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Erschienen in: Rare Metals 11/2016

01.11.2016

Rare earth texture analysis of rectangular extruded Mg alloys and a comparison of different alloying adding ways

verfasst von: Xiu-Li Hou, Yi-Xuan Zhai, Peng Zhang, Shun Guo, Zhi-Zhong Yuan, Qing-Feng Guan

Erschienen in: Rare Metals | Ausgabe 11/2016

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Abstract

The microstructures and textures of four rectangular extruded Mg alloys, Mg–3Gd, Mg–3Nd, Mg–1Gd–1Nd and Mg–1.5Gd–1.5Nd (all in wt%) were investigated by using optical microscopy (OM), X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). The results demonstrate that the extruded alloys all reveal fully recrystallized microstructure and weak non-basal texture. For textures of the four extruded alloys, it is shown that the basal planes of majority grains tilt away from the sheet plane normal toward the extrusion direction. Compared with two binary alloys, the ternary alloys possess weaker texture strengths. Through orientation distribution function analysis, two types of rare earth textures, {01\(\bar{1}\)3} <0\(\bar{2}\)23> and {\(\bar{1}\)2\(\bar{1}\)5} <1\(\bar{2}\)13>, were found in the extruded alloys. Texture component {\(\bar{1}\)2\(\bar{1}\)5} <1\(\bar{2}\)13> is relatively weak, but it plays a critical role in the low texture intensities of two ternary alloys. A pairing effect of Gd and Nd elements has an influence on the texture modification. Additionally, there is a difference in the sensitivities of experimental parameters between the microstructure and texture.

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Literatur
[1]
Zurück zum Zitat Yang Y, Zhang K, Li XG, Li YJ, Ma ML, Shi GL, Yuan JW. Microstructure and phase transformation of as-cast and annealed Mg–4Zn–1Y alloy containing quasi-crystal phase. Rare Met. 2015;34(4):239.CrossRef Yang Y, Zhang K, Li XG, Li YJ, Ma ML, Shi GL, Yuan JW. Microstructure and phase transformation of as-cast and annealed Mg–4Zn–1Y alloy containing quasi-crystal phase. Rare Met. 2015;34(4):239.CrossRef
[2]
Zurück zum Zitat Zeng ZR, Zhu YM, Xu SW, Bian MZ, Davies CHJ, Birbilis N, Nie JF. Texture evolution during static recrystallization of cold-rolled magnesium alloys. Acta Mater. 2016;105(1):479.CrossRef Zeng ZR, Zhu YM, Xu SW, Bian MZ, Davies CHJ, Birbilis N, Nie JF. Texture evolution during static recrystallization of cold-rolled magnesium alloys. Acta Mater. 2016;105(1):479.CrossRef
[3]
Zurück zum Zitat Stanford N, Barnett MR. The origin of “rare earth” texture development in extruded Mg-based alloys and its effect on tensile ductility. Mater Sci Eng, A. 2008;496(1):399.CrossRef Stanford N, Barnett MR. The origin of “rare earth” texture development in extruded Mg-based alloys and its effect on tensile ductility. Mater Sci Eng, A. 2008;496(1):399.CrossRef
[4]
Zurück zum Zitat Stanford N, Barnett MR. Effect of composition on the texture and deformation behaviour of wrought Mg alloys. Scr Mater. 2008;58(3):179.CrossRef Stanford N, Barnett MR. Effect of composition on the texture and deformation behaviour of wrought Mg alloys. Scr Mater. 2008;58(3):179.CrossRef
[5]
Zurück zum Zitat Stanford N. Micro-alloying Mg with Y, Ce, Gd and La for texture modification—a comparative study. Mater Sci Eng, A. 2010;527(10–11):2669.CrossRef Stanford N. Micro-alloying Mg with Y, Ce, Gd and La for texture modification—a comparative study. Mater Sci Eng, A. 2010;527(10–11):2669.CrossRef
[6]
Zurück zum Zitat Lentz M, Nissen J, Fahrenson C, Vogel SC, Reimers W. Macro- and microtexture evolution of an extruded Mg–Mn–Ce alloy during annealing. Mater Sci Eng, A. 2016;655(1):17.CrossRef Lentz M, Nissen J, Fahrenson C, Vogel SC, Reimers W. Macro- and microtexture evolution of an extruded Mg–Mn–Ce alloy during annealing. Mater Sci Eng, A. 2016;655(1):17.CrossRef
[7]
Zurück zum Zitat Jung IH, Sanjari M, Kim J, Yue S. Role of RE in the deformation and recrystallization of Mg alloy and a new alloy design concept for Mg–RE alloys. Scr Mater. 2015;102(1):1.CrossRef Jung IH, Sanjari M, Kim J, Yue S. Role of RE in the deformation and recrystallization of Mg alloy and a new alloy design concept for Mg–RE alloys. Scr Mater. 2015;102(1):1.CrossRef
[8]
Zurück zum Zitat Al-Samman T, Li X. Sheet texture modification in magnesium-based alloys by selective rare earth alloying. Mater Sci Eng, A. 2011;528(10–11):3809.CrossRef Al-Samman T, Li X. Sheet texture modification in magnesium-based alloys by selective rare earth alloying. Mater Sci Eng, A. 2011;528(10–11):3809.CrossRef
[9]
Zurück zum Zitat Hantzsche K, Bohlen J, Wendt J, Kainer KU, Yi SB, Letzig D. Effect of rare earth additions on microstructure and texture development of magnesium alloy sheets. Scr Mater. 2010;63(7):725.CrossRef Hantzsche K, Bohlen J, Wendt J, Kainer KU, Yi SB, Letzig D. Effect of rare earth additions on microstructure and texture development of magnesium alloy sheets. Scr Mater. 2010;63(7):725.CrossRef
[10]
Zurück zum Zitat Mackenzie LWF, Pekguleryuz MO. The recrystallization and texture of magnesium–zinc–cerium alloys. Scr Mater. 2008;59(6):665.CrossRef Mackenzie LWF, Pekguleryuz MO. The recrystallization and texture of magnesium–zinc–cerium alloys. Scr Mater. 2008;59(6):665.CrossRef
[11]
Zurück zum Zitat Ball EA, Prangnell PB. Tensile-compressive yield asymmetries in high strength wrought magnesium alloys. Scr Metall Mater. 1994;31(2):111.CrossRef Ball EA, Prangnell PB. Tensile-compressive yield asymmetries in high strength wrought magnesium alloys. Scr Metall Mater. 1994;31(2):111.CrossRef
[12]
Zurück zum Zitat Mackenzie LWF, Davis B, Humphreys FJ, Lorimer GW. The deformation, recrystallization and texture of three magnesium alloy extrusions. Mater Sci Technol. 2007;23(23):1173.CrossRef Mackenzie LWF, Davis B, Humphreys FJ, Lorimer GW. The deformation, recrystallization and texture of three magnesium alloy extrusions. Mater Sci Technol. 2007;23(23):1173.CrossRef
[13]
Zurück zum Zitat Laser T, Hartig C, Nürnberg MR, Letzig D, Bormann R. The influence of calcium and cerium mischmetal on the microstructural evolution of Mg–3Al–1Zn during extrusion and resulting mechanical properties. Acta Mater. 2008;56(12):2791.CrossRef Laser T, Hartig C, Nürnberg MR, Letzig D, Bormann R. The influence of calcium and cerium mischmetal on the microstructural evolution of Mg–3Al–1Zn during extrusion and resulting mechanical properties. Acta Mater. 2008;56(12):2791.CrossRef
[14]
Zurück zum Zitat Bohlen J, Nurnberg MR, Senn JW, Letzig D, Agnew SR. The texture and anisotropy of magnesium–zinc–rare earth alloy sheets. Acta Mater. 2007;55(6):2101.CrossRef Bohlen J, Nurnberg MR, Senn JW, Letzig D, Agnew SR. The texture and anisotropy of magnesium–zinc–rare earth alloy sheets. Acta Mater. 2007;55(6):2101.CrossRef
[15]
Zurück zum Zitat Basu I, Al-Samman T, Gottstein G. Shear band-related recrystallization and grain growth in two rolled magnesium-rare earth alloys. Mater Sci Eng, A. 2013;579(9):50.CrossRef Basu I, Al-Samman T, Gottstein G. Shear band-related recrystallization and grain growth in two rolled magnesium-rare earth alloys. Mater Sci Eng, A. 2013;579(9):50.CrossRef
[16]
Zurück zum Zitat Basu I, Al-Samman T. Triggering rare earth texture modification in magnesium alloys by addition of zinc and zirconium. Acta Mater. 2014;67(2):116.CrossRef Basu I, Al-Samman T. Triggering rare earth texture modification in magnesium alloys by addition of zinc and zirconium. Acta Mater. 2014;67(2):116.CrossRef
[17]
Zurück zum Zitat Sanjari M, Farzadfar A, Kabir ASH, Utsunomiya H, Jung IH, Petrov R, Kestens L, Yue S. Promotion of texture weakening in magnesium by alloying and thermomechanical processing: (I) alloying. J Mater Sci. 2014;49(3):1408.CrossRef Sanjari M, Farzadfar A, Kabir ASH, Utsunomiya H, Jung IH, Petrov R, Kestens L, Yue S. Promotion of texture weakening in magnesium by alloying and thermomechanical processing: (I) alloying. J Mater Sci. 2014;49(3):1408.CrossRef
[18]
Zurück zum Zitat Stanford N, Callaghan MD, Jong BD. The effect of rare earth elements on the behaviour of magnesium-based alloys: part 1—hot deformation behavior. Mater Sci Eng, A. 2013;565(1):459.CrossRef Stanford N, Callaghan MD, Jong BD. The effect of rare earth elements on the behaviour of magnesium-based alloys: part 1—hot deformation behavior. Mater Sci Eng, A. 2013;565(1):459.CrossRef
[19]
Zurück zum Zitat Pan SW, Xin YC, Huang GJ, Li Q, Guo FL, Liu Q. Tailoring the texture and mechanical anisotropy of a Mg–2Zn–2Gd plate by varying the rolling path. Mater Sci Eng, A. 2016;653(1):93.CrossRef Pan SW, Xin YC, Huang GJ, Li Q, Guo FL, Liu Q. Tailoring the texture and mechanical anisotropy of a Mg–2Zn–2Gd plate by varying the rolling path. Mater Sci Eng, A. 2016;653(1):93.CrossRef
[20]
Zurück zum Zitat Xu DK, Li CQ, Wang BJ, Han EH. Effect of icosahedral phase on the crystallographic texture and mechanical anisotropy of duplex structured Mg–Li alloys. Mater Des. 2015;88(1):88. Xu DK, Li CQ, Wang BJ, Han EH. Effect of icosahedral phase on the crystallographic texture and mechanical anisotropy of duplex structured Mg–Li alloys. Mater Des. 2015;88(1):88.
[21]
Zurück zum Zitat Ma Q, Li B, Whittington WR, Oppedal AL, Wang PT, Horstemeyer MF. Texture evolution during dynamic recrystallization in a magnesium alloy at 450°C. Acta Mater. 2014;67(1):102.CrossRef Ma Q, Li B, Whittington WR, Oppedal AL, Wang PT, Horstemeyer MF. Texture evolution during dynamic recrystallization in a magnesium alloy at 450°C. Acta Mater. 2014;67(1):102.CrossRef
[22]
Zurück zum Zitat Sarker D, Chen DL. Texture transformation in an extruded magnesium alloy under pressure. Mater Sci Eng, A. 2013;582(1):63.CrossRef Sarker D, Chen DL. Texture transformation in an extruded magnesium alloy under pressure. Mater Sci Eng, A. 2013;582(1):63.CrossRef
[23]
Zurück zum Zitat Yi SB, Brokmeier HG, Letzig D. Microstructural evolution during the annealing of an extruded AZ31 magnesium alloy. J Alloys Compd. 2010;506(1):364.CrossRef Yi SB, Brokmeier HG, Letzig D. Microstructural evolution during the annealing of an extruded AZ31 magnesium alloy. J Alloys Compd. 2010;506(1):364.CrossRef
[24]
Zurück zum Zitat Yi SB, Zaefferer S, Brokmeier HG. Mechanical behaviour and microstructural evolution of magnesium alloy AZ31 in tension at different temperatures. Mater Sci Eng, A. 2006;424(1–2):275.CrossRef Yi SB, Zaefferer S, Brokmeier HG. Mechanical behaviour and microstructural evolution of magnesium alloy AZ31 in tension at different temperatures. Mater Sci Eng, A. 2006;424(1–2):275.CrossRef
[25]
Zurück zum Zitat Stanford N, Atwell D, Beer A, Davies C, Barnett MR. Effect of microalloying with rare-earth elements on the texture of extruded magnesium-based alloys. Scr Mater. 2008;59(7):772.CrossRef Stanford N, Atwell D, Beer A, Davies C, Barnett MR. Effect of microalloying with rare-earth elements on the texture of extruded magnesium-based alloys. Scr Mater. 2008;59(7):772.CrossRef
[26]
Zurück zum Zitat Huppmann M, Gall S, Muller S, Reimers W. Changes of the texture and the mechanical properties of the extruded Mg alloy ME21 as a function of the process parameters. Mater Sci Eng, A. 2010;528(1):342.CrossRef Huppmann M, Gall S, Muller S, Reimers W. Changes of the texture and the mechanical properties of the extruded Mg alloy ME21 as a function of the process parameters. Mater Sci Eng, A. 2010;528(1):342.CrossRef
[27]
Zurück zum Zitat Stanford N. The effect of rare earth elements on the behaviour of magnesium-based alloys: part 2—recrystallisation and texture development. Mater Sci Eng, A. 2013;565(5):469.CrossRef Stanford N. The effect of rare earth elements on the behaviour of magnesium-based alloys: part 2—recrystallisation and texture development. Mater Sci Eng, A. 2013;565(5):469.CrossRef
[28]
Zurück zum Zitat Bohlen J, Yi S, Letzig D, Kainer KU. Effect of rare earth elements on the microstructure and texture development in magnesium–manganese alloys during extrusion. Mater Sci Eng, A. 2010;527(26):7092.CrossRef Bohlen J, Yi S, Letzig D, Kainer KU. Effect of rare earth elements on the microstructure and texture development in magnesium–manganese alloys during extrusion. Mater Sci Eng, A. 2010;527(26):7092.CrossRef
[29]
Zurück zum Zitat Cottam R, Robson J, Lorimer G, Davis B. Dynamic recrystallization of Mg and Mg–Y alloys: crystallographic texture development. Mater Sci Eng, A. 2008;485(1–2):375.CrossRef Cottam R, Robson J, Lorimer G, Davis B. Dynamic recrystallization of Mg and Mg–Y alloys: crystallographic texture development. Mater Sci Eng, A. 2008;485(1–2):375.CrossRef
[30]
Zurück zum Zitat Hadorn JP, Hantzsche K, Yi SB, Bohlen J, Letzig D, Wollmershauser JA, Agnew SR. Role of solute in the texture modification during hot deformation of Mg-rare earth alloys. Metall Mater Trans A. 2012;43(4):1347.CrossRef Hadorn JP, Hantzsche K, Yi SB, Bohlen J, Letzig D, Wollmershauser JA, Agnew SR. Role of solute in the texture modification during hot deformation of Mg-rare earth alloys. Metall Mater Trans A. 2012;43(4):1347.CrossRef
[31]
Zurück zum Zitat Hadorn JP, Hantzsche K, Yi SB, Bohlen J, Letzig D, Agnew SR. Effects of solute and second-phase particles on the texture of Nd-containing Mg alloys. Metall Mater Trans A. 2012;43(4):1363.CrossRef Hadorn JP, Hantzsche K, Yi SB, Bohlen J, Letzig D, Agnew SR. Effects of solute and second-phase particles on the texture of Nd-containing Mg alloys. Metall Mater Trans A. 2012;43(4):1363.CrossRef
[32]
Zurück zum Zitat Mayama T, Noda M, Chiba R, Kuroda M. Crystal plasticity analysis of texture development in magnesium alloy during extrusion. Int J Plast. 2011;27(12):1916.CrossRef Mayama T, Noda M, Chiba R, Kuroda M. Crystal plasticity analysis of texture development in magnesium alloy during extrusion. Int J Plast. 2011;27(12):1916.CrossRef
[33]
Zurück zum Zitat Hirsch J, Al-Samman T. Superior light metals by texture engineering: optimized aluminum and magnesium alloys for automotive applications. Acta Mater. 2013;61(3):818.CrossRef Hirsch J, Al-Samman T. Superior light metals by texture engineering: optimized aluminum and magnesium alloys for automotive applications. Acta Mater. 2013;61(3):818.CrossRef
[34]
Zurück zum Zitat Bozzolo N, Dewobroto N, Grosdidier T, Wagner F. Texture evolution during grain growth in recrystallized commercially pure titanium. Mater Sci Eng A. 2005;397(1–2):346.CrossRef Bozzolo N, Dewobroto N, Grosdidier T, Wagner F. Texture evolution during grain growth in recrystallized commercially pure titanium. Mater Sci Eng A. 2005;397(1–2):346.CrossRef
[35]
Zurück zum Zitat Molodov DA, Bozzolo N. Observations on the effect of a magnetic field on the annealing texture and microstructure evolution in zirconium. Acta Mater. 2010;58(10):3568.CrossRef Molodov DA, Bozzolo N. Observations on the effect of a magnetic field on the annealing texture and microstructure evolution in zirconium. Acta Mater. 2010;58(10):3568.CrossRef
[36]
Zurück zum Zitat Ma Q, Li B, Marin EB, Horstemeyer SJ. Twinning-induced dynamic recrystallization in a magnesium alloy extruded at 450°C. Scr Mater. 2011;65(9):823.CrossRef Ma Q, Li B, Marin EB, Horstemeyer SJ. Twinning-induced dynamic recrystallization in a magnesium alloy extruded at 450°C. Scr Mater. 2011;65(9):823.CrossRef
[37]
Zurück zum Zitat Stanford N, Sha G, Xia JH, Ringer SP, Barnett MR. Solute segregation and texture modification in an extruded magnesium alloy containing gadolinium. Scr Mater. 2011;65(10):919.CrossRef Stanford N, Sha G, Xia JH, Ringer SP, Barnett MR. Solute segregation and texture modification in an extruded magnesium alloy containing gadolinium. Scr Mater. 2011;65(10):919.CrossRef
Metadaten
Titel
Rare earth texture analysis of rectangular extruded Mg alloys and a comparison of different alloying adding ways
verfasst von
Xiu-Li Hou
Yi-Xuan Zhai
Peng Zhang
Shun Guo
Zhi-Zhong Yuan
Qing-Feng Guan
Publikationsdatum
01.11.2016
Verlag
Nonferrous Metals Society of China
Erschienen in
Rare Metals / Ausgabe 11/2016
Print ISSN: 1001-0521
Elektronische ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-016-0796-2

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