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Erschienen in: Rare Metals 3/2022

16.05.2015

Characterization of ZrO2 ceramic coatings on ZrH1.8 prepared in different electrolytes by micro-arc oxidation

verfasst von: Zhi-Gang Wang, Wei-Dong Chen, Shu-Fang Yan, Xiu-Juan Fan, Zhi-Gao Xu

Erschienen in: Rare Metals | Ausgabe 3/2022

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Abstract

ZrO2 ceramic coatings were directly prepared on the surface of ZrH1.8 in silicate and phosphate electrolytes by micro-arc oxidation (MAO) technique, respectively. The microstructure, chemical composition and phase composition of ZrO2 ceramic coatings were investigated by X-ray diffraction (XRD), energy-dispersive spectrometry (EDS) and scanning electron microscopy (SEM). The anti-permeation effect was measured by means of vacuum dehydrogenation experiment. It is found that the coating fabricated in phosphate electrolyte is more compact than that in silicate electrolyte. The coatings fabricated on the surface of ZrH1.8 are composed of M-ZrO2, T-ZrO2 and C-ZrO2. EDS analysis indicates that the coatings are mainly composed of O and Zr. Vacuum dehydrogenation experiment shows that the permeation reduction factor (PRF) of coating prepared in phosphate electrolyte is superior to that in the silicate electrolyte, and the PRF value reaches up to 11.2, which can enhance the resistance effect of hydrogen significantly.

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Metadaten
Titel
Characterization of ZrO2 ceramic coatings on ZrH1.8 prepared in different electrolytes by micro-arc oxidation
verfasst von
Zhi-Gang Wang
Wei-Dong Chen
Shu-Fang Yan
Xiu-Juan Fan
Zhi-Gao Xu
Publikationsdatum
16.05.2015
Verlag
Nonferrous Metals Society of China
Erschienen in
Rare Metals / Ausgabe 3/2022
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-015-0503-8

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