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European Journal of Wood and Wood Products

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04.11.2023 | Original Article

Changes in chemical properties and microstructure of Pinus taeda and Eucalyptus bosistoana woods modified by contact charring

verfasst von: F. Diğdem Tuncer, S. Nami Kartal, Ekim Elçin Soytürk, Rachel A. Arango, Katie M. Ohno, M. Serdar Önses, Nusret Çelik, Claudia Marcela Ibanez

Erschienen in: European Journal of Wood and Wood Products | Ausgabe 1/2024

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Abstract

This study evaluated the effect of contact charring plus linseed oil submersion on wood chemistry and microstructure in Pinus taeda and Eucalyptus bosistoana wood specimens. Fourier-transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and Raman spectroscopy analyses were performed to characterize charred wood in comparison to uncharred controls. Total lignin content increased to nearly 53% and 55% in the outer surfaces of the charred P. taeda and E. bosistoana specimens, respectively. The inner parts of the charred specimens also demonstrated increases higher than 50% in total lignin content. Total carbohydrate content of charred wood specimens decreased after the carbonization process. In the charred P. taeda specimens, the highest reductions in carbohydrate units observed were arabinan, xylan, and mannan. In the charred E. bosistoana specimens, arabinan, galactan and xylan showed the highest reductions in carbohydrate units. After charring, all wood specimens exhibited elevated contact angles when compared to control specimens due to increased hydrophobicity. The FTIR spectra analyses also indicated polysaccharide depolymerization and the formation of furans and alkylated aromatic compounds in charred specimens. Oil submersion led to saturation of cell lumens in both wood species used in this study. Charring led to sensitivity and homogeneity in cell walls although cells and pits retained their structural integrity and shape. Additionally, crack formation and separation occurred along the cell wall in some tracheid and fiber cells.

Vorheriger Artikel Properties improvement of seven hardwood species by combination of thermal and chemical modifications

Nächster Artikel Gap-filling properties of adhesives used for cross-laminated timber

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Titel: Changes in chemical properties and microstructure of Pinus taeda and Eucalyptus bosistoana woods modified by contact charring
verfasst von: F. Diğdem Tuncer
S. Nami Kartal
Ekim Elçin Soytürk
Rachel A. Arango
Katie M. Ohno
M. Serdar Önses
Nusret Çelik
Claudia Marcela Ibanez
Publikationsdatum: 04.11.2023
Verlag: Springer Berlin Heidelberg
Erschienen in: European Journal of Wood and Wood Products / Ausgabe 1/2024
Print ISSN: 0018-3768
Elektronische ISSN: 1436-736X
DOI: https://doi.org/10.1007/s00107-023-02011-9

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