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Erschienen in:
06.12.2017
Synthesis, growth and characterization of dichlorobis(4-chloroaniline-κN)zinc semiorganic crystal
Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 5/2018
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Abstract
Semiorganic material dichlorobis(4-chloroaniline-κN)zinc (DCBCAZ) was synthesized and single crystal of DCBCAZ was grown at room temperature by slow evaporation solution growth technique. Fourier transform infrared and Fourier transform Raman spectral studies confirmed the presence of functional groups in the DCBCAZ material. Three dimensional crystal structure elucidated from single crystal X-ray diffraction analysis showed that DCBCAZ crystallizes in monoclinic crystal system with centrosymmetric space group C2/c. Crystalline perfection of the grown crystal was studied by employing high resolution X-ray diffraction analysis. Mechanical properties were estimated using Vicker’s microhardness test which shows that DCBCAZ belongs to the soft materials category. Thermal properties were carried out using thermogravimetric and differential thermal analyses and the DCBCAZ melts at 135 °C. The antibacterial activity of DCBCAZ was tested using disk diffusion method.