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The International Journal of Advanced Manufacturing Technology

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16.02.2024 | ORIGINAL ARTICLE

Effect of milling time on structural, physical and photocatalytical properties of Ti-Ni alloy for biomedical applications

verfasst von: Nabila Bouchareb, Mamoun Fellah, Naouel Hezil, Fouzia Hamadi, Alex Montagne, Obrosov Aleksei, Krishna Kumar Yadav, Gamal A. El-Hiti

Erschienen in: The International Journal of Advanced Manufacturing Technology | Ausgabe 7-8/2024

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Abstract

Ti-Ni shape memory alloys (SMA) are used extensively in the field of orthopedics owing to their unique physical and mechanical features, excellent corrosion resistance, and good biocompatibility in the human body environment. This study aims to investigate how milling time affects the characteristics of Ti-Ni alloys which were synthesized with equal atomic percentages by using a high-energy ball milling type (Planetary Micro Mill Pulverisette P7, Fritsch GmbH, Germany) under varying milling periods (2, 6, 12, and 18 h). The duration of the grinding process refines the grain and diminishes the material's porosity, improving the material's physical and structural characteristics as well as its photocatalytic activity. The milled powders of Ti₅₀-Ni₅₀ alloys underwent characterization employing scanning electron microscopy (SEM) associated with an energy dispersive spectrometer (EDS), X-ray diffraction (XRD), and spectrophotometery of visible and ultraviolet light (UV–VIS) to measure the solution absorbance of methylene blue (MB). The results revealed that the milling process influences the particle size and shape of powders, where the proportion of fine particles increased with increasing grinding times from 2 to 18 h due to severe deformation and fracturing. The crystallite size was reduced, and the microstrain increased, attaining values of 29 nm and 0.99%, respectively. In addition, the pores of samples were decreased to 10 nm at higher milling times. Furthermore, solutions of MB containing powders of Ti₅₀-Ni₅₀ milled at 18 h exhibited good photocatalytic activity with a degradation rate value of 93.23% after 60 min of irradiation time because of a greater surface area. The improved properties of Ti₅₀-Ni₅₀ alloys make them clinically useful for biomedical implantation in humans. Plus, they are considered to be effective materials for photocatalytic applications.

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Titel: Effect of milling time on structural, physical and photocatalytical properties of Ti-Ni alloy for biomedical applications
verfasst von: Nabila Bouchareb
Mamoun Fellah
Naouel Hezil
Fouzia Hamadi
Alex Montagne
Obrosov Aleksei
Krishna Kumar Yadav
Gamal A. El-Hiti
Publikationsdatum: 16.02.2024
Verlag: Springer London
Erschienen in: The International Journal of Advanced Manufacturing Technology / Ausgabe 7-8/2024
Print ISSN: 0268-3768
Elektronische ISSN: 1433-3015
DOI: https://doi.org/10.1007/s00170-024-13207-5

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