nach oben

Journal of Nanoparticle Research

Erschienen in:

01.09.2020 | Research paper

Synthesis and characterization of elution behavior of nonspherical gold nanoparticles in asymmetrical flow field-flow fractionation (AsFlFFF)

verfasst von: Jangjae Lee, Emad S. Goda, Jeayeong Choi, Joontaek Park, Seungho Lee

Erschienen in: Journal of Nanoparticle Research | Ausgabe 9/2020

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

Asymmetrical flow FFF (AsFlFFF) is a member of field-flow fractionation (FFF) and can provide the separation of particles with size from nano to microscale based on their hydrodynamic diameters with smaller particles being eluted earlier than larger ones. For spheres, if the AsFlFFF conditions are well optimized, the FFF theory allows prediction of the elution time for a given diameter. Herein, we aim to use the AsFlFFF channel to compare the elution behavior of the gold nanoparticles with three different morphologies and give a comprehensive depiction for the mechanism of their separation in AsFlFFF. Furthermore, the particles size obtained from AsFlFFF was compared with that obtained from other techniques such as transmission electron microscopy (TEM), and dynamic light scattering. In this study, gold nanospheres (GNS), gold nanotriangles (GNT), and gold nanorods (GNR) were synthesized. TEM data stated that the mean particle diameter and the edge length of GNS and GNT were 51 and 35 nm, respectively, and the length of GNR was 47 nm. Although, the diameter of GNS is close to the length of GNR, the elution time of GNS (4.45 min) was much longer than that of the GNR (3.70 min) at the same AsFlFFF conditions. Also, the elution time of GNT was longer than that of GNR, even though it has smaller size than GNR. This might be attributed to GNR reaching an equilibrium position that is farther away from the accumulation wall of the channel than GNS, resulting in earlier elution than GNS. The GNT particles are rather similar in shape to spheres, and may behave more closely to the spheres than GNR. It seem that AsFlFFF could be an analytical technique for particle size analysis and separation of nanoparticles of different shapes.

Vorheriger Artikel The photocatalytic selectivity between molecularly imprinted TiO2 and target contaminants

Nächster Artikel In vivo fate of Ag2Te quantum dot and comparison with other NIR-II silver chalcogenide quantum dots

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Abu Elella MH, ElHafeez EA, Goda ES, Lee S, Yoon KR (2019) Smart bactericidal filter containing biodegradable polymers for crystal violet dye adsorption. Cellulose 26(17):9179–9206. https://doi.org/10.1007/s10570-019-02698-1CrossRef

Alfi M, Park J (2014) Theoretical analysis of the local orientation effect and the lift-hyperlayer mode of rodlike particles in field-flow fractionation. J Sep Sci 37(7):876–883. https://doi.org/10.1002/jssc.201300902CrossRef

Al-Shalalfeh MM, Saleh TA, Al-Saadi AA (2016) Silver colloid and film substrates in surface-enhanced Raman scattering for 2-thiouracil detection. RSC Adv 6(79):75282–75292. https://doi.org/10.1039/c6ra14832hCrossRef

Al-Shalalfeh MM, Onawole AT, Saleh TA, Al-Saadi AA (2017) Spherical silver nanoparticles as substrates in surface-enhanced Raman spectroscopy for enhanced characterization of ketoconazole. Mater Sci Eng C Mater Biol Appl 76:356–364. https://doi.org/10.1016/j.msec.2017.03.081CrossRef

Amde M, Tan ZQ, Liu J (2019) Separation and size characterization of zinc oxide nanoparticles in environmental waters using asymmetrical flow field-flow fractionation. Talanta 200:357–365. https://doi.org/10.1016/j.talanta.2019.03.074CrossRef

Aureli A, Damato M, Raggi A, Cubadda F (2015) Quantitative characterization of silica nanoparticles by asymmetric flow field flow fractionation coupled with online multiangle light scattering and ICP - MS/MS detection. J Anal At Spectrom 30:1266–1273CrossRef

Bae J, Kim W, Rah K, Jung EC, Lee S (2012) Application of flow field-flow fractionation (FlFFF) for size characterization of carbon black particles in ink. Microchem J 104:44–48. https://doi.org/10.1016/j.microc.2012.04.007CrossRef

Chen B, Selegue JP (2002) Separation and characterization of single-walled and multiwalled carbon nanotubes by using flow field-flow fractionation. Anal Chem 74:4774–4780CrossRef

Choi J, Kwen HD, Kim YS, Choi SH, Lee S (2014) γ-Ray synthesis and size characterization of CdS quantum dot (QD) particles using flow and sedimentation field-flow fractionation (FFF). Microchem J 117:34–39. https://doi.org/10.1016/j.microc.2014.06.002CrossRef

Chun J, Fagan JA, Hobbie EK, Bauer BJ (2008) Size separation of single-wall carbon nanotubesby flow-field flow fractionation. Anal Chem 80:2514–2523CrossRef

Dou H, Zhou B, Jang HD, Lee S (2014) Study on antidiabetic activity of wheat and barley starch using asymmetrical flow field-flow fractionation coupled with multiangle light scattering. J Chromatogr A 1340:115–120. https://doi.org/10.1016/j.chroma.2014.03.014CrossRef

Gab-Allah MA, Goda ES, Shehata AB, Gamal H (2020) Critical review on the analytical methods for the determination of sulfur and trace elements in crude oil. Crit Rev Anal Chem 50(2):161–178. https://doi.org/10.1080/10408347.2019.1599278CrossRef

Giddings JC, Yang FJ, Myers MN (1976) Flow-field-flow fractionation: a versatile new separation method. Science 193(4259):1244–1245CrossRef

Gigault J, Cho TJ, MacCuspie RI, Hackley VA (2013) Gold nanorod separation and characterization by asymmetric-flow field flow fractionation with UV-Vis detection. Anal Bioanal Chem 405(4):1191–1202. https://doi.org/10.1007/s00216-012-6547-9CrossRef

Goda ES, Yoon KR, El-sayed SH, Hong SE (2018) Halloysite nanotubes as smart flame retardant and economic reinforcing materials: a review. Thermochim Acta 669:173–184. https://doi.org/10.1016/j.tca.2018.09.017CrossRef

Goda ES, Gab-Allah MA, Singu BS, Yoon KR (2019) Halloysite nanotubes based electrochemical sensors: a review. Microchem J 147:1083–1096. https://doi.org/10.1016/j.microc.2019.04.011CrossRef

Goda ES, Lee S, Sohail M, Yoon KR (2020a) Prussian blue and its analogues as advanced supercapacitor electrodes. J Energy Chem 50:206–229. https://doi.org/10.1016/j.jechem.2020.03.031

Goda ES, Singu BS, Hong SE, Yoon KR (2020b) Good dispersion of poly(δ-gluconolactone)-grafted graphene in poly(vinyl alcohol) for significantly enhanced mechanical strength. Mater Chem Phys:123465. doi:https://doi.org/10.1016/j.matchemphys.2020.123465

Haruna K, Saleh TA, Al Thagfi J, Al-Saadi AA (2016a) Structural properties, vibrational spectra and surface-enhanced Raman scattering of 2,4,6-trichloro- and tribromoanilines: a comparative study. J Mol Struct 1121:7–15. https://doi.org/10.1016/j.molstruc.2016.05.021CrossRef

Haruna K, Saleh TA, Hossain MK, Al-Saadi AA (2016b) Hydroxylamine reduced silver colloid for naphthalene and phenanthrene detection using surface-enhanced Raman spectroscopy. Chem Eng J304:141–148. https://doi.org/10.1016/j.cej.2016.06.050CrossRef

Holthoff H, Egelhaaf S, Borkovec M, Schurtenberger P, Stiche H (1996) Coagulation rate measurements of colloidal particles by simultaneous static and dynamic light scattering. Langmuir 12:5541–5549CrossRef

Hormozi-Nezhad MR, Karami P, Robatjazi H (2013) A simple shape-controlled synthesis of gold nanoparticles using nonionic surfactants. RSC Adv 3:7726–7736. https://doi.org/10.1039/c3ra40280kCrossRef

Jiang XC, Pileni MP (2007) Gold nanorods: influence of various parameters as seeds, solvent, surfactant on shape control. Coll Surf A Physicochem Eng Asp 295(1–3):228–232. https://doi.org/10.1016/j.colsurfa.2006.09.003CrossRef

Kamran M, Haroon M, Popoola SA, Almohammedi AR, Al-Saadi AA, Saleh TA (2019) Characterization of valeric acid using substrate of silver nanoparticles with SERS. J Mol Liq 273:536–542. https://doi.org/10.1016/j.molliq.2018.10.037CrossRef

Kuttner C, Mayer M, Dulle M, Moscoso A, Lopez-Romero JM, Forster S, Fery A, Perez-Juste J, Contreras-Caceres R (2018) Seeded growth synthesis of gold nanotriangles: size control, SAXS analysis, and SERS performance. ACS Appl Mater Interfaces 10(13):11152–11163. https://doi.org/10.1021/acsami.7b19081CrossRef

Lee S, Rao SP, Moon M, Giddings JC (1996) Determination of mean diameter and particle size distribution of acrylate latex using flow field-flow fractionation, photon correlation spectroscopy, and electron microscopy. Anal Chem 68:1545–1549CrossRef

Lee JH, Gibson KJ, Chen G, Weizmann Y (2015) Bipyramid-templated synthesis of monodisperse anisotropic gold nanocrystals. Nat Commun 6:7571. https://doi.org/10.1038/ncomms8571CrossRef

Letzel A, Gökce B, Menzel A, Plech A, Barcikowski S (2018) Primary particle diameter differentiation and bimodality identification by five analytical methods using gold nanoparticle size distributions synthesized by pulsed laser ablation in liquids. Appl Surf Sci 435:743–751. https://doi.org/10.1016/j.apsusc.2017.11.130CrossRef

Li J, Kan C, Liu Y, Xu J, Wang C, Ni Y, Ke S (2017) The growth of Cu nanostructures induced by Au nanobipyramids. Journal of advances in Nanomaterials 2(4):219–227. https://doi.org/10.22606/jan.2017.24004CrossRef

Lim J, Yeap SP, Che H, Low SC (2013) Characterization of magnetic nanoparticle by dynamic light scattering. Nanoscale Res Lett 8:1–14CrossRef

Liu X, Dai Q, Austin L, Coutts J, Knowles G, Zou J, Chen H, Huo Q (2008) A one-step homogeneous immunoassay for cancer biomarker detection using gold nanoparticle probes coupled with dynamic light scattering. J Am Chem Soc 30:2780–2782CrossRef

Liu H, Pierre-Pierre N, Huo Q (2012) Dynamic light scattering for gold nanorod size characterization and study of nanorod–protein interactions. Gold Bull 45(4):187–195. https://doi.org/10.1007/s13404-012-0067-4CrossRef

Long NN, Vu LV, Kiem CD, Doanh SC, Nguyet CT, Hang PT, Thien ND, Quynh LM (2009) Synthesis and optical properties of colloidal gold nanoparticles. J Phys Conf Ser 187:1–8. https://doi.org/10.1088/1742-6596/187/1/012026CrossRef

Martin-Sanchez C, Gonzalez-Rubio G, Mulvaney P, Guerrero-Martinez A, Liz-Marzan LM, Rodriguez F (2019) Monodisperse gold nanorods for high-pressure refractive index sensing. J Phys Chem Lett 10(7):1587–1593. https://doi.org/10.1021/acs.jpclett.9b00636CrossRef

Meisterjahn B, Wagner S, von der Kammer F, Hennecke D, Hofmann T (2016) Silver and gold nanoparticle separation using asymmetrical flow-field flow fractionation: influence of run conditions and of particle and membrane charges. J Chromatogr A 1440:150–159. https://doi.org/10.1016/j.chroma.2016.02.059CrossRef

Mekprayoon S, Siripinyanond A (2019) Performance evaluation of flow field-flow fractionation and electrothermal atomic absorption spectrometry for size characterization of gold nanoparticles. J Chromatogr A 1604:460493. https://doi.org/10.1016/j.chroma.2019.460493CrossRef

Monikh FA, Grundschober N, Romeijn S, Arenas-Lago D, Vijver MG, Jiskoot W, Peijnenburg W (2019) Development of methods for extraction and analytical characterization of carbon-based nanomaterials (nanoplastics and carbon nanotubes) in biological and environmental matrices by asymmetrical flow field-flow fractionation. Environ Pollut 255(Pt 2):113304. https://doi.org/10.1016/j.envpol.2019.113304

Nguyen TM, Pettibone JM, Gigault J, Hackley VA (2016) In situ monitoring, separation, and characterization of gold nanorod transformation during seed-mediated synthesis. Anal Bioanal Chem 408(9):2195–2201. https://doi.org/10.1007/s00216-016-9366-6CrossRef

Nikoobakht B, El-Sayed MA (2003) Preparation and growth mechanism of gold Nanorods (NRs) using seed-mediated growth method. Chem Mater 15:1957–1962CrossRef

Nikoobakht B, Wang J, El-Sayed MA (2002) Surface-enhanced Raman scattering of molecules adsorbedon gold nanorods: off-surface plasmon resonance condition. Chem Phys Lett 366:17–23CrossRef

Onawole AT, Popoola SA, Saleh TA, Al-Saadi AA (2018) Silver-loaded graphene as an effective SERS substrate for clotrimazole detection: DFT and spectroscopic studies. Spectrochim Acta A Mol Biomol Spectrosc 201:354–361. https://doi.org/10.1016/j.saa.2018.05.018CrossRef

Park J (2014) Shape-based particle separation using field flow fractionation: past and current research. Laboratory Journal – Business Web for Users in Science and Industry PP1–3

Phelan FR Jr, Bauer BJ (2007) Simulation of nanotube separation in field-flow fractionation (FFF). Chem Eng Sci 62(17):4620–4635. https://doi.org/10.1016/j.ces.2007.04.019CrossRef

Ratanathanawongs SK, Lee I, Giddings J (1991) Separation and characterization of 0.01-50 um particles using flow field-flow fractionation. J C ACS Symp Ser 472:229-246 " in Particle size distribution II, T Provder, Ed, ACS Symp Series No 472, American Chemical Society, Washington, DC, 1991, Chapter 15

Runyon JR, Goering A, Yong KT, Williams SK (2013) Preparation of narrow dispersity gold nanorods by asymmetrical flow field-flow fractionation and investigation of surface plasmon resonance. Anal Chem 85(2):940–948. https://doi.org/10.1021/ac302571gCrossRef

Saleh TA, Al-Shalalfeh MM, Al-Saadi AA (2016) Graphene Dendrimer-stabilized silver nanoparticles for detection of methimazole using surface-enhanced Raman scattering with computational assignment. Sci Rep 6:32185. https://doi.org/10.1038/srep32185CrossRef

Saleh TA, Al-Shalalfeh MM, Al-Saadi AA (2017) Silver nanoparticles for detection of methimazole by surface-enhanced Raman spectroscopy. Mater Res Bull 91:173–178. https://doi.org/10.1016/j.materresbull.2017.03.041CrossRef

Saleh TA, Al-Shalalfeh MM, Al-Saadi AA (2018) Silver loaded graphene as a substrate for sensing 2-thiouracil using surface-enhanced Raman scattering. Sens Actuators B Chem 254:1110–1117. https://doi.org/10.1016/j.snb.2017.07.179CrossRef

Scarabelli L, Coronado-Puchau M, Giner-Casares J, Langer J, Liz-Marza’n L (2014) Monodisperse gold Nanotriangles: size control, large-scale self assembly, and performance in surface-enhanced Raman scattering. ACS Nano 8:5833–5842

Schimpf ME, Caldwell K, Giddings JC (2000a) Field-flow fractionation handbook. Mark R Schure, Martin E Schimpf, PD Schettler (Eds), Chapter 2 Retention-Normal Mode, Wiley-Interscience, New York, pp 31–48

Schimpf ME, Caldwell K, Giddings JC (2000b) Field-flow fractionation handbook. KG Wahlund (Ed), Chapter 18 Asymmetrical Flow Field-Flow Fractionation, Wiley-Interscience, New York, pp 279–294

Smitha SL, Gopchandran KG, Smijesh N, Philip R (2013) Size-dependent optical properties of Au nanorods. Prog Nat Sci 23(1):36–43. https://doi.org/10.1016/j.pnsc.2013.01.005CrossRef

Thünemann A, Kegel J, Polte J, Emmerling F (2008) Superparamagnetic maghemite nanorods: analysis by coupling field-flow fractionation and small-angle X-ray scattering. Anal Chem 80:5905–5911CrossRef

Tomar A, Garg G (2013) Short review on application of gold nanoparticles. Glob J Pharmacol 7(1):34–38. https://doi.org/10.5829/idosi.gjp.2013.7.1.66173CrossRef

Wei G-T, Liu F-K, Wang C (1999) Shape separation of nanometer gold particles by size-exclusion chromatography. Anal Chem 71:2085–2091CrossRef

Williams S, Caldwell KD (2012) Field-flow fractionation in biopolymer analysis. (1st ed), Springer-Verlag, Wien

Yeh YC, Creran B, Rotello VM (2012) Gold nanoparticles: preparation, properties, and applications in bionanotechnology. Nanoscale 4(6):1871–1880. https://doi.org/10.1039/c1nr11188dCrossRef

Zheng T, Bott S, Huo Q (2016) Techniques for accurate sizing of gold nanoparticles using dynamic light scattering with particular application to chemical and biological sensing based on aggregate formation. ACS Appl Mater Interfaces 8(33):21585–21594. https://doi.org/10.1021/acsami.6b06903CrossRef

Zimbone M, Baeri P, Calcagno L, Musumeci P, Contino A, Barcellona ML, Bonaventura G (2014) Dynamic light scattering on bioconjugated laser generated gold nanoparticles. PLoS One 9(3):e89048. https://doi.org/10.1371/journal.pone.0089048CrossRef

Zuber A, Purdey M, Schartner E, Forbes C, van der Hoek B, Giles D, Abell A, Monro T, Ebendorff-Heidepriem H (2016) Detection of gold nanoparticles with different sizes using absorption and fluorescence based method. Sensors Actuators B Chem 227:117–127. https://doi.org/10.1016/j.snb.2015.12.044CrossRef

Titel: Synthesis and characterization of elution behavior of nonspherical gold nanoparticles in asymmetrical flow field-flow fractionation (AsFlFFF)
verfasst von: Jangjae Lee
Emad S. Goda
Jeayeong Choi
Joontaek Park
Seungho Lee
Publikationsdatum: 01.09.2020
Verlag: Springer Netherlands
Erschienen in: Journal of Nanoparticle Research / Ausgabe 9/2020
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-020-04987-4

Premium Partner

Marktübersichten

Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.

Zur Marktübersicht

Springer Professional

Abstract

Bitte loggen Sie sich ein, um Zugang zu Ihrer Lizenz zu erhalten.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Springer Professional "Technik"

Weitere Artikel der Ausgabe 9/2020

Band energy modulation on Cu-doped Sb2S3-based photoelectrodes for charge generation and transfer property of quantum dot–sensitized solar cells

44Ti diffusion labelling of commercially available, engineered TiO2 and SiO2 nanoparticles

Structural evolution, electronic and physicochemical properties of tin ozonide nanoclusters: a density functional theory perspective

Coupled hybrid nanoparticles for improved dispersion stability of nanosuspensions: a review

Reactive magnetron sputtered–assisted deposition of nanocomposite thin films with tuneable magnetic, electrical and interfacial properties

La3+,Gd3+-codoped BiVO4 nanorods with superior visible-light-driven photocatalytic performance for simultaneous removing aqueous Cr(VI) and azo dye

Premium Partner

Marktübersichten