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31.01.2020 | Original Research

Superior crack initiation and growth characteristics of cellulose nanopapers

verfasst von: Chengyun Miao, Haishun Du, Mahesh Parit, Zhihua Jiang, Hareesh V. Tippur, Xinyu Zhang, Zhongqi Liu, Junhao Li, Ruigang Wang

Erschienen in: Cellulose | Ausgabe 6/2020

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Abstract

In this work, tension and fracture behaviors of cellulose nanopaper (CNP) made from two different preparation approaches are comparatively studied. The CNP are prepared by casting (or C-CNP) and filtration (or F-CNP) of CNF suspension. The resulting CNP are mechanically characterized using the vision-based full-field optical method of Digital Image Correlation. Tension tests show that F-CNP has a higher strength and greater nonlinearity than the C-CNP. The crack initiation and growth characteristics of the two types of CNP are investigated using optical measurements. The data are analyzed under small-scale-yielding conditions to quantify the fracture parameters such as stress intensity factors and energy release rates at crack initiation as well as during crack growth. The results indicate that both C-CNP and F-CNP show significant crack growth resistance in the post-crack initiation regime. The F-CNP particularly offers substantial resistance to crack growth relative to the C-CNP demonstrating that filtration is the preferred method to make CNP with higher tensile strength and better fracture properties.

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Vorheriger Artikel Cellulose II nanocrystal: a promising bio-template for porous or hollow nano SiO2 fabrication

Nächster Artikel Synthesis and characterization of triazole based sulfonated nanocrystalline cellulose proton conductor

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It is worth noting that values of SIF at crack initiation of C-CNP are comparable to conventional tough polymers such as bulk polycarbonate (K_Ic = 3–4 MPa√m) which offers lower elastic modulus (E = 2.5 GPa). The same for F-CNP are substantially higher, by 50%, suggesting a clear superiority in terms of crack initiation.

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Titel: Superior crack initiation and growth characteristics of cellulose nanopapers
verfasst von: Chengyun Miao
Haishun Du
Mahesh Parit
Zhihua Jiang
Hareesh V. Tippur
Xinyu Zhang
Zhongqi Liu
Junhao Li
Ruigang Wang
Publikationsdatum: 31.01.2020
Verlag: Springer Netherlands
Erschienen in: Cellulose / Ausgabe 6/2020
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI: https://doi.org/10.1007/s10570-020-03015-x

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Abstract

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