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Topics in Catalysis
Erschienen in: Topics in Catalysis 18-19/2018

06.07.2018 | Original Paper

Cobalt-Catalyzed Green Cross-Dehydrogenative C(sp2)-H/P-H Coupling Reactions

verfasst von: Mikhail Khrizanforov, Sofia Strekalova, Vera Khrizanforova, Alexey Dobrynin, Kirill Kholin, Tatyana Gryaznova, Valeriya Grinenko, Aidar Gubaidullin, M. K. Kadirov, Yulia Budnikova

Erschienen in: Topics in Catalysis | Ausgabe 18-19/2018

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Abstract

Joined electrolysis of arenes (benzene or coumarin derivatives) and diethyl-H-phosphonate (EtO)2P(O)H in the presence of [CoCl2(bpy)] catalyst (5%) in an ethanol-aqueous solution in reductive conditions allows obtaining the desired products in a single step by aromatic C–H bonds phosphonation with yields up to 70%. The only by-product is hydrogen; the reaction proceeds at room temperature and does not require specially added reducing agents and oxidants or other initiators. Radical mechanism has been confirmed for the catalytic reaction proceeding via bicobalt phosphonates with Co–P bond, the structure of which also has been identified.
Vorheriger Artikel A Rational Revisiting of Niobium Oxophosphate Catalysts for Carbohydrate Biomass Reactions
Nächster Artikel Metal-Free Catalytic Wet Oxidation: From Powder to Structured Catalyst Using N-Doped Carbon Nanotubes

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Metadaten
Titel
Cobalt-Catalyzed Green Cross-Dehydrogenative C(sp2)-H/P-H Coupling Reactions
verfasst von
Mikhail Khrizanforov
Sofia Strekalova
Vera Khrizanforova
Alexey Dobrynin
Kirill Kholin
Tatyana Gryaznova
Valeriya Grinenko
Aidar Gubaidullin
M. K. Kadirov
Yulia Budnikova
Publikationsdatum
06.07.2018
Verlag
Springer US
Erschienen in
Topics in Catalysis / Ausgabe 18-19/2018
Print ISSN: 1022-5528
Elektronische ISSN: 1572-9028
DOI
https://doi.org/10.1007/s11244-018-1014-2

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