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Journal of Sol-Gel Science and Technology
Erschienen in: Journal of Sol-Gel Science and Technology 3/2022

05.05.2022 | Invited Paper: Nano-structured materials (particles, fibers, colloids, composites, etc.)

Hydrothermal synthesis of perovskite-type solid electrolyte nanoplate

verfasst von: Ken-ichi Mimura, Naoki Hamao, Hiroki Itasaka, Zheng Liu, Koichi Hamamoto

Erschienen in: Journal of Sol-Gel Science and Technology | Ausgabe 3/2022

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Abstract

Perovskite-type (A,La)TiO3 (A: Li or Na) nanoplates were synthesized by hydrothermal reaction using titanium bis(ammonium lactate) dihydroxide as a starting material at 260 °C for 48 h. When NaOH was used as a mineralizer, perovskite single phase was obtained, but when LiOH was used, impurities including lanthanum hydroxide were obtained, and no perovskite phase was obtained. Scanning transmission electron microscopy (STEM) analyses demonstrated that perovskite NPs have plate-like morphology with plane index of {100}. Energy dispersive X-ray spectroscopy (EDX) revealed that Na partly occupied in A-site of perovskite structure. The nanoplates were pressed into a pellet and sintered at 1000 °C. The pellet exhibited an ionic conductivity of 3.8 × 10−6 S/cm.
Vorheriger Artikel Superacid-catalyzed preparation of ionic polyhedral oligomeric silsesquioxanes and their properties, polymerization, and hybridization
Nächster Artikel Effects of the silicon-containing chemical species dissolved from chitosan–siloxane hybrids on nerve cells

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Metadaten
Titel
Hydrothermal synthesis of perovskite-type solid electrolyte nanoplate
verfasst von
Ken-ichi Mimura
Naoki Hamao
Hiroki Itasaka
Zheng Liu
Koichi Hamamoto
Publikationsdatum
05.05.2022
Verlag
Springer US
Erschienen in
Journal of Sol-Gel Science and Technology / Ausgabe 3/2022
Print ISSN: 0928-0707
Elektronische ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-022-05810-3

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Correction

Correction to: Preparation of transparent and mechanically hard inorganic-organic hybrid thick films from 3-glycidoxypropyltrimethoxysilane and zirconium propoxide

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