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Journal of Materials Science
Erschienen in: Journal of Materials Science 13/2014

01.07.2014

Increase of Fe solubility in ZnO induced by the grain boundary adsorption

verfasst von: S. G. Protasova, B. B. Straumal, A. A. Mazilkin, S. V. Stakhanova, P. B. Straumal, B. Baretzky

Erschienen in: Journal of Materials Science | Ausgabe 13/2014

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Abstract

Nanograined (grain size 6–15 nm) ZnO films with various Fe content (between 0 and 40 at.%) were synthesized by the novel liquid ceramics method. The films with 0, 0.1, 5 and 10 at.% Fe contain only ZnO-based solid solution with wurtzite structure. The films with 20 at.% Fe contain mainly amorphous phase. The peaks of the second phase (ZnFe2O4 with cubic lattice) become visible in the X-ray diffraction spectra at 30 at.% Fe. Therefore, the overall solubility of Fe in nanograined ZnO films at 550 °C is about 20 at.% Fe. The solubility limit in the bulk is about 1.5 at.% Fe. The recently published papers on the structure and magnetic behaviour of Fe-doped ZnO allowed us to obtain the dependence of Fe solubility in ZnO on the grain size. The overall Fe solubility drastically increases with the decreasing grain size. The quantitative estimation shows that, close to the bulk solubility limit, the thickness of a Fe-enriched layer in grain boundaries is that of several monolayers.
Vorheriger Artikel Material surface engineering for multiplex cell culture in microwell
Nächster Artikel Structural phase and morphology control of tetragonal and hexagonal YPO4:Eu nanoflakes for tunable luminescence properties

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Metadaten
Titel
Increase of Fe solubility in ZnO induced by the grain boundary adsorption
verfasst von
S. G. Protasova
B. B. Straumal
A. A. Mazilkin
S. V. Stakhanova
P. B. Straumal
B. Baretzky
Publikationsdatum
01.07.2014
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 13/2014
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-014-8146-y

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