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Metallurgical and Materials Transactions A
Erschienen in: Metallurgical and Materials Transactions A 6/2020

19.03.2020

Preparation of Pulse Electrodeposited Ni-B Coating with RSM Software and Evaluation of Its Microhardness and Electrochemical Behavior

verfasst von: Somayeh Ahmadiyeh, Ali Rasooli, Mir Ghasem Hosseini

Erschienen in: Metallurgical and Materials Transactions A | Ausgabe 6/2020

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Abstract

In this study, the electrodeposition parameters were optimized to attain Ni-B alloy coatings with high hardness and corrosion resistance. The optimum plating parameters of the Ni-B coatings to get desirable properties (high microhardness and corrosion resistance) were determined by the response surface method (RSM) software. The effects of the boron concentration, average current density and duty cycle on the hardness of the deposited coatings were evaluated by the Vickers microhardness (HV) tester. The electrochemical behavior of the deposits was studied by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization (Tafel) methods. According to the results, raising the boron content and current density and decreasing the duty cycle led to increased microhardness (from 707 to 1116 HV) and improved corrosion resistance. Great corrosion resistance of 44 kΩ/cm2 with a low corrosion current density of 0.121 µA/cm2 was achieved at a boron concentration of 11 g/l, current density of 50 mA/cm2 and duty cycle of 20 pct.
Vorheriger Artikel Unusual Iron Nitride Formation Upon Nitriding Fe-Si Alloy
Nächster Artikel Effects of Robotic Hammer Peening on Structural Properties of Ni-Based Single-Crystal Superalloy: Dislocation Slip Traces and Crystallographic Reorientations

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Metadaten
Titel
Preparation of Pulse Electrodeposited Ni-B Coating with RSM Software and Evaluation of Its Microhardness and Electrochemical Behavior
verfasst von
Somayeh Ahmadiyeh
Ali Rasooli
Mir Ghasem Hosseini
Publikationsdatum
19.03.2020
Verlag
Springer US
Erschienen in
Metallurgical and Materials Transactions A / Ausgabe 6/2020
Print ISSN: 1073-5623
Elektronische ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-020-05718-z

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