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Journal of Materials Science: Materials in Electronics
Erschienen in: Journal of Materials Science: Materials in Electronics 19/2020

17.08.2020

Optical properties of CdS nanocrystalline thin films in the abrupt phase transition from zinc blende to wurtzite

verfasst von: C. G. Torres-Castanedo, J. Márquez-Marín, R. Castanedo-Pérez, G. Torres-Delgado, M. A. Aguilar-Frutis, S. Arias-Cerón, O. Zelaya-Ángel

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 19/2020

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Abstract

A set of cadmium sulfide (CdS) thin films was grown on glass substrates by the chemical bath deposition technique at different bath temperatures (Tb). A microwave oven was used to heat the precursor aqueous solution employed to prepare the films in the 60–97 °C interval. The average crystallite size of the CdS films lies in the 7–20 nm range, calculated from X-ray diffraction data. The diffraction patterns reveal that the crystalline structure of CdS nanoparticles is cubic zinc blende (ZB) for 60 ≤ Tb ≤ 93 °C, hexagonal wurtzite (WZ) for 95 ≤ Tb ≤ 97 °C, and ZB-WZ mix of phases for the critical temperature Tb ≅ 94 °C (Tbc). The mixture of both phases is supported by Transmission Electron Microscopy. The CdS films show preferred orientation along (111) and (002) directions for ZB and WZ, respectively. The optical properties reveal significant changes at Tbc, namely, the energy band gap, photoluminescence emission, and refractive index. The photoluminescence results show an additional band at the critical phase transition temperature due to the presence of a high-density Cd interstitial/vacancies, produced by the mix of phases. Furthermore, high-energy transitions above the conduction band also exhibit splitting due to the phase transition.
Vorheriger Artikel Effect of Cu2+ doping on the structural, optical, and vapor-sensing properties of ZnO thin films prepared by SILAR method
Nächster Artikel Enhanced thermoelectric performance of Ca3Co4O9 doped with aluminum

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Metadaten
Titel
Optical properties of CdS nanocrystalline thin films in the abrupt phase transition from zinc blende to wurtzite
verfasst von
C. G. Torres-Castanedo
J. Márquez-Marín
R. Castanedo-Pérez
G. Torres-Delgado
M. A. Aguilar-Frutis
S. Arias-Cerón
O. Zelaya-Ángel
Publikationsdatum
17.08.2020
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 19/2020
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-020-04211-y

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