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Colloid and Polymer Science
Erschienen in: Colloid and Polymer Science 12/2013

01.12.2013 | Original Contribution

Crystallization of calcium carbonate controlled by Pluronic P123 in room-temperature ionic liquid

verfasst von: Yingyuan Zhao, Ni Cheng, Min Liu, Li Yu

Erschienen in: Colloid and Polymer Science | Ausgabe 12/2013

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Abstract

The crystallization of calcium carbonate (CaCO3) controlled by Pluronic P123 in a room-temperature ionic liquid, ethylamine nitrate (EAN), was investigated. The CaCO3 aggregates were obtained by rapid mixing of ammonium carbonate ((NH4)2CO3) and calcium chloride (CaCl2). Cubic calcite, spherical vaterite, and bagel-like vaterite were obtained easily by changing P123 concentration and reaction temperature. The morphologies of the as-prepared CaCO3 aggregates were investigated by transmission electron microscopy and scanning electronic microscopy. The phase change of the obtained crystals was confirmed by X-ray diffraction and Fourier transform infrared spectroscopy. It was shown that higher P123 concentration and higher reaction temperature favor the formation of vaterite in EAN. Unusual bagel-like vaterite was first obtained at 60 °C in the presence of 5 g/L P123 in EAN. Mineralization of CaCO3 regulated by P123 in EAN is a simple, novel, and environment-friendly strategy for vaterite synthesis.
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Metadaten
Titel
Crystallization of calcium carbonate controlled by Pluronic P123 in room-temperature ionic liquid
verfasst von
Yingyuan Zhao
Ni Cheng
Min Liu
Li Yu
Publikationsdatum
01.12.2013
Verlag
Springer Berlin Heidelberg
Erschienen in
Colloid and Polymer Science / Ausgabe 12/2013
Print ISSN: 0303-402X
Elektronische ISSN: 1435-1536
DOI
https://doi.org/10.1007/s00396-013-3041-7

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