Skip to main content
Erschienen in: Experimental Mechanics 5/2023

09.05.2023 | Research paper

High-Throughput High-Resolution Digital Image Correlation Measurements by Multi-Beam SEM Imaging

verfasst von: R. L. Black, T. Garbowski, C. Bean, A. L. Eberle, S. Nickell, D. Texier, V. Valle, J. C. Stinville

Erschienen in: Experimental Mechanics | Ausgabe 5/2023

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

Background

Recent improvements in spatial resolution and measurement sensitivity for high-resolution digital image correlation (HR-DIC) now provide an avenue for the quantitative measurement of deformation events and capturing the physical nature of deformation mechanisms. However, HR-DIC measurements require significant time due to scanning electron image acquisition; such a limitation prevents the widespread use of HR-DIC for material characterization.

Objective

Apply a novel SEM acquisition technology to enhance HR-DIC measurements for high throughput applications.

Methods

Multi-beam SEM technology is employed to image an entire gauge length at once at high resolution and at nearly a hundredfold acceleration of typical HR-DIC image acquisition, even when automated stage movement and image acquisition are employed. These images were fed into a discontinuity-tolerant HR-DIC software to determine slip localization induced by non-metallic inclusions and grain structure.

Results

Slip localization was able to be analyzed to an unprecedented level, with over 210,000 slip bands able to be investigated, with the most intense slip localizing near and parallel to twin boundaries and in the vicinity of non-metallic inclusion clusters. Additionally, secondary slip activation and grain boundary shearing by intense dislocation pileups are observed to reduce slip amplitude near and parallel to twin boundaries.

Conclusions

By performing HR-DIC in conjunction with a multi-beam SEM, high-throughput measurements of large field-of-view, high-resolution images were able to be performed in a timely manner. These measurements provided an immense number of slip events for statistical analysis to be performed on to relate to microstructural features.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Anhänge
Nur mit Berechtigung zugänglich
Literatur
1.
2.
6.
Zurück zum Zitat Stinville JC, Charpagne MC, Cervellon A, Hemery S, Wang F, Callahan PG, Valle V, Pollock TM (2022) On the origins of fatigue strength in crystalline metallic materials. Science 377(6610):1065–1071MathSciNetCrossRef Stinville JC, Charpagne MC, Cervellon A, Hemery S, Wang F, Callahan PG, Valle V, Pollock TM (2022) On the origins of fatigue strength in crystalline metallic materials. Science 377(6610):1065–1071MathSciNetCrossRef
14.
Zurück zum Zitat Stinville JC, Francis T, Polonsky AT, Torbet CJ, Charpagne MA, Chen Z, Balbus GH, Bourdin F, Valle V, Callahan PG, Echlin MP, Pollock TM (2021) Time-resolved digital image correlation in the scanning electron microscope for analysis of time-dependent mechanisms. Exp Mech 61(2):331–348. https://doi.org/10.1007/s11340-020-00632-2. (ISSN 17412765)CrossRef Stinville JC, Francis T, Polonsky AT, Torbet CJ, Charpagne MA, Chen Z, Balbus GH, Bourdin F, Valle V, Callahan PG, Echlin MP, Pollock TM (2021) Time-resolved digital image correlation in the scanning electron microscope for analysis of time-dependent mechanisms. Exp Mech 61(2):331–348. https://​doi.​org/​10.​1007/​s11340-020-00632-2. (ISSN 17412765)CrossRef
24.
Zurück zum Zitat Rotella J, Mello AW, Venkataraman A, Buckingham R, Hardy M, Sangid MD (2021) Dwellfatigue of ni-based superalloys with serrated and planar grain boundary morphologies: yhe role of the γ phase on strain accumulation and cavitation. Metall Mater Trans A 52(11):5079–5095. https://doi.org/10.1007/s11661-021-06454-8. (ISSN 1543–1940)CrossRef Rotella J, Mello AW, Venkataraman A, Buckingham R, Hardy M, Sangid MD (2021) Dwellfatigue of ni-based superalloys with serrated and planar grain boundary morphologies: yhe role of the γ phase on strain accumulation and cavitation. Metall Mater Trans A 52(11):5079–5095. https://​doi.​org/​10.​1007/​s11661-021-06454-8. (ISSN 1543–1940)CrossRef
29.
36.
Zurück zum Zitat Texier D, Stinville JC, Charpagne MA, Chen Z, Valle V, Villechaise P, Pollock TM, Cormier J (2020) Role of non-metallic inclusions and twins on the variability in fatigue life in alloy 718 nickel base superalloy. In: Tin S, Hardy M, Clews J, Cormier J, Feng Q, Marcin J, O’Brien C, Suzuki A (eds) Superalloys. Springer International Publishing, Cham, pp 629–639 (ISBN 978–3–030–51834–9) Texier D, Stinville JC, Charpagne MA, Chen Z, Valle V, Villechaise P, Pollock TM, Cormier J (2020) Role of non-metallic inclusions and twins on the variability in fatigue life in alloy 718 nickel base superalloy. In: Tin S, Hardy M, Clews J, Cormier J, Feng Q, Marcin J, O’Brien C, Suzuki A (eds) Superalloys. Springer International Publishing, Cham, pp 629–639 (ISBN 978–3–030–51834–9)
38.
Zurück zum Zitat Hull D, Bacon DJ (2011) Introduction to dislocations. Materials science and technology. Elsevier Science (ISBN 9780080966731) Hull D, Bacon DJ (2011) Introduction to dislocations. Materials science and technology. Elsevier Science (ISBN 9780080966731)
41.
Zurück zum Zitat Stinville JC, Martin E, Karadge M, Ismonov S, Soare M, Hanlon T, Sundaram S, Echlin MP, Callahan PG, Lenthe WC, Miller VM, Miao J, Wessman AE, Finlay R, Loghin A, Marte J, Pollock TM (2018) Fatigue deformation in a polycrystalline nickel base superalloy at intermediate and high temperature: competing failure modes. Acta Mater 152:16–33. https://doi.org/10.1016/j.actamat.2018.03.035. (ISSN 1359–6454)CrossRef Stinville JC, Martin E, Karadge M, Ismonov S, Soare M, Hanlon T, Sundaram S, Echlin MP, Callahan PG, Lenthe WC, Miller VM, Miao J, Wessman AE, Finlay R, Loghin A, Marte J, Pollock TM (2018) Fatigue deformation in a polycrystalline nickel base superalloy at intermediate and high temperature: competing failure modes. Acta Mater 152:16–33. https://​doi.​org/​10.​1016/​j.​actamat.​2018.​03.​035. (ISSN 1359–6454)CrossRef
48.
Zurück zum Zitat Villechaise P, Cormier J, Billot T, Mendez J (2012) Mechanical behaviour and damage processes of Udimet 720Li: influence of localized plasticity at grain boundaries. 12th International Symposium on Superalloys, pp 15–24 Villechaise P, Cormier J, Billot T, Mendez J (2012) Mechanical behaviour and damage processes of Udimet 720Li: influence of localized plasticity at grain boundaries. 12th International Symposium on Superalloys, pp 15–24
Metadaten
Titel
High-Throughput High-Resolution Digital Image Correlation Measurements by Multi-Beam SEM Imaging
verfasst von
R. L. Black
T. Garbowski
C. Bean
A. L. Eberle
S. Nickell
D. Texier
V. Valle
J. C. Stinville
Publikationsdatum
09.05.2023
Verlag
Springer US
Erschienen in
Experimental Mechanics / Ausgabe 5/2023
Print ISSN: 0014-4851
Elektronische ISSN: 1741-2765
DOI
https://doi.org/10.1007/s11340-023-00961-y

Weitere Artikel der Ausgabe 5/2023

Experimental Mechanics 5/2023 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.