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Journal of Nanoparticle Research
Erschienen in: Journal of Nanoparticle Research 5/2020

01.05.2020 | Research paper

Electropolishing and anodization of titanium in water/ethylene glycol baths for the production of TiO2 nanotubes

verfasst von: Oliver Rodríguez-Martínez, Luz María Martínez, Marcelo Videa

Erschienen in: Journal of Nanoparticle Research | Ausgabe 5/2020

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Abstract

A greener methodology to grow TiO2 nanotubes in a non-corrosive, low-hazard, fluoride-free ethylene glycol/water electrolytic bath is presented. Results demonstrate that the formation of nanostructures by anodization of Ti foils in NaCl solutions requires glycol/water solutions with water contents (> 50%) and moderate voltages (< 30 V). Nanotube growth was dependent on the surface characteristics; anodization performed on mechanically polished surfaces showed that randomly oriented nanotubes grow on pits while vertically oriented TiO2 nanotubes were obtained on electropolished surfaces. An electropolishing methodology was developed to obtain surfaces with submicrometer roughness that favours the growth control of vertically oriented TiO2 nanotubes.
Vorheriger Artikel An intercomparison exercise of good laboratory practices for nano-aerosol size measurements by mobility spectrometers
Nächster Artikel Longevity of iron-activated persulfate oxidation for the remediation of 2,4-dinitrotoluene-contaminated groundwater

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Metadaten
Titel
Electropolishing and anodization of titanium in water/ethylene glycol baths for the production of TiO2 nanotubes
verfasst von
Oliver Rodríguez-Martínez
Luz María Martínez
Marcelo Videa
Publikationsdatum
01.05.2020
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 5/2020
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-020-04824-8

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