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Journal of Materials Engineering and Performance

Erschienen in:

19.01.2016

Corrosion Protection Properties of PPy-ND Composite Coating: Sonoelectrochemical Synthesis and Design of Experiment

verfasst von: H. Ashassi-Sorkhabi, R. Bagheri, B. Rezaei-Moghadam

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 2/2016

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Abstract

In this research, the nanocomposite coatings comprising the polypyrrole-nanodiamond, PPy-ND, on St-12 steel electrodes were electro-synthesized using in situ polymerization process under ultrasonic irradiation. The corrosion protection performance and morphology characterization of prepared coatings were investigated by electrochemical methods and scanning electron microscopy, SEM, respectively. Also, the experimental design was employed to determine the best values considering the effective parameters such as the concentration of nanoparticles, the applied current density and synthesis time to achieve the most protective films. A response surface methodology, RSM, involving a central composite design, CCD, was applied to the modeling and optimization of the PPy-ND nanocomposite deposition. Pareto graphic analysis of the parameters indicated that the applied current density and some of the interactions were effective on the response. The electrochemical results proved that the embedment of diamond nanoparticle, DNP, improves the corrosion resistance of PPy coatings significantly. Therefore, desirable correlation exists between predicted data and experimental results.

Vorheriger Artikel Modeling Corrosion Reactions of Steel in a Dilute Carbonate Solution

Nächster Artikel Effect of Intercritical Temperature on the Structure Property Correlation of Multiphase High-C Spheroidized Steel

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Titel: Corrosion Protection Properties of PPy-ND Composite Coating: Sonoelectrochemical Synthesis and Design of Experiment
verfasst von: H. Ashassi-Sorkhabi
R. Bagheri
B. Rezaei-Moghadam
Publikationsdatum: 19.01.2016
Verlag: Springer US
Erschienen in: Journal of Materials Engineering and Performance / Ausgabe 2/2016
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-016-1886-x

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