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Journal of Materials Engineering and Performance
Erschienen in: Journal of Materials Engineering and Performance 8/2022

03.03.2022 | Technical Article

Two-Step Sintering of TiO2-ZrO2-Y2O3 Nanocomposite Ceramics with Enhanced Mechanical Properties

verfasst von: Pan Luo, Jin Zhang, Feng Zhang, Kuo Ma, Junwei Xia, Wei Wang, Liping Nie

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 8/2022

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Abstract

Yttria-stabilized zirconia (YSZ, Y2O3-ZrO2) ceramic with titanium dioxide nanoparticle (nanoTiO2) is prepared using conventional pressureless and two-step sintering (TSS) methods. The microstructure, phase composition, and mechanical properties of TSS-TiO2-ZrO2-Y2O3 nanocomposite ceramics are compared to those of the ceramics sintered using conventional sintering. The effect of TSS and nanoparticles on the sintering densification of the YSZ ceramics is investigated. X-ray diffractometry revealed that nanoTiO2 destabilizes c-ZrO2 and stabilizes t-ZrO2 in the YSZ. In addition, TSS is more conducive for grain refinement and sintering densification of the TiO2-ZrO2-Y2O3 nanocomposite ceramics; the average grain size of the samples decreased from 1.446 (conventional sintering) to 0.492 μm (TSS). Meanwhile, the relative density and sintering shrinkage of the TSS-1450 sample reached the maximum (98.23% and 22.92%, respectively) at a nanoTiO2 fraction of 7 wt%. The maximum microhardness and bending strength of the TSS-1450 ceramic matrix with 7-wt% nanoTiO2 were 1823 HV and 505 MPa, respectively. The nanoparticles distributed in the grain boundary induce the crack to the matrix, which induces the transgranular fracture, and nanoTiO2 improves the densification and mechanical properties of YSZ ceramics more than titanium dioxide microparticles.
Vorheriger Artikel Stress Development During Cooling of Continuously Cast Boron-Containing Steel Slabs
Nächster Artikel Achieving Excellent Strength–Ductility Combination by Cyclic Quenching Treatment in 22MnB5 Steel

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Metadaten
Titel
Two-Step Sintering of TiO2-ZrO2-Y2O3 Nanocomposite Ceramics with Enhanced Mechanical Properties
verfasst von
Pan Luo
Jin Zhang
Feng Zhang
Kuo Ma
Junwei Xia
Wei Wang
Liping Nie
Publikationsdatum
03.03.2022
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 8/2022
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-022-06732-5

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