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Journal of Sol-Gel Science and Technology

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20.05.2022 | Invited Paper: Functional coatings, thin films and membranes (including deposition techniques)

Preparation of transparent and mechanically hard inorganic-organic hybrid thick films from 3-glycidoxypropyltrimethoxysilane and zirconium propoxide

verfasst von: Takuto Toide, Nataly Carolina Rosero-Navarro, Akira Miura, Hiromitsu Kozuka, Kiyoharu Tadanaga

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 3/2022

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Abstract

In order to lower the heating temperature, inorganic-organic hybrid films prepared by a sol-gel process are attractive candidates for glaze. Here, we prepared the inorganic-organic hybrid thick films on glass substrates by the sol-gel process at 100 °C. The precursor sol was prepared by hydrolysis and condensation of 3-glycidoxypropyltrimethoxysilane (GPTMS) and zirconium propoxide chemically modified with acetylacetone. The obtained GPTMS-ZrO₂-based thick films had a transmittance higher than 80% in the visible light of 390–800 nm. Thick films with a pencil hardness of 5H and a thickness of more than 100 µm were obtained.

Vorheriger Artikel Preparation of polyacrylamide-silica organic-inorganic hybrid membranes for carbon dioxide separation via in-situ polymerization

Nächster Artikel Correction to: Preparation of transparent and mechanically hard inorganic-organic hybrid thick films from 3-glycidoxypropyltrimethoxysilane and zirconium propoxide

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Titel: Preparation of transparent and mechanically hard inorganic-organic hybrid thick films from 3-glycidoxypropyltrimethoxysilane and zirconium propoxide
verfasst von: Takuto Toide
Nataly Carolina Rosero-Navarro
Akira Miura
Hiromitsu Kozuka
Kiyoharu Tadanaga
Publikationsdatum: 20.05.2022
Verlag: Springer US
Erschienen in: Journal of Sol-Gel Science and Technology / Ausgabe 3/2022
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI: https://doi.org/10.1007/s10971-022-05836-7

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