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Erschienen in: Rare Metals 9/2021

04.03.2019

Microstructure and mechanical properties of magnesium–lithium alloy prepared by friction stir processing

verfasst von: Qian-Ying Che, Kuai-She Wang, Wen Wang, Li-Ying Huang, Tian-Qi Li, Xiao-Peng Xi, Pai Peng, Ke Qiao

Erschienen in: Rare Metals | Ausgabe 9/2021

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Abstract

In this study, the fine-grained Mg–Li alloy was prepared by friction stir processing (FSP). The microstructure and mechanical properties of the friction-stir-processed (FSPed) Mg–Li alloy were investigated. The result showed that FSP resulted in the grain refinement, and the average grain size of the β-Li phase was about 7.5 μm. Besides the α-Mg and β-Li phases, a small amount of Li3Mg7, Li2MgAl and AlLi phases were obtained. Compared with the base metal (BM), the weakening of the crystallographic texture occurred in the FSPed material, and the c-axis of the α-phase and the <001> crystallographic orientation of the β-phase were tilted about 45° with respect to the transverse direction (TD). The average microhardness (HV 67.8) of the stir zone was higher than that of the BM (HV 61.5). The yield strength (YS) and the ultimate tensile strength (UTS) of the FSPed material were higher than those of the BM, while the elongation slightly reduced. Grain refinement had more significant effect on strength improvement compared with the texture variation for the FSPed material. The fracture surfaces of the BM and FSPed materials showed dimple characteristics.

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Literatur
[1]
Zurück zum Zitat Qiu X, Yang Q, Guan K, Bu F, Cao ZY, Liu YB, Meng J. Microstructures and tensile properties of Mg–Zn–(Gd)–Zr alloys extruded at various temperatures. Rare Met. 2017;36(12):962.CrossRef Qiu X, Yang Q, Guan K, Bu F, Cao ZY, Liu YB, Meng J. Microstructures and tensile properties of Mg–Zn–(Gd)–Zr alloys extruded at various temperatures. Rare Met. 2017;36(12):962.CrossRef
[2]
Zurück zum Zitat Li D, Xue HS, Yang G, Zhang DF. Microstructure and mechanical properties of Mg–6Zn–0.5Y magnesium alloy prepared with ultrasonic treatment. Rare Met. 2017;36(8):622.CrossRef Li D, Xue HS, Yang G, Zhang DF. Microstructure and mechanical properties of Mg–6Zn–0.5Y magnesium alloy prepared with ultrasonic treatment. Rare Met. 2017;36(8):622.CrossRef
[3]
Zurück zum Zitat Wang Y, Choo H. Influence of texture on Hall–Petch relationships in an Mg alloy. Acta Mater. 2014;81:83.CrossRef Wang Y, Choo H. Influence of texture on Hall–Petch relationships in an Mg alloy. Acta Mater. 2014;81:83.CrossRef
[4]
Zurück zum Zitat Li X, Li ZL, Duan BY, Li YM, Xu YL. Microstructure and texture of dimensional asymmetric spray deposited magnesium alloy containing Gd by extruding-rolling. Rare Met. 2018;37(10):1024. Li X, Li ZL, Duan BY, Li YM, Xu YL. Microstructure and texture of dimensional asymmetric spray deposited magnesium alloy containing Gd by extruding-rolling. Rare Met. 2018;37(10):1024.
[5]
Zurück zum Zitat Yang CW. Effect of friction stir processing on the microstructural evolution and tensile behaviors of an α/β dual-phase Mg–Li–Al–Zn alloy. Mater Trans. 2014;55(2):371.CrossRef Yang CW. Effect of friction stir processing on the microstructural evolution and tensile behaviors of an α/β dual-phase Mg–Li–Al–Zn alloy. Mater Trans. 2014;55(2):371.CrossRef
[6]
Zurück zum Zitat Chen HC, Hung FY, Lui TS, Chen LH, Huang JW. Effects of friction stir process and stabilizing heat treatment on the tensile and punch-shear properties of Mg–9Li–2Al–1Zn magnesium alloy. Mater Trans. 2013;54(4):505.CrossRef Chen HC, Hung FY, Lui TS, Chen LH, Huang JW. Effects of friction stir process and stabilizing heat treatment on the tensile and punch-shear properties of Mg–9Li–2Al–1Zn magnesium alloy. Mater Trans. 2013;54(4):505.CrossRef
[7]
Zurück zum Zitat Wang J, Zhang Q, Qin JY. Structural transition region of liquid Mg–Li alloys. Comput Mater Sci. 2016;117:259.CrossRef Wang J, Zhang Q, Qin JY. Structural transition region of liquid Mg–Li alloys. Comput Mater Sci. 2016;117:259.CrossRef
[8]
Zurück zum Zitat Kim WJ, Hong SI, Kim YS, Min SH, Jeong HT, Lee JD. Texture development and its effect on mechanical properties of an AZ61 Mg alloy fabricated by equal channel angular pressing. Acta Mater. 2014;51(11):3293.CrossRef Kim WJ, Hong SI, Kim YS, Min SH, Jeong HT, Lee JD. Texture development and its effect on mechanical properties of an AZ61 Mg alloy fabricated by equal channel angular pressing. Acta Mater. 2014;51(11):3293.CrossRef
[9]
Zurück zum Zitat Lin JB, Ren WJ, Wang QD, Ma LF, Chen YJ. Influence of grain size and texture on the yield strength of Mg alloys processed by severe plastic deformation. Adv Mater Sci Eng. 2014;2014(1):1. Lin JB, Ren WJ, Wang QD, Ma LF, Chen YJ. Influence of grain size and texture on the yield strength of Mg alloys processed by severe plastic deformation. Adv Mater Sci Eng. 2014;2014(1):1.
[10]
Zurück zum Zitat Anne G, Ramesh MR, Nayaka HS, Arya SB. Investigation of microstructure and mechanical properties of Mg–Zn/Al multilayered composite developed by accumulative roll bonding. Perspect Sci. 2016;8(C):104.CrossRef Anne G, Ramesh MR, Nayaka HS, Arya SB. Investigation of microstructure and mechanical properties of Mg–Zn/Al multilayered composite developed by accumulative roll bonding. Perspect Sci. 2016;8(C):104.CrossRef
[11]
Zurück zum Zitat Srinivasarao B, Zhilyaev AP, Urrutia IG, Prado MTP. Stabilization of metastable phases in Mg–Li alloys by high-pressure torsion. Scr Mater. 2013;68(8):583.CrossRef Srinivasarao B, Zhilyaev AP, Urrutia IG, Prado MTP. Stabilization of metastable phases in Mg–Li alloys by high-pressure torsion. Scr Mater. 2013;68(8):583.CrossRef
[12]
Zurück zum Zitat Mishra RS, Ma ZY. Friction stir welding and processing. Mater Sci Eng R. 2005;50(1):1.CrossRef Mishra RS, Ma ZY. Friction stir welding and processing. Mater Sci Eng R. 2005;50(1):1.CrossRef
[13]
Zurück zum Zitat Khorrami MS, Kazeminezhad M, Miyashita Y, Kokabi AH. Improvement in the mechanical properties of Al/SiC nanocomposites fabricated by severe plastic deformation and friction stir processing. Int J Min Met Mater. 2017;24(3):297.CrossRef Khorrami MS, Kazeminezhad M, Miyashita Y, Kokabi AH. Improvement in the mechanical properties of Al/SiC nanocomposites fabricated by severe plastic deformation and friction stir processing. Int J Min Met Mater. 2017;24(3):297.CrossRef
[15]
Zurück zum Zitat Cartigueyen S, Mahadevan K. Influence of rotational speed on the formation of friction stir processed zone in pure copper at low-heat input conditions. J Manuf Process. 2015;18:124.CrossRef Cartigueyen S, Mahadevan K. Influence of rotational speed on the formation of friction stir processed zone in pure copper at low-heat input conditions. J Manuf Process. 2015;18:124.CrossRef
[16]
Zurück zum Zitat Xie GM, Cui HB, Luo ZA, Misra RDK, Wang GD. Microstructural evolution and mechanical properties of the stir zone during friction stir processing a lean duplex stainless steel. Mater Sci Eng A. 2017;704:311.CrossRef Xie GM, Cui HB, Luo ZA, Misra RDK, Wang GD. Microstructural evolution and mechanical properties of the stir zone during friction stir processing a lean duplex stainless steel. Mater Sci Eng A. 2017;704:311.CrossRef
[17]
Zurück zum Zitat Xue G, Zhang Z, Wang W, Hai MN, Jia SW, Wang KS. Superplasticity of fine-grained AZ31/magnesium alloy prepared by friction stir processing. Rare Met Mater Eng. 2016;45(7):1855. Xue G, Zhang Z, Wang W, Hai MN, Jia SW, Wang KS. Superplasticity of fine-grained AZ31/magnesium alloy prepared by friction stir processing. Rare Met Mater Eng. 2016;45(7):1855.
[18]
Zurück zum Zitat Valle JAD, Rey P, Gesto D, Verdera D, Jiménez JA, Ruano OA. Mechanical properties of ultra-fine grained AZ91 magnesium alloy processed by friction stir processing. Mater Sci Eng A. 2015;628(2):198.CrossRef Valle JAD, Rey P, Gesto D, Verdera D, Jiménez JA, Ruano OA. Mechanical properties of ultra-fine grained AZ91 magnesium alloy processed by friction stir processing. Mater Sci Eng A. 2015;628(2):198.CrossRef
[19]
Zurück zum Zitat Xu N, Bao YF. Enhanced mechanical properties of tungsten inert gas welded AZ31 magnesium alloy joint using two-pass friction stir processing with rapid cooling. Mater Sci Eng A. 2016;655:292.CrossRef Xu N, Bao YF. Enhanced mechanical properties of tungsten inert gas welded AZ31 magnesium alloy joint using two-pass friction stir processing with rapid cooling. Mater Sci Eng A. 2016;655:292.CrossRef
[20]
Zurück zum Zitat Yang Q, Feng AH, Xiao BL, Ma ZY. Influence of texture on superplastic behavior of friction stir processed ZK60 magnesium alloy. Mater Sci Eng A. 2012;556(9):671.CrossRef Yang Q, Feng AH, Xiao BL, Ma ZY. Influence of texture on superplastic behavior of friction stir processed ZK60 magnesium alloy. Mater Sci Eng A. 2012;556(9):671.CrossRef
[21]
Zurück zum Zitat Jamili AM, Hanzaki AZ, Abedi HR, Minárik P, Soltani R. The microstructure, texture, and room temperature mechanical properties of friction stir processed Mg–Y–Nd alloy. Mater Sci Eng A. 2017;690:244.CrossRef Jamili AM, Hanzaki AZ, Abedi HR, Minárik P, Soltani R. The microstructure, texture, and room temperature mechanical properties of friction stir processed Mg–Y–Nd alloy. Mater Sci Eng A. 2017;690:244.CrossRef
[22]
Zurück zum Zitat Yuan W, Mishra RS, Carlson B, Mishra RK, Verma R, Kubic R. Effect of texture on the mechanical behavior of ultrafine grained magnesium alloy. Scr Mater. 2011;64(6):580.CrossRef Yuan W, Mishra RS, Carlson B, Mishra RK, Verma R, Kubic R. Effect of texture on the mechanical behavior of ultrafine grained magnesium alloy. Scr Mater. 2011;64(6):580.CrossRef
[23]
Zurück zum Zitat Liu FC, Tan MJ, Liao J, Ma ZY, Meng Q, Nakata K. Microstructural evolution and superplastic behavior in friction stir processed Mg–Li–Al–Zn alloy. J Mater Sci. 2013;48(24):8539.CrossRef Liu FC, Tan MJ, Liao J, Ma ZY, Meng Q, Nakata K. Microstructural evolution and superplastic behavior in friction stir processed Mg–Li–Al–Zn alloy. J Mater Sci. 2013;48(24):8539.CrossRef
[24]
Zurück zum Zitat Wu SK, Li YH, Chien KT, Chien C, Yang CS. X-ray diffraction studies on cold-rolled/solid-solution treated α + β Mg–10.2Li–1.2Al–0.4Zn alloy. J Alloys Compd. 2013;563:234.CrossRef Wu SK, Li YH, Chien KT, Chien C, Yang CS. X-ray diffraction studies on cold-rolled/solid-solution treated α + β Mg–10.2Li–1.2Al–0.4Zn alloy. J Alloys Compd. 2013;563:234.CrossRef
[25]
Zurück zum Zitat Mironov S, Zhang Y, Sato YS, Kokawa H. Development of grain structure in β-phase field during friction stir welding of Ti–6Al–4V alloy. Scr Mater. 2008;59(1):27.CrossRef Mironov S, Zhang Y, Sato YS, Kokawa H. Development of grain structure in β-phase field during friction stir welding of Ti–6Al–4V alloy. Scr Mater. 2008;59(1):27.CrossRef
[26]
Zurück zum Zitat Yu ZZ, Choo H, Feng ZL, Vogel SC. Influence of thermo-mechanical parameters on texture and tensile behavior of friction stir processed Mg alloy. Scr Mater. 2010;63(11):1112.CrossRef Yu ZZ, Choo H, Feng ZL, Vogel SC. Influence of thermo-mechanical parameters on texture and tensile behavior of friction stir processed Mg alloy. Scr Mater. 2010;63(11):1112.CrossRef
[27]
Zurück zum Zitat Vargas M, Lathabai S, Uggowitzer PJ, Qi Y, Orlov D, Estrin Y. Microstructure, crystallographic texture and mechanical behaviour of friction stir processed Mg–Zn–Ca–Zr alloy ZKX50. Mater Sci Eng A. 2017;685:253.CrossRef Vargas M, Lathabai S, Uggowitzer PJ, Qi Y, Orlov D, Estrin Y. Microstructure, crystallographic texture and mechanical behaviour of friction stir processed Mg–Zn–Ca–Zr alloy ZKX50. Mater Sci Eng A. 2017;685:253.CrossRef
[28]
Zurück zum Zitat Wang YN, Chang CI, Lee CJ, Lin HK, Huang JC. Texture and weak grain size dependence in friction stir processed Mg–Al–Zn alloy. Scr Mater. 2006;55(7):637.CrossRef Wang YN, Chang CI, Lee CJ, Lin HK, Huang JC. Texture and weak grain size dependence in friction stir processed Mg–Al–Zn alloy. Scr Mater. 2006;55(7):637.CrossRef
[29]
Zurück zum Zitat Yuan W, Mishra RS, Carlson B, Verma R, Mishra RK. Material flow and microstructural evolution during friction stir spot welding of AZ31 magnesium alloy. Mater Sci Eng A. 2012;543(5):200.CrossRef Yuan W, Mishra RS, Carlson B, Verma R, Mishra RK. Material flow and microstructural evolution during friction stir spot welding of AZ31 magnesium alloy. Mater Sci Eng A. 2012;543(5):200.CrossRef
[30]
Zurück zum Zitat Srinivasu R, Rao AS, Reddy GM, Rao KS. Friction stir surfacing of cast A356 aluminium–silicon alloy with boron carbide and molybdenum disulphide powders. Def Technol. 2015;11(2):140.CrossRef Srinivasu R, Rao AS, Reddy GM, Rao KS. Friction stir surfacing of cast A356 aluminium–silicon alloy with boron carbide and molybdenum disulphide powders. Def Technol. 2015;11(2):140.CrossRef
[31]
Zurück zum Zitat Luo C, Li X, Song D, Zhou N, Li Y, Qi W. Microstructure evolution and mechanical properties of friction stir welded dissimilar joints of Mg–Zn–Gd and Mg–Al–Zn alloys. Mater Sci Eng A. 2016;664:103.CrossRef Luo C, Li X, Song D, Zhou N, Li Y, Qi W. Microstructure evolution and mechanical properties of friction stir welded dissimilar joints of Mg–Zn–Gd and Mg–Al–Zn alloys. Mater Sci Eng A. 2016;664:103.CrossRef
[32]
Zurück zum Zitat Zeng Y, Jiang B, Yang QR, Quan GF, He JJ, Jiang ZT, Pan FS. Effect of Li content on microstructure, texture and mechanical behaviors of the as-extruded Mg–Li sheets. Mater Sci Eng A. 2017;700:59.CrossRef Zeng Y, Jiang B, Yang QR, Quan GF, He JJ, Jiang ZT, Pan FS. Effect of Li content on microstructure, texture and mechanical behaviors of the as-extruded Mg–Li sheets. Mater Sci Eng A. 2017;700:59.CrossRef
[33]
Zurück zum Zitat Karami M, Mahmudi R. Work hardening behavior of the extruded and equal-channel angularly pressed Mg–Li–Zn alloys under tensile and shear deformation modes. Mater Sci Eng A. 2014;607:512.CrossRef Karami M, Mahmudi R. Work hardening behavior of the extruded and equal-channel angularly pressed Mg–Li–Zn alloys under tensile and shear deformation modes. Mater Sci Eng A. 2014;607:512.CrossRef
[34]
Zurück zum Zitat Kumar N, Mishra RS, Dahotre NB, Brennan RE, Doherty KJ, Cho KC. Effect of friction stir processing on microstructure and mechanical properties of laser-processed Mg–4Y–3Nd alloy. Mater Des. 2016;110:663.CrossRef Kumar N, Mishra RS, Dahotre NB, Brennan RE, Doherty KJ, Cho KC. Effect of friction stir processing on microstructure and mechanical properties of laser-processed Mg–4Y–3Nd alloy. Mater Des. 2016;110:663.CrossRef
[35]
Zurück zum Zitat Chao HY, Sun HF, Wang ED. Working hardening behaviors of severely cold deformed and fine-grained AZ31Mg alloys at room temperature. Trans Nonferrous Met Soc China. 2011;21:s235.CrossRef Chao HY, Sun HF, Wang ED. Working hardening behaviors of severely cold deformed and fine-grained AZ31Mg alloys at room temperature. Trans Nonferrous Met Soc China. 2011;21:s235.CrossRef
[36]
Zurück zum Zitat Xue P, Wang BB, Chen FF, Wang WG, Xiao BL, Ma ZY. Microstructure and mechanical properties of friction stir processed Cu with an ideal ultrafine-grained structure. Mater Charact. 2016;121:187.CrossRef Xue P, Wang BB, Chen FF, Wang WG, Xiao BL, Ma ZY. Microstructure and mechanical properties of friction stir processed Cu with an ideal ultrafine-grained structure. Mater Charact. 2016;121:187.CrossRef
[37]
Zurück zum Zitat Wu HJ, Wang TZ, Wu RZ, Hou LG, Zhang JH, Li XL, Zhang ML. Effects of annealing process on the interface of alternate α/β Mg–Li composite sheets prepared by accumulative roll bonding. J Mater Process Technol. 2018;254:265.CrossRef Wu HJ, Wang TZ, Wu RZ, Hou LG, Zhang JH, Li XL, Zhang ML. Effects of annealing process on the interface of alternate α/β Mg–Li composite sheets prepared by accumulative roll bonding. J Mater Process Technol. 2018;254:265.CrossRef
[38]
Zurück zum Zitat Liu T, Zhang W, Wu SD, Jiang CB, Li SX, Xu YB. Mechanical properties of a two-phase alloy Mg–8%Li–1%Al processed by equal channel angular pressing. Mater Sci Eng A. 2003;360(1–2):345.CrossRef Liu T, Zhang W, Wu SD, Jiang CB, Li SX, Xu YB. Mechanical properties of a two-phase alloy Mg–8%Li–1%Al processed by equal channel angular pressing. Mater Sci Eng A. 2003;360(1–2):345.CrossRef
[39]
Zurück zum Zitat Wei GB, Mahmoodkhani Y, Peng XD, Hadadzadeh A, Xu TC, Liu JW, Xie WD, Wells MA. Microstructure evolution and simulation study of a duplex Mg–Li alloy during double change channel angular pressing. Mater Des. 2016;90:266.CrossRef Wei GB, Mahmoodkhani Y, Peng XD, Hadadzadeh A, Xu TC, Liu JW, Xie WD, Wells MA. Microstructure evolution and simulation study of a duplex Mg–Li alloy during double change channel angular pressing. Mater Des. 2016;90:266.CrossRef
[40]
Zurück zum Zitat Dong HW, Wang LM, Liu K, Wang LD, Jiang B, Pan FS. Microstructure and deformation behaviors of two Mg–Li dual-phase alloys with an increasing tensile speed. Mater Des. 2016;90:157.CrossRef Dong HW, Wang LM, Liu K, Wang LD, Jiang B, Pan FS. Microstructure and deformation behaviors of two Mg–Li dual-phase alloys with an increasing tensile speed. Mater Des. 2016;90:157.CrossRef
Metadaten
Titel
Microstructure and mechanical properties of magnesium–lithium alloy prepared by friction stir processing
verfasst von
Qian-Ying Che
Kuai-She Wang
Wen Wang
Li-Ying Huang
Tian-Qi Li
Xiao-Peng Xi
Pai Peng
Ke Qiao
Publikationsdatum
04.03.2019
Verlag
Nonferrous Metals Society of China
Erschienen in
Rare Metals / Ausgabe 9/2021
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-019-01217-2

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