRef
Wang H, Yuan H, Hong SS, Li Y, Cui Y (2015) Physical and chemical tuning of two-dimensional transition metal dichalcogenides. Chem Soc Rev 44(9):2664–2680CrossRef
WookáPark J, JooáPark S, SeokáKwon O (2014) High-performance Hg2+ FET-type sensors based on reduced graphene oxide–polyfuran nanohybrids. Analyst 139:3852–3855CrossRef
Xu H, Zeng L, Xing S, Shi G, Xian Y, Jin L (2008) Microwave-radiated synthesis of gold nanoparticles/carbon nanotubes composites and its application to voltammetric detection of trace mercury (II). Electrochem Commun 10:1839–1843CrossRef
Xu C, Zeng Y, Rui X, Xiao N, Zhu J, Zhang W, Chen J, Liu W, Tan H, Hng HH, Yan Q (2012) Controlled soft-template synthesis of ultrathin c@fes nanosheets with high-li-storage performance. ACS Nano 6:4713–4721CrossRef
Zhang Y, Zhao H, Wu Z, Xue Y, Zhang X, He Y, Li X, Yuan Z (2013) A novel graphene-DNA biosensor for selective detection of mercury ions. Biosens Bioelectron 48:180–187CrossRef
Zhao C, Shao C, Li M, Jiao K (2007) Flow-injection analysis of glucose without enzyme based on electrocatalytic oxidation of glucose at a nickel electrode. Talanta 71:1769–1773CrossRef
Zheng J, Cao Y, Cheng C, Chen C, Yan R-W, Huai H-X, Dong Q-F, Zheng M-S, Wang C-C (2014) Facile synthesis of Fe3S4 hollow spheres with high-performance for lithium-ion batteries and water treatment. J Mater Chem A 2:19882–19888CrossRef
Zhou Y, Dong H, Liu L, Li M, Xiao K, Xu M (2014) Selective and sensitive colorimetric sensor of mercury(II) based on gold nanoparticles and 4-mercaptophenylboronic acid. Sens Actuators B 196:106–111CrossRef
Zhu Z, Su Y, Li J, Li D, Zhang J, Song S, Zhao Y, Li G, Fan C (2009) Highly sensitive electrochemical sensor for mercury(II) ions by using a mercury-specific oligonucleotide probe and gold nanoparticle-based amplification. Anal Chem 81:7660–7666CrossRef
Metadaten
Titel
Two-dimensional FeS nanoflakes: synthesis and application to electrochemical sensor for mercury(II) ions
verfasst von
Ligang Wang
Yizhe Zhao
Yang Tian
Publikationsdatum
01.10.2015
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 10/2015
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-015-3197-9

Weitere Artikel der Ausgabe 10/2015

Journal of Nanoparticle Research 10/2015 Zur Ausgabe

Research Paper

Shape-control by microwave-assisted hydrothermal method for the synthesis of magnetite nanoparticles using organic additives

Research Paper

Preparation of a novel KCC-1/nylon 6 nanocomposite via electrospinning technique

Research Paper

Colloid electrostatic self-assembly synthesis of SnO2/graphene nanocomposite for supercapacitors

Research Paper

Enhanced stability and dissolution of CuO nanoparticles by extracellular polymeric substances in aqueous environment

Research Paper

Enhanced dispersion stability and mobility of carboxyl-functionalized carbon nanotubes in aqueous solutions through strong hydrogen bonds

Research Paper

One-pot high-yield synthesis of single-crystalline gold nanorods using glycerol as a low-cost and eco-friendly reducing agent

Premium Partner

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen. 

    Zur Marktübersicht
    Bildnachweise