nach oben

Journal of Materials Science: Materials in Electronics

Erschienen in:

09.04.2016

Raman investigation of rutile-phased TiO₂ nanorods/nanoflowers with various reaction times using one step hydrothermal method

verfasst von: M. K. Ahmad, S. M. Mokhtar, C. F. Soon, N. Nafarizal, A. B. Suriani, A. Mohamed, M. H. Mamat, M. F. Malek, M. Shimomura, K. Murakami

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 8/2016

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config

KI-gestützte Suche

Aus

Abstract

Rutile-phased titanium dioxide nanorods (r-TNRs) and rutile-phased titanium dioxide nanoflowers (r-TNFs) were deposited on fluorine-doped tin oxide coated glass by using one step hydrothermal method at a fixed temperature of 150 °C. The hydrothermal treatment was conducted by varying the reaction time at 2, 3, 4, 5, 6, 7 and 8 h. The effect of reaction time on surface morphology, structure property, crystallite size and Raman spectra was investigated. The nanostructure samples were analysed using X-ray diffractometer, field emission-scanning electron microscope, micro-Raman spectroscopy, and energy-dispersive X-ray spectroscopy. The resulting micro-Raman spectra show abnormal behaviour of Raman intensity. The micro-Raman spectra of the nanostructure samples exhibit insignificant changes and shifting of Raman bands with increasing reaction time. This behaviour can be attributed to the shape and surface morphology distribution of r-TNRs/r-TNFs.

Vorheriger Artikel A single precursor route to synthesize CuO and CuS nanostructures based on copper ammine and thiourea complexes

Nächster Artikel Ferroelectric and flexible barrier resistive switching of epitaxial BiFeO3 films studied by temperature-dependent current and capacitance spectroscopy

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

Jetzt informieren

Springer Professional "Wirtschaft"

Online-Abonnement

Mit Springer Professional "Wirtschaft" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 340 Zeitschriften

aus folgenden Fachgebieten:

Bauwesen + Immobilien
Business IT + Informatik
Finance + Banking
Management + Führung
Marketing + Vertrieb
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Jetzt informieren

I. Lukačević, S.K. Gupta, P.K. Jha, D. Kirin, Lattice dynamics and Raman spectrum of rutile TiO₂: the role of soft phonon modes in pressure induced phase transition. Mater. Chem. Phys. 137(1), 282–289 (2012)CrossRef

Y. Wang, L. Zhang, K. Deng, X. Chen, Z. Zou, Low temperature synthesis and photocatalytic activity of rutile TiO₂ nanorod superstructures. J. Phys. Chem. C 111, 2709–2714 (2007)CrossRef

Y. Ohno, K. Tomita, Y. Komatsubara, T. Taniguchi, K. Katsumata et al., Pseudo-cube shaped brookite (TiO₂) nanocrystals synthesized by an oleate-modified hydrothermal growth method. Cryst. Growth Des. 11(11), 4831–4836 (2015)CrossRef

M. Landmann, E. Rauls, W.G. Schmidt, The electronic structure and optical response of rutile, anatase and brookite TiO₂. J. Phys.: Condens. Matter 24(19), 195503 (2012)

A.L. Linsebigler, A.L. Linsebigler, J.T. Yates Jr, G. Lu, G. Lu, J.T. Yates, Photocatalysis on TiO₂ surfaces: principles, mechanisms, and selected results. Chem. Rev. 95(3), 735–758 (1995)CrossRef

J. Xiong, B. Yang, J. Yuan, L. Fan, X. Hu, H. Xie, L. Lyu, R. Cui, Y. Zou, C. Zhou, D. Niu, Y. Gao, J. Yang, Efficient organic photovoltaics using solution-processed, annealing-free TiO₂ nanocrystalline particles as an interface modification layer. Org. Electron. 17, 253–261 (2015)CrossRef

M. Okuya, K. Shiozaki, N. Horikawa, T. Kosugi, G.R.A. Kumara, J.Á. Madarász, S. Kaneko, G. Pokol, Porous TiO₂ thin films prepared by spray pyrolysis deposition (SPD) technique and their application to UV sensors. Solid State Ionics 172(1–4), 527–531 (2004)CrossRef

Abdul Qader Dawood Faisal, Synthesis and characteristic study of TiO₂ nanowires and nanoflowers on FTO/glass and glass substrates via hydrothermal method. J. Mater. Sci.: Mater. Electron. 26, 317–321 (2015)

H. Yang, S. Zhu, N. Pan, Studying the mechanisms of titanium dioxide as ultraviolet-blocking additive for films and fabrics by an improved scheme. J. Appl. Polym. Sci. 92(5), 3201–3210 (2004)CrossRef

10.

B. Grzmil, B. Kic, M. Rabe, Inhibition of the anatase—rutile phase transformation with K₂O, P₂O₅, Li₂O. Chem. Pap. 58, 410–414 (2004)

11.

M.C. Mathpal, A.K. Tripathi, M.K. Singh, S.P. Gairola, S.N. Pandey, A. Agarwal, Effect of annealing temperature on Raman spectra of TiO2 nanoparticles. Chem. Phys. Lett. 555, 182–186 (2013)CrossRef

12.

E.V.A. Premalal, N. Dematage, S. Kaneko, A. Konno, Preparation of high quality spray-deposited fluorine-doped tin oxide thin films using dilute di(n-butyl)tin(iv) diacetate precursor solutions. Thin Solid Films 520(22), 6813–6817 (2012)CrossRef

13.

L. Kernazhitsky, V. Shymanovska, T. Gavrilko, V. Naumov, L. Fedorenko, V. Kshnyakin, J. Baran, Room temperature photoluminescence of anatase and rutile TiO₂ powders. J. Lumin. 146, 199–204 (2014)CrossRef

14.

H.L. Ma, J.Y. Yang, Y. Dai, Y.B. Zhang, B. Lu, G.H. Ma, Raman study of phase transformation of TiO₂ rutile single crystal irradiated by infrared femtosecond laser. Appl. Surf. Sci. 253(18), 7497–7500 (2007)CrossRef

15.

P. Liu, W. Cai, M. Fang, Z. Li, H. Zeng, J. Hu, X. Luo, W. Jing, Room temperature synthesized rutile TiO(2) nanoparticles induced by laser ablation in liquid and their photocatalytic activity. Nanotechnology 20(28), 285707 (2009)CrossRef

16.

H.W. Kim, H.S. Kim, H.G. Na, J.C. Yang, D.Y. Kim, Growth, structural, Raman, and photoluminescence properties of rutile TiO₂ nanowires synthesized by the simple thermal treatment. J. Alloys Compd. 504(1), 217–223 (2010)CrossRef

17.

S.S. Mali, C.A. Betty, P.N. Bhosale, R.S. Devan, Y.-R. Ma, S.S. Kolekar, P.S. Patil, Hydrothermal synthesis of rutile TiO₂ nanoflowers using brønsted acidic ionic liquid [BAIL]: synthesis, characterization and growth mechanism. CrystEngComm 14(6), 1920 (2012)CrossRef

18.

S. Sugapriya, R. Sriram, S. Lakshmi, Effect of annealing on TiO₂ nanoparticles. Optik 124(21), 4971–4975 (2013)CrossRef

19.

M. Gotić, M. Ivanda, S. Popović, S. Musić, A. Sekulić, A. Turković, K. Furić, Raman investigation of nanosized TiO₂. J. Raman Spectrosc. 28(7), 555–558 (1997)CrossRef

20.

X. Xue, W. Ji, Z. Mao, H. Mao, Y. Wang, X. Wang, W. Ruan, B. Zhao, J.R. Lombardi, Raman investigation of nanosized TiO₂: effect of crystallite size and quantum confinement. J. Phys. Chem. C 116(15), 8792–8797 (2012)CrossRef

21.

S.Y.D.J.R. Balaji, Phonon confinement studies in nanocrystalline anatase–TiO₂ thin films by micro Raman spectroscopy. J. Raman Spectrosc. 37, 1416–1422 (2006)CrossRef

Titel: Raman investigation of rutile-phased TiO2 nanorods/nanoflowers with various reaction times using one step hydrothermal method
verfasst von: M. K. Ahmad
S. M. Mokhtar
C. F. Soon
N. Nafarizal
A. B. Suriani
A. Mohamed
M. H. Mamat
M. F. Malek
M. Shimomura
K. Murakami
Publikationsdatum: 09.04.2016
Verlag: Springer US
Erschienen in: Journal of Materials Science: Materials in Electronics / Ausgabe 8/2016
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI: https://doi.org/10.1007/s10854-016-4783-z

Springer Professional

Abstract

Bitte loggen Sie sich ein, um Zugang zu Ihrer Lizenz zu erhalten.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Springer Professional "Technik"

Springer Professional "Wirtschaft"

Weitere Artikel der Ausgabe 8/2016

Conductivity and dielectric properties of PEDOT-PSS doped DMSO nano composite thin films

Solid state synthesis and tunable luminescence of LaNbTiO6:Eu3+

Low-temperature fired thermal-stable Li2TiO3–NiO microwave dielectric ceramics

Transparent conductive ZnO thin films grown by chemical spray pyrolysis: the effect of Mg

Fabrication and improved photocatalytic activity of n-ZnO nanorod arrays/p-CuO thin film heterojunction

Enhancements of microwave absorbing properties of weakly absorbing materials based on auxiliary absorption of SiC for microwave heating