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Rare Metals

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03.10.2019

A highly efficient pathway to recover gold from acid aqueous solution by using an amidoxime-functionalized UHMWPE fiber

verfasst von: Yu-Lin Liang, Chan Jin, Jiang-Tao Hu, Zhen Liu, Yan Li, Jian-Rong Zeng, Guo-Zhong Wu, Xiang-Jun Wei

Erschienen in: Rare Metals | Ausgabe 11/2019

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Abstract

A new amidoxime-functionalized ultrahigh molecular weight polyethylene fibrous adsorbent (UHMWPE-g-PAO) was used for the recovery of Au(III) from acid aqueous solution. The maximum experimental absorption capacity of UHMWPE-g-PAO fiber was found to be approximately 220.0 mg·g⁻¹. Au adsorption on UHMWPE-g-PAO was characterized by synchrotron radiation-based microcomputed tomography (SR-μ-CT), transmission electron microscopy (TEM), X-ray absorption near-edge structure spectroscopy (XANES) and synchrotron radiation-based Fourier transform infrared microspectroscopy (SR-FTIR). The SR-μ-CT and TEM results showed the distribution features of gold particles on the fiber. The mechanism of Au(III) recovery from aqueous solutions by UHMWPE-g-PAO was based on the adsorbed Au(III) ions, which were reduced to metallic zero-valent gold (Au(0)) by amino groups (–NH₂) in the amidoxime (AO) groups during the adsorption process, as confirmed by high-resolution TEM (HRTEM) and XANES analyses. X-ray diffraction (XRD) results indicated that the incineration ashes contained metallic zero-valent gold. In conclusion, this amidoxime-functionalized fibrous adsorbent is a promising material for recovering gold from aqueous solution.

Vorheriger Artikel Synthesis, characterization and optical studies on Sm2+-doped CdSe nanocrystals: a blueshift and fixed emission with high quantum yields

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Titel: A highly efficient pathway to recover gold from acid aqueous solution by using an amidoxime-functionalized UHMWPE fiber
verfasst von: Yu-Lin Liang
Chan Jin
Jiang-Tao Hu
Zhen Liu
Yan Li
Jian-Rong Zeng
Guo-Zhong Wu
Xiang-Jun Wei
Publikationsdatum: 03.10.2019
Verlag: Nonferrous Metals Society of China
Erschienen in: Rare Metals / Ausgabe 11/2019
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI: https://doi.org/10.1007/s12598-019-01317-z

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