Skip to main content
Erschienen in: Wood Science and Technology 3/2015

01.05.2015 | Original

Light microscopic detection of UF adhesive in industrial particle board

verfasst von: Eike Mahrdt, Frank Stöckel, Hendrikus W. G. van Herwijnen, Ulrich Müller, Wolfgang Kantner, Johann Moser, Wolfgang Gindl-Altmutter

Erschienen in: Wood Science and Technology | Ausgabe 3/2015

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

A new procedure to detect urea–formaldehyde adhesive in industrial particle board is presented. The method uses thin sections stained with a visible dye (gentian violet) and a fluorescent dye (brilliant sulphaflavine), respectively, in a two-step procedure. Microscope images of a selected area of interest acquired in visible and fluorescence modes are combined to obtain sufficient contrast, enabling semi-automated detection of adhesive by means of image analysis. No addition of dye prior to particle board production is necessary.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Literatur
Zurück zum Zitat Cyr PL, Riedl B, Wang XM, Shaler S (2006) Urea-melamine-formaldehyde (UMF) resin penetration in medium-density fibreboard (MDF) wood fibers. J Adhes Sci Technol 20(8):787–801CrossRef Cyr PL, Riedl B, Wang XM, Shaler S (2006) Urea-melamine-formaldehyde (UMF) resin penetration in medium-density fibreboard (MDF) wood fibers. J Adhes Sci Technol 20(8):787–801CrossRef
Zurück zum Zitat Dunky M (1998) Urea-formaldehyde (UF) adhesive resins for wood. Int J Adhes Adhes 18:95–107CrossRef Dunky M (1998) Urea-formaldehyde (UF) adhesive resins for wood. Int J Adhes Adhes 18:95–107CrossRef
Zurück zum Zitat Evans PD, Morrison O, Senden TJ, Vollmer S, Roberts RJ, Limaye A, Arns CH, Averdunk H, Lowe A, Knackstedt MA (2010) Visualization and numerical analysis of adhesive distribution in particleboard using X-ray micro-computed tomography. Int J Adhes Adhes 30(8):754–762CrossRef Evans PD, Morrison O, Senden TJ, Vollmer S, Roberts RJ, Limaye A, Arns CH, Averdunk H, Lowe A, Knackstedt MA (2010) Visualization and numerical analysis of adhesive distribution in particleboard using X-ray micro-computed tomography. Int J Adhes Adhes 30(8):754–762CrossRef
Zurück zum Zitat Gierlinger N, Hansmann C, Röder T, Sixta H, Gindl W, Wimmer R (2005) Comparison of UV and confocal Raman microscopy to measure the melamine-formaldehyde resin content within cell walls of impregnated spruce wood. Holzforschung 59(2):210–213CrossRef Gierlinger N, Hansmann C, Röder T, Sixta H, Gindl W, Wimmer R (2005) Comparison of UV and confocal Raman microscopy to measure the melamine-formaldehyde resin content within cell walls of impregnated spruce wood. Holzforschung 59(2):210–213CrossRef
Zurück zum Zitat Ginzel W, Stegmann G (1970) Subsequent colouring of urea-formaldehyde resins on glued wood particles for visual estimation of glue distribution (In German). Holz Roh Werkst 28(8):289–292CrossRef Ginzel W, Stegmann G (1970) Subsequent colouring of urea-formaldehyde resins on glued wood particles for visual estimation of glue distribution (In German). Holz Roh Werkst 28(8):289–292CrossRef
Zurück zum Zitat Grigsby W, Thumm A (2004) Visualisation of UF resin on MDF fibre by XPS imaging. Holz Roh Werkst 62(5):365–369CrossRef Grigsby W, Thumm A (2004) Visualisation of UF resin on MDF fibre by XPS imaging. Holz Roh Werkst 62(5):365–369CrossRef
Zurück zum Zitat Grigsby W, McDonald AG, Thumm A, Loxton C (2004) X-ray photoelectron spectroscopy determination of urea formaldehyde resin coverage on MDF fibre. Holz Roh Werkst 62(5):358–364CrossRef Grigsby W, McDonald AG, Thumm A, Loxton C (2004) X-ray photoelectron spectroscopy determination of urea formaldehyde resin coverage on MDF fibre. Holz Roh Werkst 62(5):358–364CrossRef
Zurück zum Zitat Grigsby WJ, Thumm A, Kamke FA (2005) Determination of resin distribution and coverage in MDF by fiber staining. Wood Fiber Sci 37(2):258–269 Grigsby WJ, Thumm A, Kamke FA (2005) Determination of resin distribution and coverage in MDF by fiber staining. Wood Fiber Sci 37(2):258–269
Zurück zum Zitat Hass P, Wittel FK, Mendoza M, Herrmann HJ, Niemz P (2012) Adhesive penetration in beech wood: experiments. Wood Sci Technol 46:243–256CrossRef Hass P, Wittel FK, Mendoza M, Herrmann HJ, Niemz P (2012) Adhesive penetration in beech wood: experiments. Wood Sci Technol 46:243–256CrossRef
Zurück zum Zitat Kamke FA, Lee JN (2007) Adhesive penetration in wood: a review. Wood Fiber Sci 39(2):205–220 Kamke FA, Lee JN (2007) Adhesive penetration in wood: a review. Wood Fiber Sci 39(2):205–220
Zurück zum Zitat Kamke FA, Scott KA, Ra J-B, Kamke CJC (2000) Detection of urea formaldehyde resin in MDF fiber. In: Christiansen AW, Conner AH, Baumann MGD et al. (eds) Wood adhesives 2000, South Lake Tahoe, Nevada, Forest Products Society, June 22–23, 2000 Kamke FA, Scott KA, Ra J-B, Kamke CJC (2000) Detection of urea formaldehyde resin in MDF fiber. In: Christiansen AW, Conner AH, Baumann MGD et al. (eds) Wood adhesives 2000, South Lake Tahoe, Nevada, Forest Products Society, June 22–23, 2000
Zurück zum Zitat Leemann U, Ruch F (1972) Cytofluorometric determination of basic and total proteins with sulfaflavine. J Histochem Cytochem 20(9):659–671CrossRefPubMed Leemann U, Ruch F (1972) Cytofluorometric determination of basic and total proteins with sulfaflavine. J Histochem Cytochem 20(9):659–671CrossRefPubMed
Zurück zum Zitat Loxton C, Thumm A, Grigsby WJ, Adams TA, Ede RM (2003) Resin distribution in medium density fibreboard, Quantification of UF resin distribution on blowline- and dry-blended MDF fiber and panels. Wood Fiber Sci 35(3):370–380 Loxton C, Thumm A, Grigsby WJ, Adams TA, Ede RM (2003) Resin distribution in medium density fibreboard, Quantification of UF resin distribution on blowline- and dry-blended MDF fiber and panels. Wood Fiber Sci 35(3):370–380
Zurück zum Zitat Niemz P, Wienhaus O, Schaarschmidt K, Sander D (1990) Methods for measuring the adhesive content (In German), Patent office of German Democratic Republic. 277333 A1 Niemz P, Wienhaus O, Schaarschmidt K, Sander D (1990) Methods for measuring the adhesive content (In German), Patent office of German Democratic Republic. 277333 A1
Zurück zum Zitat Pakdel H, Cyr PL, Riedl B, Deng J (2008) Quantification of urea formaldehyde resin in wood fibers using X-ray photoelectron spectroscopy and confocal laser scanning microscopy. Wood Sci Technol 42(2):133–148CrossRef Pakdel H, Cyr PL, Riedl B, Deng J (2008) Quantification of urea formaldehyde resin in wood fibers using X-ray photoelectron spectroscopy and confocal laser scanning microscopy. Wood Sci Technol 42(2):133–148CrossRef
Zurück zum Zitat Riegler M, Gindl-Altmutter W, Hauptmann M, Müller U (2012) Detection of UF resin on wood particles and in particleboards: potential of selected methods for practice-oriented offline detection. Eur J Wood Prod 70(6):829–837CrossRef Riegler M, Gindl-Altmutter W, Hauptmann M, Müller U (2012) Detection of UF resin on wood particles and in particleboards: potential of selected methods for practice-oriented offline detection. Eur J Wood Prod 70(6):829–837CrossRef
Zurück zum Zitat Sernek M, Resnik J, Kamke FA (1999) Penetration of liquid urea-formaldehyde adhesive into beech wood. Wood Fiber Sci 31(1):41–48 Sernek M, Resnik J, Kamke FA (1999) Penetration of liquid urea-formaldehyde adhesive into beech wood. Wood Fiber Sci 31(1):41–48
Zurück zum Zitat Standfest G, Kranzer S, Petutschnigg A, Dunky M (2010) Determination of the microstructure of an adhesive-bonded medium density fiberboard (MDF) using 3-D sub-micrometer computer tomography. J Adhes Sci Technol 24(8):1501–1514CrossRef Standfest G, Kranzer S, Petutschnigg A, Dunky M (2010) Determination of the microstructure of an adhesive-bonded medium density fiberboard (MDF) using 3-D sub-micrometer computer tomography. J Adhes Sci Technol 24(8):1501–1514CrossRef
Zurück zum Zitat Thumm A, McDonald AG, Donaldson LA (2001) Visualisation of UF resin in MDF by cathodoluminescence/scanning electron microscopy. Holz Roh Werkst 59(3):215–216CrossRef Thumm A, McDonald AG, Donaldson LA (2001) Visualisation of UF resin in MDF by cathodoluminescence/scanning electron microscopy. Holz Roh Werkst 59(3):215–216CrossRef
Zurück zum Zitat Walther T, Terzic K, Donath T, Beckmann F, Thoemen H (2006) Microstructural analysis of lignocellulosic fiber networks. In: Progress in biomedical optics and imaging: proceedings of SPIE, developments in X-Ray tomography V, San Diego, United States, 2006, Vol. 6318, Article number 631812 Walther T, Terzic K, Donath T, Beckmann F, Thoemen H (2006) Microstructural analysis of lignocellulosic fiber networks. In: Progress in biomedical optics and imaging: proceedings of SPIE, developments in X-Ray tomography V, San Diego, United States, 2006, Vol. 6318, Article number 631812
Zurück zum Zitat Wilson JB, Krahmer RL (1976) Particleboard: microscopic observations of resin distribution and board fracture. Forest Prod J 26(11):42–45 Wilson JB, Krahmer RL (1976) Particleboard: microscopic observations of resin distribution and board fracture. Forest Prod J 26(11):42–45
Zurück zum Zitat Xing C, Riedl B, Cloutier A, Shaler SM (2005) Characterisation of urea-formaldehyde resin penetration into medium density fiber-board fibers. Wood Sci Technol 39(5):374–384CrossRef Xing C, Riedl B, Cloutier A, Shaler SM (2005) Characterisation of urea-formaldehyde resin penetration into medium density fiber-board fibers. Wood Sci Technol 39(5):374–384CrossRef
Zurück zum Zitat Xing C, Riedl B, Cloutier A, Deng J, Zhang SY (2006) UF resin efficiency of MDF as affected by resin content loss, coverage level and pre-cure. Holz Roh Werkst 64(3):221–226CrossRef Xing C, Riedl B, Cloutier A, Deng J, Zhang SY (2006) UF resin efficiency of MDF as affected by resin content loss, coverage level and pre-cure. Holz Roh Werkst 64(3):221–226CrossRef
Metadaten
Titel
Light microscopic detection of UF adhesive in industrial particle board
verfasst von
Eike Mahrdt
Frank Stöckel
Hendrikus W. G. van Herwijnen
Ulrich Müller
Wolfgang Kantner
Johann Moser
Wolfgang Gindl-Altmutter
Publikationsdatum
01.05.2015
Verlag
Springer Berlin Heidelberg
Erschienen in
Wood Science and Technology / Ausgabe 3/2015
Print ISSN: 0043-7719
Elektronische ISSN: 1432-5225
DOI
https://doi.org/10.1007/s00226-015-0715-y

Weitere Artikel der Ausgabe 3/2015

Wood Science and Technology 3/2015 Zur Ausgabe