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2014 | OriginalPaper | Buchkapitel

Nanomechanical Characterization of Brittle Rocks

verfasst von : Annalisa Bandini, Paolo Berry, Edoardo Bemporad, Marco Sebastiani

Erschienen in: Nanomechanical Analysis of High Performance Materials

Verlag: Springer Netherlands

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Abstract

After an introduction describing the indentation techniques traditionally applied to the study of micromechanical properties of minerals and rocks, phenomena induced by the diamond tip’s penetration into crystalline rocks are analyzed. Crystalline rocks are characterized by low values of the critical breakage load, i.e. the threshold load corresponding to the transition from a ductile to a brittle behavior. As a consequence, it seems more convenient to examine the mechanical behavior of crystalline rocks by using instrumented nanoindentations. Above the critical load, ranging from rock to rock, fractures occur, affecting the indentation results and thus invalidating the values of the rock mechanical properties obtained by indentation data processing. In order to determine the correct values of the hardness and elastic modulus of brittle rocks, an innovative measurement modality for rocks, i.e. Continuous Stiffness Measurement mode, is proposed. By providing the continuous evolution of the hardness and of the elastic modulus as a function of the indentation depth, it has proven particularly suited to analyze the effects of induced fracturing on the load versus displacement curve.

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Literatur
Zurück zum Zitat Bandini A, Berry P (2013) Influence of marble's texture on its mechanical behavior. Rock Mech Rock Eng 46(4):785–799CrossRef Bandini A, Berry P (2013) Influence of marble's texture on its mechanical behavior. Rock Mech Rock Eng 46(4):785–799CrossRef
Zurück zum Zitat Bandini A, Berry P, Bemporad E, Sebastiani M (2012) Effects of intra-crystalline microcracks on the mechanical behavior of a marble under indentation. Int J Rock Mech Min Sci 54:47–55CrossRef Bandini A, Berry P, Bemporad E, Sebastiani M (2012) Effects of intra-crystalline microcracks on the mechanical behavior of a marble under indentation. Int J Rock Mech Min Sci 54:47–55CrossRef
Zurück zum Zitat Berry P, Bonifazi G, Fabbri S, Pinzari M (1989) Technological problems in cutting granite. In: MMIJ/IMM (ed) Proceedings of MMIJ/IMM joint symposium: today’s technology for the mining and metallurgical industries, Kyoto, 2–4 October 1989, pp 215–227 Berry P, Bonifazi G, Fabbri S, Pinzari M (1989) Technological problems in cutting granite. In: MMIJ/IMM (ed) Proceedings of MMIJ/IMM joint symposium: today’s technology for the mining and metallurgical industries, Kyoto, 2–4 October 1989, pp 215–227
Zurück zum Zitat Beste U, Lundvall A, Jacobson S (2004) Micro-scratch evaluation of rock types-a means to comprehend rock drill wear. Tribol Int 37(2):203–210CrossRef Beste U, Lundvall A, Jacobson S (2004) Micro-scratch evaluation of rock types-a means to comprehend rock drill wear. Tribol Int 37(2):203–210CrossRef
Zurück zum Zitat Blair SC, Cook NGW (1998) Analysis of compressive fracture in rock using statistical techniques: Part II. Effect of microscale heterogeneity on macroscopic deformation. Int J Rock Mech Min Sci 35(7):849–861CrossRef Blair SC, Cook NGW (1998) Analysis of compressive fracture in rock using statistical techniques: Part II. Effect of microscale heterogeneity on macroscopic deformation. Int J Rock Mech Min Sci 35(7):849–861CrossRef
Zurück zum Zitat Brace WF (1961) Dependence of fracture strength of rocks on grain size. In: Proceedings 4th symposium on rock mechanics, Pennsylvania State University, pp. 99–103 Brace WF (1961) Dependence of fracture strength of rocks on grain size. In: Proceedings 4th symposium on rock mechanics, Pennsylvania State University, pp. 99–103
Zurück zum Zitat Broz ME, Cook RF, Whitney DL (2006) Microhardness toughness, and modulus of Mohs scale minerals. Am Mineral 91:135–142CrossRef Broz ME, Cook RF, Whitney DL (2006) Microhardness toughness, and modulus of Mohs scale minerals. Am Mineral 91:135–142CrossRef
Zurück zum Zitat Carter GM, Henshall JL, Wakeman RJ (1993) Knoop hardness and fracture anisotropy of calcite. J Mater Sci Lett 12:407–410CrossRef Carter GM, Henshall JL, Wakeman RJ (1993) Knoop hardness and fracture anisotropy of calcite. J Mater Sci Lett 12:407–410CrossRef
Zurück zum Zitat Das B (1974) Vicker’s hardness concept in the light of Vicker’s impression. Int J Rock Mech Min Sci Geom Abstr 11:85–89CrossRef Das B (1974) Vicker’s hardness concept in the light of Vicker’s impression. Int J Rock Mech Min Sci Geom Abstr 11:85–89CrossRef
Zurück zum Zitat Delgado NS, Rodríguez-Rey A, Suárez del Río LM, Díez Sarriá I, Calleja L, Ruiz de Argandona VG (2005) The influence of rock microhardness on the sawability of Pink Porrino granite (Spain). Int J Rock Mech Min Sci 42:161–166 Delgado NS, Rodríguez-Rey A, Suárez del Río LM, Díez Sarriá I, Calleja L, Ruiz de Argandona VG (2005) The influence of rock microhardness on the sawability of Pink Porrino granite (Spain). Int J Rock Mech Min Sci 42:161–166
Zurück zum Zitat Hughes HM (1986) The relative cuttability of coal-measures stone. Min Sci Technol 3:95–109CrossRef Hughes HM (1986) The relative cuttability of coal-measures stone. Min Sci Technol 3:95–109CrossRef
Zurück zum Zitat Jian S-R (2007) Mechanical deformation induced in Si and GaN under Berkovich nanoindentation. Nanoscale Res Lett 3:6–13MathSciNetCrossRef Jian S-R (2007) Mechanical deformation induced in Si and GaN under Berkovich nanoindentation. Nanoscale Res Lett 3:6–13MathSciNetCrossRef
Zurück zum Zitat Kranz RL (1979) Crack growth and development during creep of Barre granite. Int J Rock Mech Min Sci 18:23–35MathSciNet Kranz RL (1979) Crack growth and development during creep of Barre granite. Int J Rock Mech Min Sci 18:23–35MathSciNet
Zurück zum Zitat Kranz RL (1983) Microcracks in rocks: a review. Tectonophysics 100:449–480CrossRef Kranz RL (1983) Microcracks in rocks: a review. Tectonophysics 100:449–480CrossRef
Zurück zum Zitat Lindqvist PA, Hai-Hui L (1983) Behaviour of the crushed zone in rock indentation. Rock Mech Rock Eng 16:199–207CrossRef Lindqvist PA, Hai-Hui L (1983) Behaviour of the crushed zone in rock indentation. Rock Mech Rock Eng 16:199–207CrossRef
Zurück zum Zitat Lan H, Martin CD, Hu B (2010) Effect of heterogeneity of brittle rock on micromechanical extensile behavior during compression loading. J Geophys Res 115:B01202CrossRef Lan H, Martin CD, Hu B (2010) Effect of heterogeneity of brittle rock on micromechanical extensile behavior during compression loading. J Geophys Res 115:B01202CrossRef
Zurück zum Zitat Lundberg B (1974) Penetration of rock by conical indenters. Int J Rock Mech Min Sci Geomech Abstr 11(6):209–214CrossRef Lundberg B (1974) Penetration of rock by conical indenters. Int J Rock Mech Min Sci Geomech Abstr 11(6):209–214CrossRef
Zurück zum Zitat Mahabadi OK, Randall NX, Zong Z, Grasselli G (2012) A novel approach for micro-scale characterization and modeling of geomaterials incorporating actual material heterogeneity. Geophys Res Lett 39:L01303CrossRef Mahabadi OK, Randall NX, Zong Z, Grasselli G (2012) A novel approach for micro-scale characterization and modeling of geomaterials incorporating actual material heterogeneity. Geophys Res Lett 39:L01303CrossRef
Zurück zum Zitat Oliver WC, Pharr GM (1992) An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J Mater Res 7:1564–1583CrossRef Oliver WC, Pharr GM (1992) An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J Mater Res 7:1564–1583CrossRef
Zurück zum Zitat Oliver WC, Pharr GM (2004) Measurement of hardness and elastic modulus by instrumented indentation: advances in understanding and refinements to methodology. J Mater Res 19:3–20CrossRef Oliver WC, Pharr GM (2004) Measurement of hardness and elastic modulus by instrumented indentation: advances in understanding and refinements to methodology. J Mater Res 19:3–20CrossRef
Zurück zum Zitat Pariseau WG, Fairhurst C (1967) The force-penetration characteristic for wedge penetration into rock. Int J Rock Mech Min Sci 4(2):165–180CrossRef Pariseau WG, Fairhurst C (1967) The force-penetration characteristic for wedge penetration into rock. Int J Rock Mech Min Sci 4(2):165–180CrossRef
Zurück zum Zitat Paul B, Sikarskie DL (1965) A preliminary theory of static penetration by a rigid wedge into a brittle material. Trans Soc Mining Eng 232:372–383 Paul B, Sikarskie DL (1965) A preliminary theory of static penetration by a rigid wedge into a brittle material. Trans Soc Mining Eng 232:372–383
Zurück zum Zitat Presser V, Gerlach K, Vohrer A, Nickel K, Dreher W (2010) Determination of the elastic modulus of highly porous samples by nanoindentation: a case study on sea urchin spines. J Mater Sci 45:2408–2418CrossRef Presser V, Gerlach K, Vohrer A, Nickel K, Dreher W (2010) Determination of the elastic modulus of highly porous samples by nanoindentation: a case study on sea urchin spines. J Mater Sci 45:2408–2418CrossRef
Zurück zum Zitat Saber-Samandari S, Gross KA (2009) Micromechanical properties of single crystal hydroxyapatite by nanoindentation. Acta Biomater 5:2206–2212CrossRef Saber-Samandari S, Gross KA (2009) Micromechanical properties of single crystal hydroxyapatite by nanoindentation. Acta Biomater 5:2206–2212CrossRef
Zurück zum Zitat Simmons G, Richter D (1976) Microcracks in rocks. In: Sterns RGJ (ed) The physics and chemistry of minerals and rocks. Wiley-Interscience, New York, pp 105–137 Simmons G, Richter D (1976) Microcracks in rocks. In: Sterns RGJ (ed) The physics and chemistry of minerals and rocks. Wiley-Interscience, New York, pp 105–137
Zurück zum Zitat Skrzypczak M, Guerret-Piecourt C, Bec S, Loubet JL, Guerret O (2009) Use of a nanoindentation fatigue test to characterize the ductile–brittle transition. J Eur Ceram Soc 29:1021–1028CrossRef Skrzypczak M, Guerret-Piecourt C, Bec S, Loubet JL, Guerret O (2009) Use of a nanoindentation fatigue test to characterize the ductile–brittle transition. J Eur Ceram Soc 29:1021–1028CrossRef
Zurück zum Zitat Sneddon IN (1965) The relation between load and penetration in the axisymmetric Boussinesq problem for a punch of arbitrary profile. Int J Eng Sci 3:47–57MathSciNetMATHCrossRef Sneddon IN (1965) The relation between load and penetration in the axisymmetric Boussinesq problem for a punch of arbitrary profile. Int J Eng Sci 3:47–57MathSciNetMATHCrossRef
Zurück zum Zitat Tapponnier P, Brace WF (1976) Development of stress-induced microcracks in Westerly Granite. Int J Rock Mech Min Sci Geomech Abstr 13(4):103–112CrossRef Tapponnier P, Brace WF (1976) Development of stress-induced microcracks in Westerly Granite. Int J Rock Mech Min Sci Geomech Abstr 13(4):103–112CrossRef
Zurück zum Zitat Tulliani JM, Bartuli C, Bemporad E, Naglieri V, Sebastiani M (2009) Preparation and mechanical characterization of dense and porous zirconia produced by gel casting with gelatin as a gelling agent. Ceram Int 6:2481–2491CrossRef Tulliani JM, Bartuli C, Bemporad E, Naglieri V, Sebastiani M (2009) Preparation and mechanical characterization of dense and porous zirconia produced by gel casting with gelatin as a gelling agent. Ceram Int 6:2481–2491CrossRef
Zurück zum Zitat Whitney DL, Broz M, Cook RF (2007) Hardness, toughness, and modulus of some common metamorphic minerals. Am Mineral 92:281–288CrossRef Whitney DL, Broz M, Cook RF (2007) Hardness, toughness, and modulus of some common metamorphic minerals. Am Mineral 92:281–288CrossRef
Zurück zum Zitat Wong TF (1982) Micromechanics of faulting in Westerly granite. Int J Rock Mech Min Sci 19:49–64 Wong TF (1982) Micromechanics of faulting in Westerly granite. Int J Rock Mech Min Sci 19:49–64
Zurück zum Zitat Wong TY, Bradt RC (1992) Microhardness anisotropy of single crystals of calcite, dolomite and magnesite on their cleavage planes. Mater Chem Phys 30:261–266CrossRef Wong TY, Bradt RC (1992) Microhardness anisotropy of single crystals of calcite, dolomite and magnesite on their cleavage planes. Mater Chem Phys 30:261–266CrossRef
Zurück zum Zitat Xie J, Tamaki J (2007) Parameterization of micro-hardness distribution in granite related to abrasive machining performance. J Mater Process Technol 186:253–258CrossRef Xie J, Tamaki J (2007) Parameterization of micro-hardness distribution in granite related to abrasive machining performance. J Mater Process Technol 186:253–258CrossRef
Zurück zum Zitat Yılmaz N (2011) Abrasivity assessment of granitic building stones in relation to diamond tool wear rate using mineralogy-based rock hardness indexes. Rock Mech Rock Eng 40:725–733CrossRef Yılmaz N (2011) Abrasivity assessment of granitic building stones in relation to diamond tool wear rate using mineralogy-based rock hardness indexes. Rock Mech Rock Eng 40:725–733CrossRef
Zurück zum Zitat Zhu W, Hughes JJ, Bicanic N, Pearce CJ (2007) Nanoindentation mapping of mechanical properties of cement paste and natural rocks. Mater Charact 58:1189–1198CrossRef Zhu W, Hughes JJ, Bicanic N, Pearce CJ (2007) Nanoindentation mapping of mechanical properties of cement paste and natural rocks. Mater Charact 58:1189–1198CrossRef
Metadaten
Titel
Nanomechanical Characterization of Brittle Rocks
verfasst von
Annalisa Bandini
Paolo Berry
Edoardo Bemporad
Marco Sebastiani
Copyright-Jahr
2014
Verlag
Springer Netherlands
DOI
https://doi.org/10.1007/978-94-007-6919-9_11

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