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Colloid and Polymer Science
Erschienen in: Colloid and Polymer Science 9/2018

20.07.2018 | Original Contribution

Preparation of stable, transparent superhydrophobic film via one step one pot sol-gel method

verfasst von: Ayse Senem Kaya Topcu, Edanur Erdogan, Ugur Cengiz

Erschienen in: Colloid and Polymer Science | Ausgabe 9/2018

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Abstract

Herein, we report a single step and a one pot by using spin coating method for the preparation of optically transparent superhydrophobic TEOS-silica composite films. Silica sols were prepared by keeping the molar ratio of TEOS/CH3OH/H2O (0.1 M NH4F) constant at 1:33.15:6.06, respectively. Increasing the silica content of the coating solution resulted in decreasing the transparency of the composite films from 93 to 84% (in references to 93% transmission defined by a plain glass substrate). The static water and hexadecane contact angle of transparent surfaces were found to vary between 65° and 170° (sliding angle < 3°) and 45° to 5° (sliding angle = 15°) depending on the silica content. The stability of the surface remained nearly constant for several months under stored at ambient conditions. The mechanical stability of the prepared of TEOS-silica composite was tested by scratching and adhesive tape test. For the chemical test applications, NaOH, HCl, and H2SO4 were used for the TEOS-silica composite films.
Vorheriger Artikel Time-dependent behavior in analyte-, temperature-, and shear-sensitive Pluronic PE9400/water systems
Nächster Artikel Synthesis of mesoporous silica spheres utilizing in tandem with POSS-based block copolymer and anion surfactant as dual-template

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Metadaten
Titel
Preparation of stable, transparent superhydrophobic film via one step one pot sol-gel method
verfasst von
Ayse Senem Kaya Topcu
Edanur Erdogan
Ugur Cengiz
Publikationsdatum
20.07.2018
Verlag
Springer Berlin Heidelberg
Erschienen in
Colloid and Polymer Science / Ausgabe 9/2018
Print ISSN: 0303-402X
Elektronische ISSN: 1435-1536
DOI
https://doi.org/10.1007/s00396-018-4377-9

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