Skip to main content
Erschienen in: Rare Metals 10/2017

27.09.2017

Phase fraction evolution in hot working of a two-phase titanium alloy: experiment and modeling

verfasst von: Xiao-Guang Fan, Huo-Jun Zheng, Peng-Fei Gao, Mei Zhan, Wen-Jia Mei

Erschienen in: Rare Metals | Ausgabe 10/2017

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

In the present work, the coupled effects of initial structure and processing parameters on microstructure of a two-phase titanium alloy were investigated to predict the microstructural evolution in multiple hot working. It is found that microstructure with different constituent phases can be obtained by regulating the initial structure and hot working conditions. The variation of deformation degree and cooling rate can change the morphology of the constituent phases, but do not alter the phase fraction. The phase transformation during heating and holding determines the phase fraction for a certain initial structure. β–α–β transformation occurs during heating and holding. β to α transformation leads to a significant increase in content and size of lamellar α. The α to β transformation occurs simultaneously in equiaxed α and lamellar α. The thickness of lamellar α increases with temperature, which is caused by the vanishing of fine α lamellae due to phase transformation and coarsening by termination migration. By assuming a quasi-equilibrium phase transformation in heating and holding, a modeling approach is proposed for predicting microstructural evolution. The three stages of phase transformation are modeled separately and combined to predict the variation of phase fraction with temperature. Model predictions agree well with the experimental results.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
[1]
Zurück zum Zitat Lütjering G, Williams JC. Titanium. 2nd ed. Berlin: Springer; 2007. 1. Lütjering G, Williams JC. Titanium. 2nd ed. Berlin: Springer; 2007. 1.
[2]
Zurück zum Zitat Banerjee D, Williams JC. Perspectives on titanium science and technology. Acta Mater. 2013;61(3):844.CrossRef Banerjee D, Williams JC. Perspectives on titanium science and technology. Acta Mater. 2013;61(3):844.CrossRef
[3]
Zurück zum Zitat Guo LG, Zhu S, Yang H, Fan XG, Chen FL. Quantitative analysis of microstructure evolution induced by temperature rise during(α + β) deformation of TA15 titanium alloy. Rare Met. 2016;35(3):223.CrossRef Guo LG, Zhu S, Yang H, Fan XG, Chen FL. Quantitative analysis of microstructure evolution induced by temperature rise during(α + β) deformation of TA15 titanium alloy. Rare Met. 2016;35(3):223.CrossRef
[4]
Zurück zum Zitat Fan XG, Yang H, Gao PF, Zuo R, Lei PH. The role of dynamic and post dynamic recrystallization on microstructure refinement in primary working of a coarse grained two-phase titanium alloy. J Mater Process Technol. 2016;234:290.CrossRef Fan XG, Yang H, Gao PF, Zuo R, Lei PH. The role of dynamic and post dynamic recrystallization on microstructure refinement in primary working of a coarse grained two-phase titanium alloy. J Mater Process Technol. 2016;234:290.CrossRef
[5]
Zurück zum Zitat Bieler TR, Semiatin SL. The origins of heterogeneous deformation during primary hot working of Ti-6Al-4V. Int J Plast. 2002;18(9):1165.CrossRef Bieler TR, Semiatin SL. The origins of heterogeneous deformation during primary hot working of Ti-6Al-4V. Int J Plast. 2002;18(9):1165.CrossRef
[6]
Zurück zum Zitat Gao J, Li MQ, Li XD, Zhang D, Xue JR, Jiang XQ, Zhang CY, Liu LY. Quantitative analysis on microstructure evolution of Ti-6Al-2Zr-2Sn-2Mo-1.5Cr-2Nb alloy during isothermal compression. Rare Met. 2015;34(9):625.CrossRef Gao J, Li MQ, Li XD, Zhang D, Xue JR, Jiang XQ, Zhang CY, Liu LY. Quantitative analysis on microstructure evolution of Ti-6Al-2Zr-2Sn-2Mo-1.5Cr-2Nb alloy during isothermal compression. Rare Met. 2015;34(9):625.CrossRef
[7]
Zurück zum Zitat Meng M, Yang H, Fan XG, Yan SL, Zhao AM, Zhu S. On the modeling of diffusion-controlled growth of primary α in heat treatment of two-phase Ti-alloys. J Alloy Compd. 2017;691:67.CrossRef Meng M, Yang H, Fan XG, Yan SL, Zhao AM, Zhu S. On the modeling of diffusion-controlled growth of primary α in heat treatment of two-phase Ti-alloys. J Alloy Compd. 2017;691:67.CrossRef
[8]
Zurück zum Zitat Jia BH, Song WD, Tang HP, Wang ZH, Mao XN, Ning JG. Hot deformation behavior and constitutive model of TC18 alloy during compression. Rare Met. 2014;33(4):383.CrossRef Jia BH, Song WD, Tang HP, Wang ZH, Mao XN, Ning JG. Hot deformation behavior and constitutive model of TC18 alloy during compression. Rare Met. 2014;33(4):383.CrossRef
[9]
Zurück zum Zitat Zhu YC, Zeng WD, Feng F, Sun Y, Han YF, Zhou YG. Characterization of hot deformation behavior of as-cast TC21 titanium alloy using processing map. Mater Sci Eng A. 2013;528(3):1757.CrossRef Zhu YC, Zeng WD, Feng F, Sun Y, Han YF, Zhou YG. Characterization of hot deformation behavior of as-cast TC21 titanium alloy using processing map. Mater Sci Eng A. 2013;528(3):1757.CrossRef
[10]
Zurück zum Zitat Gao PF, Fan XG, Yang H. Role of processing parameters in the development of tri-modal microstructure during isothermal local loading forming of TA15 titanium alloy. J Mater Process Technol. 2017;239:160.CrossRef Gao PF, Fan XG, Yang H. Role of processing parameters in the development of tri-modal microstructure during isothermal local loading forming of TA15 titanium alloy. J Mater Process Technol. 2017;239:160.CrossRef
[11]
Zurück zum Zitat Wang MP, Zhao YQ, Zeng WD. Phase transformation kinetics of Ti-1300 alloy during continuous heating. Rare Met. 2015;34(4):233.CrossRef Wang MP, Zhao YQ, Zeng WD. Phase transformation kinetics of Ti-1300 alloy during continuous heating. Rare Met. 2015;34(4):233.CrossRef
[12]
Zurück zum Zitat He D, Zhua JC, Zaefferer S, Raabe D, Liu Y, Lai ZL, Yang XW. Influences of deformation strain, strain rate and cooling rate on the Burgers orientation relationship and variants morphology during β → α phase transformation in a near α titanium alloy. Mater Sci Eng A. 2012;549:20.CrossRef He D, Zhua JC, Zaefferer S, Raabe D, Liu Y, Lai ZL, Yang XW. Influences of deformation strain, strain rate and cooling rate on the Burgers orientation relationship and variants morphology during β → α phase transformation in a near α titanium alloy. Mater Sci Eng A. 2012;549:20.CrossRef
[13]
Zurück zum Zitat Sha W, Guo ZL. Phase evolution of Ti-6Al-4V during continuous heating. J Alloy Compd. 1999;290(1):L3.CrossRef Sha W, Guo ZL. Phase evolution of Ti-6Al-4V during continuous heating. J Alloy Compd. 1999;290(1):L3.CrossRef
[14]
Zurück zum Zitat Wang YH, Kou HC, Chang H, Zhu ZZ, Su XF, Li JS, Zhou L. Phase transformation in TC21 alloy during continuous heating. J Alloy Compd. 2009;472(1–2):252.CrossRef Wang YH, Kou HC, Chang H, Zhu ZZ, Su XF, Li JS, Zhou L. Phase transformation in TC21 alloy during continuous heating. J Alloy Compd. 2009;472(1–2):252.CrossRef
[15]
Zurück zum Zitat Zhu S, Yang H, Guo LG, Fan XG. Effect of cooling rate on microstructure evolution during α/β heat treatment of TA15 titanium alloy. Mater Charact. 2012;70:101.CrossRef Zhu S, Yang H, Guo LG, Fan XG. Effect of cooling rate on microstructure evolution during α/β heat treatment of TA15 titanium alloy. Mater Charact. 2012;70:101.CrossRef
[16]
Zurück zum Zitat Semiatin SL, Kirby BC, Salishchev GA. Coarsening behavior of an α–β titanium alloy. Metall Mater Trans A. 2004;35(9):2809.CrossRef Semiatin SL, Kirby BC, Salishchev GA. Coarsening behavior of an α–β titanium alloy. Metall Mater Trans A. 2004;35(9):2809.CrossRef
[17]
Zurück zum Zitat Semiatin SL, Corbett MW, Fagin PN, Salishchev GA, Lee CS. Dynamic-coarsening behavior of an α/β titanium alloy. Metall Mater Trans A. 2006;37(4):1125.CrossRef Semiatin SL, Corbett MW, Fagin PN, Salishchev GA, Lee CS. Dynamic-coarsening behavior of an α/β titanium alloy. Metall Mater Trans A. 2006;37(4):1125.CrossRef
[18]
Zurück zum Zitat Zong YY, Shan DB, Xu M, Lv Y. Flow softening and microstructural evolution of TC11 titanium alloy during hot deformation. J Mater Process Technol. 2009;209(4):1988.CrossRef Zong YY, Shan DB, Xu M, Lv Y. Flow softening and microstructural evolution of TC11 titanium alloy during hot deformation. J Mater Process Technol. 2009;209(4):1988.CrossRef
[19]
Zurück zum Zitat Ma X, Zeng WD, Tian F, Zhou YG. The kinetics of dynamic globularization during hot working of a two phase titanium alloy with starting lamellar microstructure. Mater Sci Eng A. 2012;548:6.CrossRef Ma X, Zeng WD, Tian F, Zhou YG. The kinetics of dynamic globularization during hot working of a two phase titanium alloy with starting lamellar microstructure. Mater Sci Eng A. 2012;548:6.CrossRef
[20]
Zurück zum Zitat Wang K, Li MQ. Effects of heat treatment and hot deformation on the secondary α phase evolution of TC8 titanium alloy. Mater Sci Eng A. 2014;613:209.CrossRef Wang K, Li MQ. Effects of heat treatment and hot deformation on the secondary α phase evolution of TC8 titanium alloy. Mater Sci Eng A. 2014;613:209.CrossRef
[21]
Zurück zum Zitat Semiatin SL, Lehner TM, Miller JD, Doherty RD, Furrer DU. Alpha/beta heat treatment of a titanium alloy with a nonuniform microstructure. Metall Mater Trans A. 2007;38(4):910.CrossRef Semiatin SL, Lehner TM, Miller JD, Doherty RD, Furrer DU. Alpha/beta heat treatment of a titanium alloy with a nonuniform microstructure. Metall Mater Trans A. 2007;38(4):910.CrossRef
[22]
Zurück zum Zitat Carslaw HS, Jaeger JC. Conduction of Heat in Solids. London: Oxford University Press; 1959. 28. Carslaw HS, Jaeger JC. Conduction of Heat in Solids. London: Oxford University Press; 1959. 28.
[23]
Zurück zum Zitat Aaron HB, Fainstein D, Kotler GR. Diffusion-limited phase transformations: a comparison and critical evaluation of the mathematical approximations. J Appl Phys. 1970;41(11):4404.CrossRef Aaron HB, Fainstein D, Kotler GR. Diffusion-limited phase transformations: a comparison and critical evaluation of the mathematical approximations. J Appl Phys. 1970;41(11):4404.CrossRef
[24]
Zurück zum Zitat Sha W, Malinov S. Titanium Alloys: Modeling of Microstructure, Properties and Applications. Cambridge: Woodhead; 2009. 117.CrossRef Sha W, Malinov S. Titanium Alloys: Modeling of Microstructure, Properties and Applications. Cambridge: Woodhead; 2009. 117.CrossRef
[25]
Zurück zum Zitat Gao XX, Zeng WD, Zhang SF, Wang QJ. A study of epitaxial growth behaviors of equiaxed α phase at different cooling rates in near alpha titanium alloy. Acta Mater. 2017;122:298.CrossRef Gao XX, Zeng WD, Zhang SF, Wang QJ. A study of epitaxial growth behaviors of equiaxed α phase at different cooling rates in near alpha titanium alloy. Acta Mater. 2017;122:298.CrossRef
[26]
Zurück zum Zitat Fan XG, Yang H, Gao PF. Prediction of constitutive behavior and microstructure evolution in hot deformation of TA15 titanium alloy. Mater Des. 2013;51:34.CrossRef Fan XG, Yang H, Gao PF. Prediction of constitutive behavior and microstructure evolution in hot deformation of TA15 titanium alloy. Mater Des. 2013;51:34.CrossRef
[27]
Zurück zum Zitat Elmer JW, Palmer TA, Babu SS, Specht ED. In situ observations of lattice expansion and transformation rates of α and β phases in Ti–6Al–4V. Mater Sci Eng A. 2005;391(1–2):104.CrossRef Elmer JW, Palmer TA, Babu SS, Specht ED. In situ observations of lattice expansion and transformation rates of α and β phases in Ti–6Al–4V. Mater Sci Eng A. 2005;391(1–2):104.CrossRef
[28]
Zurück zum Zitat Barriobero-Vila P, Requena G, Buslaps T, Alfeld M, Boesenberg U. Role of element partitioning on the α–β phase transformation kinetics of a bi-modal Ti-6Al-6V-2Sn alloy during continuous heating. J Alloy Compd. 2015;626:330.CrossRef Barriobero-Vila P, Requena G, Buslaps T, Alfeld M, Boesenberg U. Role of element partitioning on the α–β phase transformation kinetics of a bi-modal Ti-6Al-6V-2Sn alloy during continuous heating. J Alloy Compd. 2015;626:330.CrossRef
[29]
Zurück zum Zitat Bein S, Bechet J. Comparative approach of phase transformations in titanium alloys Ti-6246, β-Cez and Ti-1023 using dilatometric analysis and electrical resistivity measurements. In: Titanium 95—Science and Technology. Proceedings of the 8th World Conference on Titanium. London: Institute of Materials. 1996. 2353. Bein S, Bechet J. Comparative approach of phase transformations in titanium alloys Ti-6246, β-Cez and Ti-1023 using dilatometric analysis and electrical resistivity measurements. In: Titanium 95—Science and Technology. Proceedings of the 8th World Conference on Titanium. London: Institute of Materials. 1996. 2353.
[30]
Zurück zum Zitat Sun ZC, Guo SS, Yang H. Nucleation and growth mechanism of α-lamellae of Ti alloy TA15 cooling from an α + β phase field. Acta Mater. 2013;61(6):2057.CrossRef Sun ZC, Guo SS, Yang H. Nucleation and growth mechanism of α-lamellae of Ti alloy TA15 cooling from an α + β phase field. Acta Mater. 2013;61(6):2057.CrossRef
[31]
Zurück zum Zitat Grong Ø, Shercliff HR. Microstructural modelling in metals processing. Prog Mater Sci. 2002;47(2):163.CrossRef Grong Ø, Shercliff HR. Microstructural modelling in metals processing. Prog Mater Sci. 2002;47(2):163.CrossRef
[32]
Zurück zum Zitat Pande CS, Rajagopal AK. Uniqueness and self similarity of size distributions in grain growth and coarsening. Acta Mater. 2001;49(10):1805.CrossRef Pande CS, Rajagopal AK. Uniqueness and self similarity of size distributions in grain growth and coarsening. Acta Mater. 2001;49(10):1805.CrossRef
[33]
Zurück zum Zitat Mei MJ, Yang H, Fan XG. Quantitative analysis of the microstructure under multi-pass thermal cycle of TA15 titanium alloy. J Plast Eng. 2014;21(4):79. Mei MJ, Yang H, Fan XG. Quantitative analysis of the microstructure under multi-pass thermal cycle of TA15 titanium alloy. J Plast Eng. 2014;21(4):79.
[34]
Zurück zum Zitat Fan XG, Gao PF, Yang H. Microstructure evolution of the transitional region in isothermal local loading of TA15 titanium alloy. Mater Sci Eng A. 2011;528(6):2694.CrossRef Fan XG, Gao PF, Yang H. Microstructure evolution of the transitional region in isothermal local loading of TA15 titanium alloy. Mater Sci Eng A. 2011;528(6):2694.CrossRef
Metadaten
Titel
Phase fraction evolution in hot working of a two-phase titanium alloy: experiment and modeling
verfasst von
Xiao-Guang Fan
Huo-Jun Zheng
Peng-Fei Gao
Mei Zhan
Wen-Jia Mei
Publikationsdatum
27.09.2017
Verlag
Nonferrous Metals Society of China
Erschienen in
Rare Metals / Ausgabe 10/2017
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-017-0950-5

Weitere Artikel der Ausgabe 10/2017

Rare Metals 10/2017 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.