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Topics in Catalysis
Erschienen in: Topics in Catalysis 9-12/2024

16.10.2023 | Original Paper

Voltammetric Quantification of D-penicillamine by Using a Carbon Paste Electrode Modified with WO3 Nanorods and Ionic Liquid as an Efficient Electrochemical Sensing Platform

verfasst von: Somayeh Tajik, Peyman Mohammadzadeh Jahani

Erschienen in: Topics in Catalysis | Ausgabe 9-12/2024

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Abstract

In this work, the electrochemical behavior and sensitive voltammetric determination of D-penicillamine are described by using a carbon paste electrode modified with WO3 nanorods and ionic liquid. The as-synthesized WO3 nanorods were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, field emission scanning electron microscopy, and energy-dispersive X-ray spectroscopy. Cyclic voltammetric measurements showed that D-penicillamine was irreversibly oxidized at WO3 nanorods/ionic liquid/carbon paste electrode at 710 mV in pH 7.0 phosphate buffer solution. The peak current of D-penicillamine was increased approximately 6.2 fold at WO3 nanorods/ionic liquid/carbon paste electrode compared to unmodified carbon paste electrode due to a good electrocatalytic efficiency of WO3 nanorods and ionic liquid. A wide linear range response between oxidation peak current and D-penicillamine concentration (0.08–235.0 µM) was observed using differential pulse voltammetry. The limit of detection for D-penicillamine on WO3 nanorods/ionic liquid/carbon paste electrode is found to be 0.03 µM. Studies conducted in the analysis of D-penicillamine capsule and urine samples confirmed that the developed sensor exhibits good applicability for accurate and sensitive voltammetric determination of D-penicillamine in real samples.
Vorheriger Artikel Hydrogen Generation by Methanolysis of NaBH4 via Efficient CuFe2O4 Nanoparticle Catalyst: A Kinetic Study and DNN Model
Nächster Artikel Detection and Determination of Quercetin in Sour Cherry and Black Tea Samples by Fluorescent Probe Prepared by Green Hydrothermal Method Using Achillea Millefolium Extract

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Metadaten
Titel
Voltammetric Quantification of D-penicillamine by Using a Carbon Paste Electrode Modified with WO3 Nanorods and Ionic Liquid as an Efficient Electrochemical Sensing Platform
verfasst von
Somayeh Tajik
Peyman Mohammadzadeh Jahani
Publikationsdatum
16.10.2023
Verlag
Springer US
Erschienen in
Topics in Catalysis / Ausgabe 9-12/2024
Print ISSN: 1022-5528
Elektronische ISSN: 1572-9028
DOI
https://doi.org/10.1007/s11244-023-01874-9

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