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Erschienen in: Microsystem Technologies 1/2016

11.02.2015 | Technical Paper

Evaluation of the bond quality of laser-joined sapphire wafers using a fresnoite-glass sealant

verfasst von: A. de Pablos-Martín, S. Tismer, F. Naumann, M. Krause, M. Lorenz, M. Grundmann, Th. Höche

Erschienen in: Microsystem Technologies | Ausgabe 1/2016

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Abstract

Two sapphire substrates were bonded using a fresnoite glass thin film as a sealant, by irradiation with a 1,064 nm ns laser. The sapphire close to the interface was examined by TEM, showing some structural defects due to the laser processing. Bond quality and strength were evaluated by scanning acoustic microscopy (SAM) and micro-chevron testing, respectively. Optimization of laser parameters lead to an improved processing speed (>1 mm/s) as well as an enhanced fracture toughness to 1.23 MPa m1/2.

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Literatur
Zurück zum Zitat Bechthold PS, Haussuhl S, Michael E, Eckstein J, Recker K, Wallrafen F (1978) 2nd Harmonic-Generation in Fresnoite, Ba2TiSi2O8. Phys Lett A 65(5–6):453–454CrossRef Bechthold PS, Haussuhl S, Michael E, Eckstein J, Recker K, Wallrafen F (1978) 2nd Harmonic-Generation in Fresnoite, Ba2TiSi2O8. Phys Lett A 65(5–6):453–454CrossRef
Zurück zum Zitat Ben-Yakar A, Harkin A, Ashmore J, Byer RL, Stone HA (2007) Thermal and fluid processes of a thin melt zone during femtosecond laser ablation of glass: the formation of rims by single laser pulses. J Phys D Appl Phys 40(5):1447–1459CrossRef Ben-Yakar A, Harkin A, Ashmore J, Byer RL, Stone HA (2007) Thermal and fluid processes of a thin melt zone during femtosecond laser ablation of glass: the formation of rims by single laser pulses. J Phys D Appl Phys 40(5):1447–1459CrossRef
Zurück zum Zitat Blasse G (1979) Fresnoite (Ba2TiSi2O8)—luminescent compound with a long decay time. J Inorg Nucl Chem 41(5):639–641CrossRef Blasse G (1979) Fresnoite (Ba2TiSi2O8)—luminescent compound with a long decay time. J Inorg Nucl Chem 41(5):639–641CrossRef
Zurück zum Zitat Carter RM, Chen J, Shephard JD, Thomson RR, Hand DP (2014) Picosecond laser welding of similar and dissimilar materials. Appl Opt 53(19):4233–4238CrossRef Carter RM, Chen J, Shephard JD, Thomson RR, Hand DP (2014) Picosecond laser welding of similar and dissimilar materials. Appl Opt 53(19):4233–4238CrossRef
Zurück zum Zitat Cvecek K, Alexeev I, Miyamoto I, Schmidt M (2010) Defect formation in glass welding by means of ultra short laser pulses. Phys Procedia 5:495–502CrossRef Cvecek K, Alexeev I, Miyamoto I, Schmidt M (2010) Defect formation in glass welding by means of ultra short laser pulses. Phys Procedia 5:495–502CrossRef
Zurück zum Zitat de Pablos-Martín A, Ebert M, Patzig C, Krause M, Dyrba M, Miclea P, Lorenz M, Grundmann M, Höche T (2014) Laser welding of sapphire wafers using a thin-film fresnoite glass solder. Microsyst Technol. doi:10.1007/s00542-00014-02398-y de Pablos-Martín A, Ebert M, Patzig C, Krause M, Dyrba M, Miclea P, Lorenz M, Grundmann M, Höche T (2014) Laser welding of sapphire wafers using a thin-film fresnoite glass solder. Microsyst Technol. doi:10.​1007/​s00542-00014-02398-y
Zurück zum Zitat Donald IW, Mallinson PM, Metcalfe BL, Gerrard LA, Fernie JA (2011) Recent developments in the preparation, characterization and applications of glass- and glass-ceramic-to-metal seals and coatings. J Mater Sci 46(7):1975–2000CrossRef Donald IW, Mallinson PM, Metcalfe BL, Gerrard LA, Fernie JA (2011) Recent developments in the preparation, characterization and applications of glass- and glass-ceramic-to-metal seals and coatings. J Mater Sci 46(7):1975–2000CrossRef
Zurück zum Zitat Dresbach C, Krombbolz A, Ebert M, Bagdahn J (2006) Mechanical properties of glass frit bonded micro packages. Microsyst Technol 12(5):473–480CrossRef Dresbach C, Krombbolz A, Ebert M, Bagdahn J (2006) Mechanical properties of glass frit bonded micro packages. Microsyst Technol 12(5):473–480CrossRef
Zurück zum Zitat Faidel D, Behr W, Groß S, Reisgen U (2010) Development of a laser-based glass sealing joining process for the fuel cell manufacturing. Phys Procedia 5:153–162CrossRef Faidel D, Behr W, Groß S, Reisgen U (2010) Development of a laser-based glass sealing joining process for the fuel cell manufacturing. Phys Procedia 5:153–162CrossRef
Zurück zum Zitat Frieser RG (1975) A Review of solder glasses. Electrocompon Sci Technol 2:163–199CrossRef Frieser RG (1975) A Review of solder glasses. Electrocompon Sci Technol 2:163–199CrossRef
Zurück zum Zitat Gamaly EG, Juodkazis S, Nishimura K, Misawa H, Luther-Davies B (2006) Laser-matter interaction in the bulk of a transparent solid: confined microexplosion and void formation. Phys Rev B 73(21):214101CrossRef Gamaly EG, Juodkazis S, Nishimura K, Misawa H, Luther-Davies B (2006) Laser-matter interaction in the bulk of a transparent solid: confined microexplosion and void formation. Phys Rev B 73(21):214101CrossRef
Zurück zum Zitat Georgiev DG, Sultana T, Mian A, Auner G, Herfurth H, Witte R, Newaz G (2005) Laser fabrication and characterization of sub-millimeter joints between polyimide and Ti-coated borosilicate glass. J Mater Sci 40(21):5641–5647CrossRef Georgiev DG, Sultana T, Mian A, Auner G, Herfurth H, Witte R, Newaz G (2005) Laser fabrication and characterization of sub-millimeter joints between polyimide and Ti-coated borosilicate glass. J Mater Sci 40(21):5641–5647CrossRef
Zurück zum Zitat Greenaway MW, Proud WG, Field JE, Goveas SG (2002) The development and study of a fiber delivery system for beam shaping. Rev Sci Instrum 73(5):2185–2189CrossRef Greenaway MW, Proud WG, Field JE, Goveas SG (2002) The development and study of a fiber delivery system for beam shaping. Rev Sci Instrum 73(5):2185–2189CrossRef
Zurück zum Zitat Iwasa M, Ueno T, Bradt C (1981) Fracture toughness of quartz and sapphire single crystals at room temperature. Zairyo 30(337):1001–1004 Iwasa M, Ueno T, Bradt C (1981) Fracture toughness of quartz and sapphire single crystals at room temperature. Zairyo 30(337):1001–1004
Zurück zum Zitat Kim T, Kim Y, Jeong Y, Na Y, Lim H, Cha MS, Ryu BK (2008) Optical properties and structure of BaO–TiO2–SiO2 glass ceramics. J Korean Ceram Soc 45(12):821–826CrossRef Kim T, Kim Y, Jeong Y, Na Y, Lim H, Cha MS, Ryu BK (2008) Optical properties and structure of BaO–TiO2–SiO2 glass ceramics. J Korean Ceram Soc 45(12):821–826CrossRef
Zurück zum Zitat Knechtel R (2005) Glass frit bonding: an universal technology for wafer level encapsulation and packaging. Microsyst Technol 12(1–2):63–68CrossRef Knechtel R (2005) Glass frit bonding: an universal technology for wafer level encapsulation and packaging. Microsyst Technol 12(1–2):63–68CrossRef
Zurück zum Zitat Liu P, Wang J, Tong L, Tao Y (2014) Advances in the fabrication processes and applications of wafer level packaging. J Electron Packag 136(2):024002CrossRef Liu P, Wang J, Tong L, Tao Y (2014) Advances in the fabrication processes and applications of wafer level packaging. J Electron Packag 136(2):024002CrossRef
Zurück zum Zitat Lorenz M, Rao R (eds) (2014) 25 years of pulsed laser deposition. J Phys D: Appl Phys 47:030301 Lorenz M, Rao R (eds) (2014) 25 years of pulsed laser deposition. J Phys D: Appl Phys 47:030301
Zurück zum Zitat Müller A, Lorenz M, Brachwitz K, Lenzner J, Mittwoch K, Skorupa W, Grundmann M, Höche T (2011) Fresnoite thin films grown by pulsed laser deposition: photoluminescence and laser crystallization. Cryst Eng Comm 13(21):6377–6385CrossRef Müller A, Lorenz M, Brachwitz K, Lenzner J, Mittwoch K, Skorupa W, Grundmann M, Höche T (2011) Fresnoite thin films grown by pulsed laser deposition: photoluminescence and laser crystallization. Cryst Eng Comm 13(21):6377–6385CrossRef
Zurück zum Zitat Naumann F, Brand S, Bernasch M, Tismer S, Czurratis P, Wünsch D, Petzold M (2013) Advanced characterization of glass frit bonded micro-chevron-test samples based on scanning acoustic microscopy. Microsyst Technol 19(5):689–695CrossRef Naumann F, Brand S, Bernasch M, Tismer S, Czurratis P, Wünsch D, Petzold M (2013) Advanced characterization of glass frit bonded micro-chevron-test samples based on scanning acoustic microscopy. Microsyst Technol 19(5):689–695CrossRef
Zurück zum Zitat Ohmura E, Kawahito Y, Fukumitsu K, Okuma J, Morita H (2010) Analysis of internal crack propagation in silicon due to permeable pulse laser irradiation: study on processing mechanism of stealth dicing, pp 799603–799608 Ohmura E, Kawahito Y, Fukumitsu K, Okuma J, Morita H (2010) Analysis of internal crack propagation in silicon due to permeable pulse laser irradiation: study on processing mechanism of stealth dicing, pp 799603–799608
Zurück zum Zitat Petzold M, Katzer D, Wiemer M, Bagdahn J (2002) Strength and long-term reliability testing of wafer-bonded MEMS. Proc SPIE Int Soc Opt Eng 4755:613–623 Petzold M, Katzer D, Wiemer M, Bagdahn J (2002) Strength and long-term reliability testing of wafer-bonded MEMS. Proc SPIE Int Soc Opt Eng 4755:613–623
Zurück zum Zitat Shen C, Zhang H, Cong H, Yu H, Wang J, Zhang S (2014) Investigations on the thermal and piezoelectric properties of fresnoite Ba2TiSi2O8 single crystals. J Appl Phys 116(4):044106CrossRef Shen C, Zhang H, Cong H, Yu H, Wang J, Zhang S (2014) Investigations on the thermal and piezoelectric properties of fresnoite Ba2TiSi2O8 single crystals. J Appl Phys 116(4):044106CrossRef
Zurück zum Zitat Strecker A, Salzberger U, Mayer J (1993) Specimen preparation for transmission electron microscopy: reliable method for cross-sections and brittle materials. Prak Metallogr Pract Metallogr 30(10):482–495 Strecker A, Salzberger U, Mayer J (1993) Specimen preparation for transmission electron microscopy: reliable method for cross-sections and brittle materials. Prak Metallogr Pract Metallogr 30(10):482–495
Zurück zum Zitat Takahashi Y, Kitamura K, Benino Y, Fujiwara T, Komatsu T (2005) Second-order optical nonlinear and luminescent properties of Ba2TiSi2O8 nanocrystallized glass. Appl Phys Lett 86(9):091110–091113CrossRef Takahashi Y, Kitamura K, Benino Y, Fujiwara T, Komatsu T (2005) Second-order optical nonlinear and luminescent properties of Ba2TiSi2O8 nanocrystallized glass. Appl Phys Lett 86(9):091110–091113CrossRef
Zurück zum Zitat Takahashi Y, Iwasaki K, Fujiwara T (2012) Photoluminescence in mineral-derived titanosilicates with various Ti-polyhedral types for rare-earth free phosphor. Phys Status Solidi C Curr Top Solid State Phys 9(12):2336–2339 Takahashi Y, Iwasaki K, Fujiwara T (2012) Photoluminescence in mineral-derived titanosilicates with various Ti-polyhedral types for rare-earth free phosphor. Phys Status Solidi C Curr Top Solid State Phys 9(12):2336–2339
Zurück zum Zitat Wissinger A, Olowinsky A, Gillner A, Poprawe R (2013a) Laser transmission bonding of silicon to silicon with metallic interlayers for wafer-level packaging. Microsyst Technol 19(5):669–673CrossRef Wissinger A, Olowinsky A, Gillner A, Poprawe R (2013a) Laser transmission bonding of silicon to silicon with metallic interlayers for wafer-level packaging. Microsyst Technol 19(5):669–673CrossRef
Zurück zum Zitat Wissinger A, Schmitz M, Olowinsky A, Gillner A, Poprawe R (2013b) Laser transmission bonding of silicon with titanium and copper layer for wafer-level packaging. ECS Trans 50(7):189–198CrossRef Wissinger A, Schmitz M, Olowinsky A, Gillner A, Poprawe R (2013b) Laser transmission bonding of silicon with titanium and copper layer for wafer-level packaging. ECS Trans 50(7):189–198CrossRef
Zurück zum Zitat Zhang JP, Lee BI, Schwartz RW, Ding ZY (1999) Grain oriented crystallization, piezoelectric, and pyroelectric properties of (BaxSr2-x)TiSi2O8 glass ceramics. J Appl Phys 85(12):8343–8348CrossRef Zhang JP, Lee BI, Schwartz RW, Ding ZY (1999) Grain oriented crystallization, piezoelectric, and pyroelectric properties of (BaxSr2-x)TiSi2O8 glass ceramics. J Appl Phys 85(12):8343–8348CrossRef
Zurück zum Zitat Zheng Q, Smedskjaer MM, Youngman RE, Potuzak M, Mauro JC, Yue Y (2012) Influence of aluminum speciation on the stability of aluminosilicate glasses against crystallization. Appl Phys Lett 101(4):041906CrossRef Zheng Q, Smedskjaer MM, Youngman RE, Potuzak M, Mauro JC, Yue Y (2012) Influence of aluminum speciation on the stability of aluminosilicate glasses against crystallization. Appl Phys Lett 101(4):041906CrossRef
Zurück zum Zitat Zhu MK, Yang YH, Li XH, Wang B, Wang H, Yan H (2003) Preparation of Ba2Si2TiO8 thin films by magnetron sputtering. Microelectron Eng 66(1–4):745–749CrossRef Zhu MK, Yang YH, Li XH, Wang B, Wang H, Yan H (2003) Preparation of Ba2Si2TiO8 thin films by magnetron sputtering. Microelectron Eng 66(1–4):745–749CrossRef
Metadaten
Titel
Evaluation of the bond quality of laser-joined sapphire wafers using a fresnoite-glass sealant
verfasst von
A. de Pablos-Martín
S. Tismer
F. Naumann
M. Krause
M. Lorenz
M. Grundmann
Th. Höche
Publikationsdatum
11.02.2015
Verlag
Springer Berlin Heidelberg
Erschienen in
Microsystem Technologies / Ausgabe 1/2016
Print ISSN: 0946-7076
Elektronische ISSN: 1432-1858
DOI
https://doi.org/10.1007/s00542-015-2459-x

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