nach oben

Erschienen in:

2014 | OriginalPaper | Buchkapitel

Mechanical Properties of Biomaterials Determined by Nano-Indentation and Nano-Scratch Tests

verfasst von : A. Karimzadeh, M. R. Ayatollahi

Erschienen in: Nanomechanical Analysis of High Performance Materials

Verlag: Springer Netherlands

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

Nano-indentation and nano-scratch tests are appropriate methods for measuring the mechanical and tribological properties of bulk samples, thin films and coatings. Using nano-scale tests, numerous properties like modulus of elasticity, hardness, fracture toughness, elastic–plastic behavior and wear resistance can be obtained. Macro-scale tests are conventional methods for determining the mechanical properties of biomaterials, but they are often expensive and require rather large test samples. In this article, the mechanical and tribological properties of hand-mixed and vacuum-mixed bone cements and a dental nano-composite determined by using nano-indentation and nano-scratch tests will be described and discussed. It is shown that bone cement mixed using the vacuum mixing exhibits significantly improved mechanical and tribological properties compared with the hand-mixed bone cement. Moreover, it is demonstrated that thermocycling affect the mechanical properties of dental nano-composite considerably.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Vorheriges Kapitel Nanoindentation Applied to Closed-Cell Aluminium Foams

Nächstes Kapitel Nanomechanical Characterization of Brittle Rocks

Anstis GR, Chantikul P, Lawn BR, Marshall DB (1981) A critical evaluation of indentation techniques for measuring fracture toughness. I. Direct crack measurements. J Am Ceram Soc 64(9):533–538CrossRef

Ayatollahi MR, Karimzadeh A (2012) Determination of fracture toughness of bone cement by nano-indentation test. Int J Fract 175:193–198CrossRef

Bao YW, Wang W, Zhou YC (2004) Investigation of the relationship between elastic modulus and hardness based on depth-sensing indentation measurements. Acta Mater 52:5397CrossRef

Briscoe BJ, Evans PD, Pelillo E, Sinha SK (1996) Scratching maps for polymers. Wear 200:137CrossRef

Briscoe BJ, Sinha SK (2003) Scratch resistance and localised damage characteristics of polymer surfaces – a review. Materialwissenschaft und Werkstofftechnik 34(10–11):989–1002

Chudoba T, Richter F (2001) Investigation of creep behaviour under load during indentation experiments and its influence on hardness and modulus results. Surf Coat Technol 148:191CrossRef

Cook RF, Pharr GM (1990) Direct observation and analysis of indentation cracking in glasses and ceramics. J Am Ceram Soc 73(4):787–817CrossRef

Duncan JC (1999) Mechanical properties and testing of polymers. Kluwer Academic Publishers, Dordrecht, p 43 12CrossRef

Dunne NJ, Orr JF (2001) Influence of mixing techniques on the physical properties of acrylic bone cement. Biomaterials 22:1819CrossRef

Fett T (2002) Computation of the crack opening displacements for Vickers indentation cracks. Forschungszentrum Karlsruhe, Report FZKA 6757, Karlsruhe, Germany

Fett T, Njiwa ABK, Rodel J (2005) Crack opening displacements of Vickers indentation cracks. Eng Fract Mech 72(5):647–659CrossRef

Gale MS, Darvell BW (1999) Thermal cycling procedures for laboratory testing of dental restorations. J Dent 27:89–99

Hu Y, Shen L, Yang H, Wang M, Liu T, Liang T, Zhang J (2006) Nanoindentation studies on nylon 11/clay nanocomposites. Polym Test 25:492CrossRef

ISO-14577-1 (2002) Metallic materials: instrumented indentation test for hardness and materials parameters part 1: test method. Switzerland, Geneva

ISO-14577-4 (2007) Metallic materials: instrumented indentation test for hardness and materials parameters part 4-test method for metallic and non-metallic coatings. Switzerland, Geneva

Jee A, Lee M (2010) Comparative analysis on the nanoindentation of polymers using atomic force microscopy. Polym Test 29:95CrossRef

Karimzadeh A, Ayatollahi MR (2012) Investigation of mechanical and tribological properties of bone cement by nano-indentation and nano-scratch experiments. Polym Test 31:828–833CrossRef

Kruzic JJ, Ritchie RO (2003) Determining the toughness of ceramics from Vickers indentations using the crack-opening displacements: an experimental study. J Am Ceram Soc 86(8):1433–1436CrossRef

Kruzica JJ, Kimb DK, Koesterc KJ, Ritchiec RO (2009) Indentation techniques for evaluating the fracture toughness of biomaterials and hard tissues. J Mech Behav Biomed Mater 2:384–395CrossRef

Lawn BR, Evans AG, Marshall DB (1980) Elastic/plastic indentation damage in ceramics: the median/radial crack system. J Am Ceram Soc 63(910):574–581CrossRef

Lidgren L, Bodelind B, Moller J (1987) Bone cement improved by vacuum mixing and chilling. Acta Orthop Scand 57:27

Liu TX, Phang IY, Shen L, Chow SY, Zhang W-D (2004) Morphology and mechanical properties of multiwalled carbon nanotubes reinforced nylon-6 composites. Macromolecules 37:7214CrossRef

Montes-G GM, Draughn RA (1986) In vitro surface degradation of composites by water and thermal cycling. Dent Mater 2:193–197CrossRef

Munz D, Bubsey RT, Shannon J (1980) Fracture toughness determination of A12O3 using four-point-bend specimens with straight-through and chevron notches. J Am Ceram Soc 63(5–6):300–305CrossRef

Murphy BP, Prendergast PJ (1999) Measurement of non-linear microcrack accumulation rates in polymethylmethacrylate bone cement under cyclic loading. J Mater Sci 10:779

Ngan AHW, Wang HT, Tang B, Sze KY (2005) Correcting power-law viscoelastic effects in elastic modulus measurement using depth-sensing indentation. Int J Solid Struct 42:1831MATHCrossRef

Oliver WC, Pharr GM (2004) Measurement of hardness and elastic modulus by instrumented indentation: advances in understanding and refinements to methodology. J Mater Res 19:3–20CrossRef

Pharr GM (1998) Measurement of mechanical properties by ultra-low load indentation. Mater Sci Eng A253:151–159

Sinha SK, Song T, Wan X, Tong Y (2009) Scratch and normal hardness characteristics of polyamide 6/nano-clay composite. Wear 266:814–821CrossRef

Smeds S, Goertzen D, Ivarsson I (1997) Influence of temperature and vacuum mixing on bone cement properties. Clin Orthop Relat Res 334:326CrossRef

Sneddon LN (1965) The relation between load and penetration in the axisymmetric Boussinesq problem for a punch of arbitrary profile. Int J Eng Sci 3:47MathSciNetMATHCrossRef

Wang JS, Toksvig-Larsen S, Müller-Wille P, Franzén H (1996) Is there any difference between vacuum mixing systems in reducing bone cement porosity? J Biomed Mater Res Appl Biomater 33:115CrossRef

Williams JA (1996) Analytical models of scratch hardness. Tribol Int 29:675CrossRef

Titel: Mechanical Properties of Biomaterials Determined by Nano-Indentation and Nano-Scratch Tests
verfasst von: A. Karimzadeh
M. R. Ayatollahi
Verlag: Springer Netherlands
Buch: Nanomechanical Analysis of High Performance Materials
Print ISBN: 978-94-007-6918-2

Electronic ISBN: 978-94-007-6919-9

Copyright-Jahr: 2014
DOI: https://doi.org/10.1007/978-94-007-6919-9_10

Premium Partner

Marktübersichten

Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.

Zur Marktübersicht