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Erschienen in: Progress in Additive Manufacturing 1/2020

Open Access 27.02.2020 | Full Research Article

Properties of a superelastic NiTi shape memory alloy using laser powder bed fusion and adaptive scanning strategies

verfasst von: Tobias Gustmann, Florian Gutmann, Franziska Wenz, Peter Koch, Ralph Stelzer, Welf-Guntram Drossel, Hannes Korn

Erschienen in: Progress in Additive Manufacturing | Ausgabe 1/2020

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Abstract

A NiTi shape memory alloy with the nominal composition Ni50.9Ti49.1 (at%) was processed by laser beam melting/laser powder bed fusion and the process parameters as well as the type of scanning strategy (point-like exposure) were optimized in a first step to obtain delicate lattice structures (strut diameters below 200 µm). In the second step, the lattice structures were analyzed by means of optical and electron microscopy as well as computer tomography to obtain the interrelation between the process parameters, strut diameter and the uniformity of the corresponding struts. The processing, especially the laser power and the type of point-like exposure, has a strong influence on the resulting strut diameter and, therefore, on the haptic stiffness of lattice structures and the mechanical properties (deformability, superelasticity). Unlike other approaches, our findings imply that filigree NiTi lattices with high uniformity can be manufactured on a standard industry laser powder bed fusion machine without modifying its hard- or software configuration.

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Literatur
1.
Zurück zum Zitat Elahinia M (ed) (2016) Shape memory alloy actuators. Wiley, HobokenMATH Elahinia M (ed) (2016) Shape memory alloy actuators. Wiley, HobokenMATH
2.
Zurück zum Zitat Chowdhury P (2018) Frontiers of theoretical research on shape memory alloys: a general overview. Shap Mem Superelasticity 4:26–40CrossRef Chowdhury P (2018) Frontiers of theoretical research on shape memory alloys: a general overview. Shap Mem Superelasticity 4:26–40CrossRef
3.
Zurück zum Zitat Meier H, Haberland C, Frenzel J (2012) Structural and functional properties of NiTi shape memory alloys produced by selective laser melting, Adv Res Virtual Rapid Prototyping 291–296 Meier H, Haberland C, Frenzel J (2012) Structural and functional properties of NiTi shape memory alloys produced by selective laser melting, Adv Res Virtual Rapid Prototyping 291–296
4.
Zurück zum Zitat Turabi AS, Saedi S, Saghaian SM, Karaca HE, Elahinia M (2016) Experimental characterization of shape memory alloys. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 239–278 Turabi AS, Saedi S, Saghaian SM, Karaca HE, Elahinia M (2016) Experimental characterization of shape memory alloys. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 239–278
5.
Zurück zum Zitat van Humbeeck J, Chandrasekaran M, Delaey L (1991) Shape memory alloys: materials in action, Endeavour (Pergamon-Elsevier Science Ltd) 148–154 van Humbeeck J, Chandrasekaran M, Delaey L (1991) Shape memory alloys: materials in action, Endeavour (Pergamon-Elsevier Science Ltd) 148–154
6.
Zurück zum Zitat Otsuka K, Wayman CM (eds) (1998) Shape memory materials. Cambridge University Press, Cambridge Otsuka K, Wayman CM (eds) (1998) Shape memory materials. Cambridge University Press, Cambridge
7.
Zurück zum Zitat Dadbakhsh S, Speirs M, van Humbeeck J, Kruth J-P (2016) Laser additive manufacturing of bulk and porous shape-memory NiTi alloys: from processes to potential biomedical applications. MRS Bull 41:765–774CrossRef Dadbakhsh S, Speirs M, van Humbeeck J, Kruth J-P (2016) Laser additive manufacturing of bulk and porous shape-memory NiTi alloys: from processes to potential biomedical applications. MRS Bull 41:765–774CrossRef
8.
Zurück zum Zitat Haberland C, Kadkhodaei M, Elahinia M (2016) Introduction. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 1–44 Haberland C, Kadkhodaei M, Elahinia M (2016) Introduction. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 1–44
9.
Zurück zum Zitat Masseling L, Hargedorn Y.-C, Wissenbach K (2016) Fabrication of micro structures with NiTi shape memory alloy via µSLM. Proc Fraunhofer Direct Digit Manuf Conf DDMC2016 Masseling L, Hargedorn Y.-C, Wissenbach K (2016) Fabrication of micro structures with NiTi shape memory alloy via µSLM. Proc Fraunhofer Direct Digit Manuf Conf DDMC2016
10.
Zurück zum Zitat Otsuka K, Ren X (2005) Physical metallurgy of Ti–Ni-based shape memory alloys. Prog Mater Sci 50:511–678CrossRef Otsuka K, Ren X (2005) Physical metallurgy of Ti–Ni-based shape memory alloys. Prog Mater Sci 50:511–678CrossRef
11.
Zurück zum Zitat Jani JM, Leary M, Subic A, Gibson MA (2014) A review of shape memory alloy research, applications and opportunities. Mat Des 56:1078–1113CrossRef Jani JM, Leary M, Subic A, Gibson MA (2014) A review of shape memory alloy research, applications and opportunities. Mat Des 56:1078–1113CrossRef
12.
Zurück zum Zitat Saburi T (1998) Ti-Ni shape memory alloys. In: Otsuka K, Wayman CM (eds) Shape memory materials. Cambridge University Press, Cambridge, pp 49–96 Saburi T (1998) Ti-Ni shape memory alloys. In: Otsuka K, Wayman CM (eds) Shape memory materials. Cambridge University Press, Cambridge, pp 49–96
13.
Zurück zum Zitat Haberland C, Elahinia M, Walker JM, Meier H, Frenzel J (2014) On the development of high quality NiTi shape memory and pseudoelastic parts by additive manufacturing. Smart Mater Struct 23:104002CrossRef Haberland C, Elahinia M, Walker JM, Meier H, Frenzel J (2014) On the development of high quality NiTi shape memory and pseudoelastic parts by additive manufacturing. Smart Mater Struct 23:104002CrossRef
14.
Zurück zum Zitat Frenzel J, George EP, Dlouhy A, Somsen C, Wagner MF-X, Eggeler G (2010) Influence of Ni on martensitic phase transformations in NiTi shape memory alloys. Acta Mater 58:3444–3458CrossRef Frenzel J, George EP, Dlouhy A, Somsen C, Wagner MF-X, Eggeler G (2010) Influence of Ni on martensitic phase transformations in NiTi shape memory alloys. Acta Mater 58:3444–3458CrossRef
15.
Zurück zum Zitat Frenzel J, Zhang Z, Neuking K, Eggeler G (2004) High quality vacuum induction melting of small quantities of NiTi shape memory alloys in graphite crucibles. J Alloy Compd 385:214–223CrossRef Frenzel J, Zhang Z, Neuking K, Eggeler G (2004) High quality vacuum induction melting of small quantities of NiTi shape memory alloys in graphite crucibles. J Alloy Compd 385:214–223CrossRef
16.
Zurück zum Zitat Elahinia MH, Hashemi M, Tabesh M, Bhaduri SB (2012) Manufacturing and processing of NiTi implants: a review. Prog Mater Sci 57:911–946CrossRef Elahinia MH, Hashemi M, Tabesh M, Bhaduri SB (2012) Manufacturing and processing of NiTi implants: a review. Prog Mater Sci 57:911–946CrossRef
17.
Zurück zum Zitat Haberland C, Elahinia M, Walker J, Meier J (2013) Visions, concepts and strategies for smart NiTiNOL actuators and complex NiTiNOL structures produced by additive manufacturing, Proc ASME 2013 Conf Smart Mat, Adapt Struct Intel Syst SMASIS2013 Haberland C, Elahinia M, Walker J, Meier J (2013) Visions, concepts and strategies for smart NiTiNOL actuators and complex NiTiNOL structures produced by additive manufacturing, Proc ASME 2013 Conf Smart Mat, Adapt Struct Intel Syst SMASIS2013
18.
Zurück zum Zitat EUROFLEX GmbH, Company brochure (03/2017) High quality semi-finished products and components for the medical industry EUROFLEX GmbH, Company brochure (03/2017) High quality semi-finished products and components for the medical industry
19.
Zurück zum Zitat Melton KN (1998) General applications of SMA´s and smart materials. In: Otsuka K, Wayman CM (eds) Shape memory materials. Cambridge University Press, Cambridge, pp 220–239 Melton KN (1998) General applications of SMA´s and smart materials. In: Otsuka K, Wayman CM (eds) Shape memory materials. Cambridge University Press, Cambridge, pp 220–239
20.
Zurück zum Zitat Elahinia M, Moghaddam NS, Andani MT, Amerinatanzi A, Bimber BA, Hamilton RF (2016) Fabrication of NiTi through additive manufacturing: a review. Prog Mater Sci 83:630–663CrossRef Elahinia M, Moghaddam NS, Andani MT, Amerinatanzi A, Bimber BA, Hamilton RF (2016) Fabrication of NiTi through additive manufacturing: a review. Prog Mater Sci 83:630–663CrossRef
21.
Zurück zum Zitat van Humbeeck J (2018) Additive manufacturing of shape memory alloys. Shap Mem Superelasticity 4:309–312CrossRef van Humbeeck J (2018) Additive manufacturing of shape memory alloys. Shap Mem Superelasticity 4:309–312CrossRef
22.
Zurück zum Zitat Li S, Hassanin H, Attallah MM, Adkins NJE, Essa K (2016) The development of TiNi-based negative Poisson's ratio structure using selective laser melting. Acta Mater 105:75–83CrossRef Li S, Hassanin H, Attallah MM, Adkins NJE, Essa K (2016) The development of TiNi-based negative Poisson's ratio structure using selective laser melting. Acta Mater 105:75–83CrossRef
23.
Zurück zum Zitat Haberland C, Elahinia M (2016) Fabricating NiTi SMA Components. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 191–238 Haberland C, Elahinia M (2016) Fabricating NiTi SMA Components. In: Elahinia M (ed) Shape memory alloy actuators. Wiley, Hoboken, pp 191–238
24.
Zurück zum Zitat Abele E, Stoffregen HA, Klimkeit K, Hoche H, Oechsner M (2015) Optimisation of process parameters for lattice structures. Rapid Prototyping Journal 21:117–127CrossRef Abele E, Stoffregen HA, Klimkeit K, Hoche H, Oechsner M (2015) Optimisation of process parameters for lattice structures. Rapid Prototyping Journal 21:117–127CrossRef
25.
Zurück zum Zitat Speirs M, van Hooreweder B, van Humbeeck J, Kruth J-P (2017) Fatigue behaviour of NiTi shape memory alloy scaffolds produced by SLM, a unit cell design comparison. J Mech Behav Biomed Mater 70:53–59CrossRef Speirs M, van Hooreweder B, van Humbeeck J, Kruth J-P (2017) Fatigue behaviour of NiTi shape memory alloy scaffolds produced by SLM, a unit cell design comparison. J Mech Behav Biomed Mater 70:53–59CrossRef
26.
Zurück zum Zitat Korn H, Koch P, Kordaß R, Schöne C, Müller B, Stelzer R (2018) Influences of scan strategy and exposure parameters on diameter and surface quality of struts in lattice structures. Proc Fraunhofer Direct Digit Manuf Conf DDMC2018 Korn H, Koch P, Kordaß R, Schöne C, Müller B, Stelzer R (2018) Influences of scan strategy and exposure parameters on diameter and surface quality of struts in lattice structures. Proc Fraunhofer Direct Digit Manuf Conf DDMC2018
27.
Zurück zum Zitat Merkt SJ (2015) Qualifizierung von generativ gefertigten Gitterstrukturen für maßgeschneiderte Bauteilfunktionen, Rheinisch-Westfälische Technische Hochschule Aachen, Dissertationsschrift Merkt SJ (2015) Qualifizierung von generativ gefertigten Gitterstrukturen für maßgeschneiderte Bauteilfunktionen, Rheinisch-Westfälische Technische Hochschule Aachen, Dissertationsschrift
28.
Zurück zum Zitat Korn H, Koch P, Bittner F, Kordaß R, Holtzhausen S, Müller B, Schöne C, et al (2018) CAD-integrated slice data generation for fine lattice structures and determination of suitable manufacturing parameters for laser beam melting. Sci Artic Rapid Tech Conf (Forum AM Science) Rapid.Tech 2018 Korn H, Koch P, Bittner F, Kordaß R, Holtzhausen S, Müller B, Schöne C, et al (2018) CAD-integrated slice data generation for fine lattice structures and determination of suitable manufacturing parameters for laser beam melting. Sci Artic Rapid Tech Conf (Forum AM Science) Rapid.Tech 2018
29.
Zurück zum Zitat Koch P, Korn H, Kordaß R, Holtzhausen S, Schöne C, Müller B, Stelzer R (2018) A CAD-based workflow and mechanical characterization for additive manufacturing of tailored lattice structures. Pro Int Solid Freeform Fabr Symp SFF 2018:782–790 Koch P, Korn H, Kordaß R, Holtzhausen S, Schöne C, Müller B, Stelzer R (2018) A CAD-based workflow and mechanical characterization for additive manufacturing of tailored lattice structures. Pro Int Solid Freeform Fabr Symp SFF 2018:782–790
30.
Zurück zum Zitat Vock S, Klöden B, Kirchner A, Weißgärber T, Kieback B (2019) Powders for powder bed fusion: a review. Prog Addit Manuf 67:544 Vock S, Klöden B, Kirchner A, Weißgärber T, Kieback B (2019) Powders for powder bed fusion: a review. Prog Addit Manuf 67:544
31.
Zurück zum Zitat Westermann J, Raatz G (2016) Improving quality control through effective particle characterisation of metal powders. Powder Metall Rev 5:95–99 Westermann J, Raatz G (2016) Improving quality control through effective particle characterisation of metal powders. Powder Metall Rev 5:95–99
32.
Zurück zum Zitat Gerking C (2018) The finest art of atomizing metal melts: the crucible-free nanoval process. Proc Fraunhofer Direct Digit Manuf Conf DDMC2018 Gerking C (2018) The finest art of atomizing metal melts: the crucible-free nanoval process. Proc Fraunhofer Direct Digit Manuf Conf DDMC2018
33.
Zurück zum Zitat Gustmann T, Schwab H, Kühn U, Pauly S (2018) Selective laser remelting of an additively manufactured Cu-Al-Ni-Mn shape-memory alloy. Mater Des 153:129–138CrossRef Gustmann T, Schwab H, Kühn U, Pauly S (2018) Selective laser remelting of an additively manufactured Cu-Al-Ni-Mn shape-memory alloy. Mater Des 153:129–138CrossRef
34.
Zurück zum Zitat Gustmann T, dos Santos JM, Gargarella P, Kühn U, van Humbeeck J, Pauly S (2017) Properties of Cu-based shape-memory alloys prepared by selective laser melting. Shap Mem Superelasticity 3:24–36CrossRef Gustmann T, dos Santos JM, Gargarella P, Kühn U, van Humbeeck J, Pauly S (2017) Properties of Cu-based shape-memory alloys prepared by selective laser melting. Shap Mem Superelasticity 3:24–36CrossRef
35.
Zurück zum Zitat Bormann T, Müller B, Schinhammer M, Kessler A, Thalmann P, de Wild M (2014) Microstructure of selective laser melted nickel–titanium. Mater Charact 94:189–202CrossRef Bormann T, Müller B, Schinhammer M, Kessler A, Thalmann P, de Wild M (2014) Microstructure of selective laser melted nickel–titanium. Mater Charact 94:189–202CrossRef
36.
Zurück zum Zitat Saedi S, Turabi AS, Andani MT, Moghaddam NS, Elahinia M, Karaca HE (2017) Texture, aging, and superelasticity of selective laser melting fabricated Ni-rich NiTi alloys. Mater Sci Eng, A 686:1–10CrossRef Saedi S, Turabi AS, Andani MT, Moghaddam NS, Elahinia M, Karaca HE (2017) Texture, aging, and superelasticity of selective laser melting fabricated Ni-rich NiTi alloys. Mater Sci Eng, A 686:1–10CrossRef
37.
Zurück zum Zitat Zeidler H, Boettger-Hiller F, Edelmann J, Schubert A (2016) Surface finish machining of medical parts using plasma electrolytic polishing. Procedia CIRP 49:83–87CrossRef Zeidler H, Boettger-Hiller F, Edelmann J, Schubert A (2016) Surface finish machining of medical parts using plasma electrolytic polishing. Procedia CIRP 49:83–87CrossRef
38.
Zurück zum Zitat Moghaddam NS, Saedi S, Amerinatanzi A, Hinojos A, Ramazani A, Kundin J, Mills MJ et al (2019) Achieving superelasticity in additively manufactured NiTi in compression without post-process heat treatment. Sci Rep 9:41CrossRef Moghaddam NS, Saedi S, Amerinatanzi A, Hinojos A, Ramazani A, Kundin J, Mills MJ et al (2019) Achieving superelasticity in additively manufactured NiTi in compression without post-process heat treatment. Sci Rep 9:41CrossRef
39.
Zurück zum Zitat Sam J, Franco B, Ma J, Karaman I, Elwany A, Mabe JH (2018) Tensile actuation response of additively manufactured nickel-titanium shape memory alloys. Scripta Mater 146:164–168CrossRef Sam J, Franco B, Ma J, Karaman I, Elwany A, Mabe JH (2018) Tensile actuation response of additively manufactured nickel-titanium shape memory alloys. Scripta Mater 146:164–168CrossRef
Metadaten
Titel
Properties of a superelastic NiTi shape memory alloy using laser powder bed fusion and adaptive scanning strategies
verfasst von
Tobias Gustmann
Florian Gutmann
Franziska Wenz
Peter Koch
Ralph Stelzer
Welf-Guntram Drossel
Hannes Korn
Publikationsdatum
27.02.2020
Verlag
Springer International Publishing
Erschienen in
Progress in Additive Manufacturing / Ausgabe 1/2020
Print ISSN: 2363-9512
Elektronische ISSN: 2363-9520
DOI
https://doi.org/10.1007/s40964-020-00118-6

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