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Erschienen in: Journal of Nanoparticle Research 2/2010

01.02.2010 | Research Paper

Assisted spray pyrolysis production and characterisation of ZnO nanoparticles with narrow size distribution

verfasst von: S. Turner, S. M. F. Tavernier, G. Huyberechts, E. Biermans, S. Bals, K. J. Batenburg, G. Van Tendeloo

Erschienen in: Journal of Nanoparticle Research | Ausgabe 2/2010

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Abstract

Nano-sized ZnO particles with a narrow size distribution and high crystallinity were prepared from aqueous solutions with high concentrations of Zn2+ containing salts and citric acid in a conventional spray pyrolysis setup. Structure, morphology and size of the produced material were compared to ZnO material produced by simple spray pyrolysis of zinc nitrates in the same experimental setup. Using transmission electron microscopy and electron tomography it has been shown that citric acid-assisted spray pyrolysed material is made up of micron sized secondary particles comprising a shell of lightly agglomerated, monocrystalline primary ZnO nanoparticles with sizes in the 20–30 nm range, separable by a simple ultrasonic treatment step.

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Literatur
Zurück zum Zitat Bals S, Batenburg KJ, Verbeeck J, Sijbers J, Van Tendeloo G (2007) Quantitative three-dimensional reconstruction of catalyst particles for bamboo-like carbon nanotubes. Nano Lett 7:3669–3674CrossRefADS Bals S, Batenburg KJ, Verbeeck J, Sijbers J, Van Tendeloo G (2007) Quantitative three-dimensional reconstruction of catalyst particles for bamboo-like carbon nanotubes. Nano Lett 7:3669–3674CrossRefADS
Zurück zum Zitat Batenburg KJ, Bals S, Sijbers J, Kübel C, Kaiser U, Conorado EA, Midgley PA, Hernandez J-C, Van Tendeloo G (2009) 3D imaging of nanomaterials by discrete tomography. Ultramicroscopy (in press), corrected proof. Available online 31 January 2009, ISSN 0304-3991. doi:10.1016/j.ultramic.2009.01.009 Batenburg KJ, Bals S, Sijbers J, Kübel C, Kaiser U, Conorado EA, Midgley PA, Hernandez J-C, Van Tendeloo G (2009) 3D imaging of nanomaterials by discrete tomography. Ultramicroscopy (in press), corrected proof. Available online 31 January 2009, ISSN 0304-3991. doi:10.​1016/​j.​ultramic.​2009.​01.​009
Zurück zum Zitat Dang ZM, Fan LZ, Zhao SJ, Nan CW (2003) Preparation of nanosized ZnO and dielectric properties of composites filled with nanosized ZnO. Mater Sci Eng B 99:386–389CrossRef Dang ZM, Fan LZ, Zhao SJ, Nan CW (2003) Preparation of nanosized ZnO and dielectric properties of composites filled with nanosized ZnO. Mater Sci Eng B 99:386–389CrossRef
Zurück zum Zitat Gilbert P (1972) Iterative methods for the three-dimensional reconstruction of an object from projections. J Theor Biol 36:105–117CrossRefPubMed Gilbert P (1972) Iterative methods for the three-dimensional reconstruction of an object from projections. J Theor Biol 36:105–117CrossRefPubMed
Zurück zum Zitat Gregor J, Benson T (2008) Computational analysis and improvement of SIRT. IEEE Trans Med Imaging 27:918–924CrossRefPubMed Gregor J, Benson T (2008) Computational analysis and improvement of SIRT. IEEE Trans Med Imaging 27:918–924CrossRefPubMed
Zurück zum Zitat Kang HS, Kang YC, Park HD, Shul YG (2003) Morphology of particle prepared by spray pyrolysis from organic precursor solution. Mater Lett 57:1288–1294CrossRef Kang HS, Kang YC, Park HD, Shul YG (2003) Morphology of particle prepared by spray pyrolysis from organic precursor solution. Mater Lett 57:1288–1294CrossRef
Zurück zum Zitat Kodas TT, Hampden-Smith MJ (1999) Aerosol processing of materials. Wiley, New York Kodas TT, Hampden-Smith MJ (1999) Aerosol processing of materials. Wiley, New York
Zurück zum Zitat Lee JH, Ko KH, Park BO (2003) Electrical and optical properties of ZnO transparent conducting films by the sol–gel method. J Cryst Growth 247:119–125CrossRefADS Lee JH, Ko KH, Park BO (2003) Electrical and optical properties of ZnO transparent conducting films by the sol–gel method. J Cryst Growth 247:119–125CrossRefADS
Zurück zum Zitat Lee KK, Kang YC, Jung KY, Kim JH (2005) Preparation of nano-sized BaTiO3 particle by citric-acid assisted spray pyrolysis. J Alloy Compd 395:280–285CrossRef Lee KK, Kang YC, Jung KY, Kim JH (2005) Preparation of nano-sized BaTiO3 particle by citric-acid assisted spray pyrolysis. J Alloy Compd 395:280–285CrossRef
Zurück zum Zitat Lenggoro IW, Itoh Y, Lida N, Okuyama K (2003) Control of size and morphology in NiO particles prepared by a low-pressure spray pyrolysis. Mater Res Bull 38:1819–1827CrossRef Lenggoro IW, Itoh Y, Lida N, Okuyama K (2003) Control of size and morphology in NiO particles prepared by a low-pressure spray pyrolysis. Mater Res Bull 38:1819–1827CrossRef
Zurück zum Zitat Look DC (2001) Recent advances in ZnO materials and devices. Mater Sci Eng B 80:383–387CrossRef Look DC (2001) Recent advances in ZnO materials and devices. Mater Sci Eng B 80:383–387CrossRef
Zurück zum Zitat Panatarani C, Lenggoro IW, Okuyama K (2003) Synthesis of single crystalline ZnO nanoparticles by salt-assisted spray pyrolysis. J Nanopart Res 5:47–53CrossRef Panatarani C, Lenggoro IW, Okuyama K (2003) Synthesis of single crystalline ZnO nanoparticles by salt-assisted spray pyrolysis. J Nanopart Res 5:47–53CrossRef
Zurück zum Zitat Singh P, Kumar A, Deepak DK (2007) Growth and characterization of ZnO nanocrystalline thin films and nanopowder via low-cost ultrasonic spray pyrolysis. J Cryst Growth 306:303–310CrossRefADS Singh P, Kumar A, Deepak DK (2007) Growth and characterization of ZnO nanocrystalline thin films and nanopowder via low-cost ultrasonic spray pyrolysis. J Cryst Growth 306:303–310CrossRefADS
Zurück zum Zitat Tian ZR, Voigt JA, Liu J, Mckenzie B, McDermott MJ, Rodriguez MA, Konishi H, Xu H (2003) Complex and oriented ZnO nanostructures. Nat Mat 2(12):821–826CrossRef Tian ZR, Voigt JA, Liu J, Mckenzie B, McDermott MJ, Rodriguez MA, Konishi H, Xu H (2003) Complex and oriented ZnO nanostructures. Nat Mat 2(12):821–826CrossRef
Zurück zum Zitat Wang XD, Summers CJ, Wang ZL (2004) Large-scale hexagonal-patterned growth of aligned ZnO nanorods for nano-optoelectronics and nanosensor arrays. Nano Lett 4:423–426CrossRefADS Wang XD, Summers CJ, Wang ZL (2004) Large-scale hexagonal-patterned growth of aligned ZnO nanorods for nano-optoelectronics and nanosensor arrays. Nano Lett 4:423–426CrossRefADS
Zurück zum Zitat Xia B, Lenggoro IW, Okuyama K (2001) Novel route to nanoparticle synthesis by salt-assisted aerosol decomposition. Adv Mater 13:1579–1582CrossRef Xia B, Lenggoro IW, Okuyama K (2001) Novel route to nanoparticle synthesis by salt-assisted aerosol decomposition. Adv Mater 13:1579–1582CrossRef
Zurück zum Zitat Yang Y, Chen H, Zhao B, Bao X (2004) Size control of ZnO nanoparticles via thermal decomposition of zinc acetate coated on organic additives. J Cryst Growth 263:447–453CrossRefADS Yang Y, Chen H, Zhao B, Bao X (2004) Size control of ZnO nanoparticles via thermal decomposition of zinc acetate coated on organic additives. J Cryst Growth 263:447–453CrossRefADS
Metadaten
Titel
Assisted spray pyrolysis production and characterisation of ZnO nanoparticles with narrow size distribution
verfasst von
S. Turner
S. M. F. Tavernier
G. Huyberechts
E. Biermans
S. Bals
K. J. Batenburg
G. Van Tendeloo
Publikationsdatum
01.02.2010
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 2/2010
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-009-9630-1

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