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2014 | OriginalPaper | Buchkapitel

Mechanical Property Mapping at the Nanoscale Using PeakForce QNM Scanning Probe Technique

verfasst von : Bede Pittenger, Natalia Erina, Chanmin Su

Erschienen in: Nanomechanical Analysis of High Performance Materials

Verlag: Springer Netherlands

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Abstract

Development of PeakForce QNM® a new, powerful scanning probe microscopy (SPM) method for high resolution, nanoscale quantitative mapping of mechanical properties is described. Material properties such as elastic modulus, dissipation, adhesion, and deformation are mapped simultaneously with topography at real imaging speeds with nanoscale resolution. PeakForce QNM has several distinct advantages over other SPM based methods for nanomechanical characterization including ease of use, unambiguous and quantitative material information, non-destructive to both tip and sample, and fast acquisition times. This chapter discusses the theory and operating principles of PeakForce QNM and applications to measure mechanical properties of a variety of materials ranging from polymer blends and films to single crystals and even cement paste.

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Literatur
Zurück zum Zitat Cleveland JP, Anczykowski B, Schmid AE, Elings VB (1998) Energy dissipation in tapping-mode atomic force microscopy. Appl Phys Lett 72(20):2613–2615CrossRef Cleveland JP, Anczykowski B, Schmid AE, Elings VB (1998) Energy dissipation in tapping-mode atomic force microscopy. Appl Phys Lett 72(20):2613–2615CrossRef
Zurück zum Zitat Dokukin ME, Sokolov I (2012) Quantitative mapping of the elastic modulus of soft materials with HarmoniX and PeakForce QNM AFM modes. Langmuir 28(46):16060–16071. doi:10.1021/la302706b CrossRef Dokukin ME, Sokolov I (2012) Quantitative mapping of the elastic modulus of soft materials with HarmoniX and PeakForce QNM AFM modes. Langmuir 28(46):16060–16071. doi:10.​1021/​la302706b CrossRef
Zurück zum Zitat Israelachvili N (1992) Intermolecular and surface forces Academic Press, New York Israelachvili N (1992) Intermolecular and surface forces Academic Press, New York
Zurück zum Zitat Legleiter J, Park M, Cusick B, Kowalewski T (2006) Scanning probe acceleration microscopy (SPAM) in fluids: Mapping mechanical properties of surfaces at the nanoscale. Proc Nat Acad Sci United States of Am 103(13):4813–4818. doi:10.1073/pnas.0505628103 Legleiter J, Park M, Cusick B, Kowalewski T (2006) Scanning probe acceleration microscopy (SPAM) in fluids: Mapping mechanical properties of surfaces at the nanoscale. Proc Nat Acad Sci United States of Am 103(13):4813–4818. doi:10.​1073/​pnas.​0505628103
Zurück zum Zitat Magonov S, Erina N (2005) Modern Trends in Atomic Force Microscopy of Polymers. Bruker application note AN84 Magonov S, Erina N (2005) Modern Trends in Atomic Force Microscopy of Polymers. Bruker application note AN84
Zurück zum Zitat Maugis D (2000) Contact, adhesion and rupture of elastic solids. Springer-Verlag, BerlinMATHCrossRef Maugis D (2000) Contact, adhesion and rupture of elastic solids. Springer-Verlag, BerlinMATHCrossRef
Zurück zum Zitat Pittenger B, Erina N, Su C (2010) Quantitative Mechanical Property Mapping at the Nanoscale with Peak Force QNM. Bruker application note AN128 Pittenger B, Erina N, Su C (2010) Quantitative Mechanical Property Mapping at the Nanoscale with Peak Force QNM. Bruker application note AN128
Zurück zum Zitat Proksch R (2006) Multifrequency, repulsive-mode amplitude-modulated atomic force microscopy. Appl Phys Lett 89(11):113121–113123CrossRef Proksch R (2006) Multifrequency, repulsive-mode amplitude-modulated atomic force microscopy. Appl Phys Lett 89(11):113121–113123CrossRef
Zurück zum Zitat Radmacher M, Cleveland JP, Fritz M, Hansma HG and Hansma PK (1994) Mapping interaction forces with the atomic force microscope. Biophys J 66:2159–2165 Radmacher M, Cleveland JP, Fritz M, Hansma HG and Hansma PK (1994) Mapping interaction forces with the atomic force microscope. Biophys J 66:2159–2165
Zurück zum Zitat Rode S, Oyabu N, Kobayashi K, Yamada H, Kühnle A (2009) True atomic-resolution Imaging of (1014) calcite in aqueous solution by frequency modulation atomic force microscopy. Langmuir 25(5):2850–2853. doi:10.1021/la803448v CrossRef Rode S, Oyabu N, Kobayashi K, Yamada H, Kühnle A (2009) True atomic-resolution Imaging of (1014) calcite in aqueous solution by frequency modulation atomic force microscopy. Langmuir 25(5):2850–2853. doi:10.​1021/​la803448v CrossRef
Zurück zum Zitat Rodriguez TR, Garcia R (2004) Compositional mapping of surfaces in atomic force microscopy by excitation of the second normal mode of the microcantilever. Appl Phys Lett 84(3):449–451CrossRef Rodriguez TR, Garcia R (2004) Compositional mapping of surfaces in atomic force microscopy by excitation of the second normal mode of the microcantilever. Appl Phys Lett 84(3):449–451CrossRef
Zurück zum Zitat Rosa-Zeiser A, Weilandt E, Hild S, Marti O (1997) The simultaneous measurement of elastic, electrostatic and adhesive properties by scanning force microscopy: pulsed-force mode operation. Meas Sci Technol 8(11):1333CrossRef Rosa-Zeiser A, Weilandt E, Hild S, Marti O (1997) The simultaneous measurement of elastic, electrostatic and adhesive properties by scanning force microscopy: pulsed-force mode operation. Meas Sci Technol 8(11):1333CrossRef
Zurück zum Zitat Sahin O (2005) Harmonic force microscope: a new tool for biomolecular identification and material characterization based on nanomechanical Measurements. Stanford University Sahin O (2005) Harmonic force microscope: a new tool for biomolecular identification and material characterization based on nanomechanical Measurements. Stanford University
Zurück zum Zitat Sahin O (2007) Harnessing bifurcations in tapping-mode atomic force microscopy to calibrate time-varying tip-sample force measurements. Rev Sci Instrum 78(10):103707–103704CrossRef Sahin O (2007) Harnessing bifurcations in tapping-mode atomic force microscopy to calibrate time-varying tip-sample force measurements. Rev Sci Instrum 78(10):103707–103704CrossRef
Zurück zum Zitat Sahin O, Magonov S, Su C, Quate CF, Solgaard O (2007) An atomic force microscope tip designed to measure time-varying nanomechanical forces. Nat Nanotechnol 2(8):507–514CrossRef Sahin O, Magonov S, Su C, Quate CF, Solgaard O (2007) An atomic force microscope tip designed to measure time-varying nanomechanical forces. Nat Nanotechnol 2(8):507–514CrossRef
Zurück zum Zitat Stark M, Stark RW, Heckl WM, Guckenberger R (2002) Inverting dynamic force microscopy: From signals to time-resolved interaction forces. Proc Nat Acad Sci 99(13):8473–8478. doi:10.1073/pnas.122040599 Stark M, Stark RW, Heckl WM, Guckenberger R (2002) Inverting dynamic force microscopy: From signals to time-resolved interaction forces. Proc Nat Acad Sci 99(13):8473–8478. doi:10.​1073/​pnas.​122040599
Zurück zum Zitat Tamayo J, Garcia R (1997) Effects of elastic and inelastic interactions on phase contrast images in tapping-mode scanning force microscopy. Appl Phys Lett 71(16):2394–2396CrossRef Tamayo J, Garcia R (1997) Effects of elastic and inelastic interactions on phase contrast images in tapping-mode scanning force microscopy. Appl Phys Lett 71(16):2394–2396CrossRef
Zurück zum Zitat Veeco (2010) Quantitative mechanical property mapping at the nanoscale with PeakForce QNM Veeco (2010) Quantitative mechanical property mapping at the nanoscale with PeakForce QNM
Zurück zum Zitat Young TJ, Monclus MA, Burnett TL, Broughton WR, Ogin SL, Smith PA (2011) The use of the PeakForce TM quantitative nanomechanical mapping AFM-based method for high-resolution Young’s modulus measurement of polymers. Meas Sci Technol 22(12):125703CrossRef Young TJ, Monclus MA, Burnett TL, Broughton WR, Ogin SL, Smith PA (2011) The use of the PeakForce TM quantitative nanomechanical mapping AFM-based method for high-resolution Young’s modulus measurement of polymers. Meas Sci Technol 22(12):125703CrossRef
Metadaten
Titel
Mechanical Property Mapping at the Nanoscale Using PeakForce QNM Scanning Probe Technique
verfasst von
Bede Pittenger
Natalia Erina
Chanmin Su
Copyright-Jahr
2014
Verlag
Springer Netherlands
DOI
https://doi.org/10.1007/978-94-007-6919-9_2

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