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Metallurgical and Materials Transactions B
Erschienen in: Metallurgical and Materials Transactions B 1/2018

22.11.2017

Experimental Liquidus Studies of the Pb-Fe-Si-O System in Equilibrium with Metallic Pb

verfasst von: M. Shevchenko, E. Jak

Erschienen in: Metallurgical and Materials Transactions B | Ausgabe 1/2018

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Abstract

Phase equilibria of the Pb-Fe-Si-O system have been investigated at 943 K to 1773 K (670 °C to 1500 °C) for oxide liquid in equilibrium with liquid Pb metal and solid oxide phases: (a) quartz, tridymite, or cristobalite; (b) (fayalite + tridymite) or (fayalite + spinel); (c) spinel (Fe3O4); (d) complex lead-iron silicates (melanotekite PbO·FeO1.5·SiO2, barysilite 8PbO·FeO·6SiO2, 5PbO·FeO1.5·SiO2, and 6PbO·FeO1.5·SiO2); (e) lead silicates (Pb2SiO4, Pb11Si3O17); (f) lead ferrites (magnetoplumbite Pb1+x Fe12−x O19−x solid solution range); and (g) lead oxide (PbO, massicot). High-temperature equilibration on primary phase or iridium substrates, followed by quenching and direct measurement of Pb, Fe, and Si concentrations in the phases with the electron probe X-ray microanalysis, has been used to accurately characterize the system in equilibrium with Pb metal. All results are projected onto the PbO-“FeO”-SiO2 plane for presentation purposes. The present study is the first systematic characterization of liquidus over a wide range of compositions in this system in equilibrium with metallic Pb.
Vorheriger Artikel Effect of Si Content on Oxide Formation on Surface of Molten Fe-Cr-C Alloy Bath During Oxygen Top Blowing
Nächster Artikel Distribution of P2O5 and Na2O Between Solid Solution and Liquid Phase in the CaO-SiO2-Fe2O3-P2O5-Na2O Slag System with High P2O5 Content

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Metadaten
Titel
Experimental Liquidus Studies of the Pb-Fe-Si-O System in Equilibrium with Metallic Pb
verfasst von
M. Shevchenko
E. Jak
Publikationsdatum
22.11.2017
Verlag
Springer US
Erschienen in
Metallurgical and Materials Transactions B / Ausgabe 1/2018
Print ISSN: 1073-5615
Elektronische ISSN: 1543-1916
DOI
https://doi.org/10.1007/s11663-017-1136-0

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