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Journal of Nanoparticle Research
Erschienen in: Journal of Nanoparticle Research 4/2012

01.03.2012 | Brief Communication

One-pot reaction to synthesize superparamagnetic iron oxide nanoparticles by adding phenol as reducing agent and stabilizer

verfasst von: Yuanfeng Wang, Zhanwang Zhu, Feng Xu, Xinlin Wei

Erschienen in: Journal of Nanoparticle Research | Ausgabe 4/2012

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Abstract

An improved thermal decomposition method was used to directly prepare water-soluble Fe3O4 magnetic nanoparticles (MNPs) with relatively higher quality via reductive decomposition of ferric acetylacetonate [Fe(acac)3], in the presence of benzyl ether and phenol, in which inexpensive phenol acted as reducing agent and stabilizer, produce the semi phenol-benzoquinone coated on the Fe3O4 and make the Fe3O4·MNPs water-soluble and the colloidal solution stable. By changing the molar ratio of phenol to Fe(acac)3 and reaction time, the size of Fe3O4·MNPs could be varied from 19.3 ± 4.4 nm to 9.7 ± 1.5 nm, with the saturation magnetizations in the range of 51.3–62.9 emu/g.
Vorheriger Artikel Early patterns of commercial activity in graphene
Nächster Artikel A novel ethanol templating synthesis of ordered lamellar superstructured crystalline zirconia

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Metadaten
Titel
One-pot reaction to synthesize superparamagnetic iron oxide nanoparticles by adding phenol as reducing agent and stabilizer
verfasst von
Yuanfeng Wang
Zhanwang Zhu
Feng Xu
Xinlin Wei
Publikationsdatum
01.03.2012
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 4/2012
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-012-0755-2

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