Skip to main content
Erschienen in: Journal of Materials Engineering and Performance 7/2018

17.05.2018

Multiphase Microstructure in a Metastability-Assisted Medium Carbon Alloy Steel

verfasst von: Cheng Liu, Xixi Cui, Chen Yang

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 7/2018

Einloggen

Aktivieren Sie unsere intelligente Suche, um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

A medium carbon alloy steel is processed by austenizing at 900 °C for 30 min, then rapid quenching into a patented quenching liquid and holding at 170 °C for 5 min, finally isothermally holding at 250 °C for different times. The morphology and mechanical properties are performed by using optical microscopy and scanning electron microscopy. A multiphase microstructure characterized by a mixture of lenticular prior martensite (PM), fine needle bainitic ferrite and filmy retained austenite (RA) is obtained. It is found that the PM formed firstly upon quenching can accelerate the subsequent bainitic transformation and promote refinement of multiphase colonies. The results show that an optimum mechanical property of a 4000.9 MPa bending strength and a 2030 MPa tensile strength is achieved at 250 °C for 120 min, which is attributed to the multiphase microstructural characteristics and a high product of the volume fraction of RA and the carbon content of austenite.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat F.G. Caballero, S. Allain, J.D. Puerta-Velásquez, and C. Garcia-Mateo, Exploring Carbide-Free Bainitic Structures for Hot Dip Galvanizing Products, ISIJ Int., 2013, 53, p 1253-1259CrossRef F.G. Caballero, S. Allain, J.D. Puerta-Velásquez, and C. Garcia-Mateo, Exploring Carbide-Free Bainitic Structures for Hot Dip Galvanizing Products, ISIJ Int., 2013, 53, p 1253-1259CrossRef
2.
Zurück zum Zitat D.T. Pierce, D.R. Coughlin, D.L. Williamson, K.D. Clarke, A.J. Clarke, J.G. Speer, and E. De Moor, Characterization of Transition Carbides in Quench and Partitioned Steel Microstructures by Mössbauer Spectroscopy and Complementary Techniques, Acta Mater., 2015, 90, p 417-430CrossRef D.T. Pierce, D.R. Coughlin, D.L. Williamson, K.D. Clarke, A.J. Clarke, J.G. Speer, and E. De Moor, Characterization of Transition Carbides in Quench and Partitioned Steel Microstructures by Mössbauer Spectroscopy and Complementary Techniques, Acta Mater., 2015, 90, p 417-430CrossRef
3.
Zurück zum Zitat Y. Chang, G.Z. Li, C.Y. Wang, X.D. Li, and H. Dong, Effect of Quenching and Partitioning with Hot Stamping on Martensite Transformation and Mechanical Properties of AHSS, J. Mater. Eng. Perform., 2015, 24, p 3194-3200CrossRef Y. Chang, G.Z. Li, C.Y. Wang, X.D. Li, and H. Dong, Effect of Quenching and Partitioning with Hot Stamping on Martensite Transformation and Mechanical Properties of AHSS, J. Mater. Eng. Perform., 2015, 24, p 3194-3200CrossRef
4.
Zurück zum Zitat N. Fonstein, Candidates for Third-Generation Steels: Q&P Processed Steels. In Advanced High Strength Sheet Steels: Physical Metallurgy, Design, Processing, and Properties, 1st edn (Springer International Publishing, 2015), chapter 10: p 327-368 N. Fonstein, Candidates for Third-Generation Steels: Q&P Processed Steels. In Advanced High Strength Sheet Steels: Physical Metallurgy, Design, Processing, and Properties, 1st edn (Springer International Publishing, 2015), chapter 10: p 327-368
5.
Zurück zum Zitat D.V. Edmonds, K. He, F.C. Rizzo, B.C. De Cooman, D.K. Matlock, and J.G. Speer, Quenching and Partitioning Martensite—A Novel Steel Heat Treatment, Mater. Sci. Eng. A, 2006, 438-440, p 25-34CrossRef D.V. Edmonds, K. He, F.C. Rizzo, B.C. De Cooman, D.K. Matlock, and J.G. Speer, Quenching and Partitioning Martensite—A Novel Steel Heat Treatment, Mater. Sci. Eng. A, 2006, 438-440, p 25-34CrossRef
6.
Zurück zum Zitat H. Wu, C. Liu, Z. Zhao, Y. Zhao, S. Zhu, Y. Liu, and S. Bhole, Design of Air-cooled Bainitic Microalloyed Steel for a Heavy Truck Front Axle Beam, Mater. Des., 2006, 27, p 651-656CrossRef H. Wu, C. Liu, Z. Zhao, Y. Zhao, S. Zhu, Y. Liu, and S. Bhole, Design of Air-cooled Bainitic Microalloyed Steel for a Heavy Truck Front Axle Beam, Mater. Des., 2006, 27, p 651-656CrossRef
7.
Zurück zum Zitat S. Samanta, S. Das, D. Chakrabarti, I. Samajdar, S.B. Singh, and A. Haldar, Development of Multiphase Microstructure with Bainite, Martensite, and Retained Austenite in a Co-Containing Steel Through Quenching and Partitioning (Q&P) Treatment, Metall. Mater. Trans. A, 2013, 44, p 5653-5664CrossRef S. Samanta, S. Das, D. Chakrabarti, I. Samajdar, S.B. Singh, and A. Haldar, Development of Multiphase Microstructure with Bainite, Martensite, and Retained Austenite in a Co-Containing Steel Through Quenching and Partitioning (Q&P) Treatment, Metall. Mater. Trans. A, 2013, 44, p 5653-5664CrossRef
8.
Zurück zum Zitat M. Koyama, Z. Zhang, M.M. Wang, D. Ponge, D. Raabe, K. Tsuzaki, H. Noguchi, and C.C. Tasan, Bone-like Crack Resistance in Hierarchical Metastable Nanolaminate Steels, Science, 2017, 355, p 1055-1057CrossRef M. Koyama, Z. Zhang, M.M. Wang, D. Ponge, D. Raabe, K. Tsuzaki, H. Noguchi, and C.C. Tasan, Bone-like Crack Resistance in Hierarchical Metastable Nanolaminate Steels, Science, 2017, 355, p 1055-1057CrossRef
9.
Zurück zum Zitat C. Yang, X.X. Cui, and C. Liu, Multiphase Matrix Structure of Unalloyed Austempered Ductile Iron, Mater. Sci. Technol., 2018, 34, p 261-267CrossRef C. Yang, X.X. Cui, and C. Liu, Multiphase Matrix Structure of Unalloyed Austempered Ductile Iron, Mater. Sci. Technol., 2018, 34, p 261-267CrossRef
10.
Zurück zum Zitat F. Tariq and R.A. Baloch, One-Step Quenching and Partitioning Heat Treatment of Medium Carbon Low Alloy Steel, J. Mater. Eng. Perform., 2014, 23, p 1726-1739CrossRef F. Tariq and R.A. Baloch, One-Step Quenching and Partitioning Heat Treatment of Medium Carbon Low Alloy Steel, J. Mater. Eng. Perform., 2014, 23, p 1726-1739CrossRef
11.
Zurück zum Zitat C. Liu, C. Yang, L.M. Yuan, and D.O. Northwood, Role of Pre-formed Martensite on Transformation of Austempered Ductile Iron, Mater. Sci. Technol., 2017, 33, p 1819-1828CrossRef C. Liu, C. Yang, L.M. Yuan, and D.O. Northwood, Role of Pre-formed Martensite on Transformation of Austempered Ductile Iron, Mater. Sci. Technol., 2017, 33, p 1819-1828CrossRef
12.
Zurück zum Zitat H. Amel-Farzad, H.R. Faridi, F. Rajabpour, A. Abolhasani, S. Kazemi, and Y. Khaledzadeh, Developing Very Hard Nanostructured Bainitic Steel, Mater. Sci. Eng. A, 2013, 559, p 68-73CrossRef H. Amel-Farzad, H.R. Faridi, F. Rajabpour, A. Abolhasani, S. Kazemi, and Y. Khaledzadeh, Developing Very Hard Nanostructured Bainitic Steel, Mater. Sci. Eng. A, 2013, 559, p 68-73CrossRef
13.
Zurück zum Zitat R.M. Wu, W. Li, S. Zhou, Y. Zhong, L. Wang, and X.J. Jin, Effect of Retained Austenite on the Fracture Toughness of Quenching and Partitioning (Q&P)-treated Sheet Steels, Metall. Mater. Trans. A, 2014, 45, p 1892-1902CrossRef R.M. Wu, W. Li, S. Zhou, Y. Zhong, L. Wang, and X.J. Jin, Effect of Retained Austenite on the Fracture Toughness of Quenching and Partitioning (Q&P)-treated Sheet Steels, Metall. Mater. Trans. A, 2014, 45, p 1892-1902CrossRef
14.
Zurück zum Zitat Y. Toji, H. Matsuda, and D. Raabe, Effect of Si on the Acceleration of Bainite Transformation by Pre-existing Martensite, Acta Mater., 2016, 116, p 250-262CrossRef Y. Toji, H. Matsuda, and D. Raabe, Effect of Si on the Acceleration of Bainite Transformation by Pre-existing Martensite, Acta Mater., 2016, 116, p 250-262CrossRef
15.
Zurück zum Zitat C.E. Ericsson, M.S. Bhat, E.R. Parker, and V.F. Zackay, Isothermal Studies of Bainitic and Martensitic Transformations in Some Low Alloy Steels, Metall. Trans. A, 1976, 7, p 1800-1803CrossRef C.E. Ericsson, M.S. Bhat, E.R. Parker, and V.F. Zackay, Isothermal Studies of Bainitic and Martensitic Transformations in Some Low Alloy Steels, Metall. Trans. A, 1976, 7, p 1800-1803CrossRef
16.
Zurück zum Zitat H. Kawata, K. Hayashi, N. Sugiura, N. Yoshinaga, and M. Takahashi, Effect of Martensite in Initial Structure on Bainite Transformation, Mater. Sci. Forum, 2010, 638, p 3307-3312CrossRef H. Kawata, K. Hayashi, N. Sugiura, N. Yoshinaga, and M. Takahashi, Effect of Martensite in Initial Structure on Bainite Transformation, Mater. Sci. Forum, 2010, 638, p 3307-3312CrossRef
17.
Zurück zum Zitat W. Gong, Y. Tomota, S. Harjo, Y.H. Su, and K. Aizawa, Effect of Prior Martensite on Bainite Transformation in Nanobainite Steel, Acta Mater., 2015, 85, p 243-249CrossRef W. Gong, Y. Tomota, S. Harjo, Y.H. Su, and K. Aizawa, Effect of Prior Martensite on Bainite Transformation in Nanobainite Steel, Acta Mater., 2015, 85, p 243-249CrossRef
18.
Zurück zum Zitat A. Navarro-López, J. Sietsma, and M.J. Santofimia, Effect of Prior Athermal Martensite on the Isothermal Transformation Kinetics Below Ms in a Low-C High-Si Steel, Metall. Mater. Trans. A, 2016, 47, p 1028-1039CrossRef A. Navarro-López, J. Sietsma, and M.J. Santofimia, Effect of Prior Athermal Martensite on the Isothermal Transformation Kinetics Below Ms in a Low-C High-Si Steel, Metall. Mater. Trans. A, 2016, 47, p 1028-1039CrossRef
19.
Zurück zum Zitat H. Santos, A. Duarte, and J. Seabra, Austempered Ductile Iron with Tempered Martensite, lnt. J. Cast Met. Res., 2002, 15, p 117-124CrossRef H. Santos, A. Duarte, and J. Seabra, Austempered Ductile Iron with Tempered Martensite, lnt. J. Cast Met. Res., 2002, 15, p 117-124CrossRef
20.
Zurück zum Zitat C.J. Martis, S.K. Putatunda, and J. Boileau, Processing of New High Strength High Toughness Steel with Duplex Microstructure (Ferrite + Austenite), Mater. Des., 2013, 46, p 168-174CrossRef C.J. Martis, S.K. Putatunda, and J. Boileau, Processing of New High Strength High Toughness Steel with Duplex Microstructure (Ferrite + Austenite), Mater. Des., 2013, 46, p 168-174CrossRef
21.
Zurück zum Zitat Y. Huang, X.L. Zhang, W.N. Liu, X.M. Wang, and J.K. Han, Microstructure and Mechanical Properties of NANOBAIN Steel, J. Iron. Steel Res. Int., 2016, 23, p 253-260CrossRef Y. Huang, X.L. Zhang, W.N. Liu, X.M. Wang, and J.K. Han, Microstructure and Mechanical Properties of NANOBAIN Steel, J. Iron. Steel Res. Int., 2016, 23, p 253-260CrossRef
22.
Zurück zum Zitat M.N. Yoozbashi and S. Yazdani, Mechanical Properties of Nanostructured, Low Temperature Bainitic Steel Designed Using a Thermodynamic Model, Mater. Sci. Eng. A, 2010, 527, p 3200-3205CrossRef M.N. Yoozbashi and S. Yazdani, Mechanical Properties of Nanostructured, Low Temperature Bainitic Steel Designed Using a Thermodynamic Model, Mater. Sci. Eng. A, 2010, 527, p 3200-3205CrossRef
23.
Zurück zum Zitat P. Luo, G. Gao, H. Zhang, Z. Tan, R.D.K. Misra, and B.Z. Bai, On Structure-property Relationship in Nanostructured Bainitic Steel Subjected to the quenching and partitioning process, Mater. Sci. Eng. A, 2016, 661, p 1-8CrossRef P. Luo, G. Gao, H. Zhang, Z. Tan, R.D.K. Misra, and B.Z. Bai, On Structure-property Relationship in Nanostructured Bainitic Steel Subjected to the quenching and partitioning process, Mater. Sci. Eng. A, 2016, 661, p 1-8CrossRef
24.
Zurück zum Zitat H. Wu, Y. Jiang, S.S. You, Y. Han, and Y.X. Liu, Study on TRIP Effect of Retained Austenite in Super-bainite Microstructure, J. Mech. Eng., 2014, 50, p 69-75 (in Chinese)CrossRef H. Wu, Y. Jiang, S.S. You, Y. Han, and Y.X. Liu, Study on TRIP Effect of Retained Austenite in Super-bainite Microstructure, J. Mech. Eng., 2014, 50, p 69-75 (in Chinese)CrossRef
25.
Zurück zum Zitat Y. Han, H. Wu, C. Liu, and Y.X. Liu, Medium Carbon Super-Bainitic Steel After Isothermal Transformation. J. Mater. Eng. Perform. 2014, 23, p 4230-4236CrossRef Y. Han, H. Wu, C. Liu, and Y.X. Liu, Medium Carbon Super-Bainitic Steel After Isothermal Transformation. J. Mater. Eng. Perform. 2014, 23, p 4230-4236CrossRef
26.
Zurück zum Zitat X. Zhang, G. Xu, X. Wang, D. Embury, O. Bouaziz, O. Bouaziz, G.R. Purdy, and H.S. Zurob, Mechanical Behavior of Carbide-free Medium Carbon Bainitic Steels, Metall. Mater. Trans. A, 2014, 45, p 1352-1361CrossRef X. Zhang, G. Xu, X. Wang, D. Embury, O. Bouaziz, O. Bouaziz, G.R. Purdy, and H.S. Zurob, Mechanical Behavior of Carbide-free Medium Carbon Bainitic Steels, Metall. Mater. Trans. A, 2014, 45, p 1352-1361CrossRef
27.
Zurück zum Zitat D.P. Koistinen and R.E. Marburger, A General Equation Prescribing the Extent of the Austenite-Martensite Transformation in Pure Iron-carbon Alloys and Plain Carbon Steels, Acta Metall., 1959, 7, p 59-60CrossRef D.P. Koistinen and R.E. Marburger, A General Equation Prescribing the Extent of the Austenite-Martensite Transformation in Pure Iron-carbon Alloys and Plain Carbon Steels, Acta Metall., 1959, 7, p 59-60CrossRef
28.
Zurück zum Zitat J. Mallia, M. Grech, and R.E. Smallman, Effect of Silicon Content on Transformation Kinetics of Austempered Ductile Iron, Mater. Sci. Technol., 1998, 14, p 452-460CrossRef J. Mallia, M. Grech, and R.E. Smallman, Effect of Silicon Content on Transformation Kinetics of Austempered Ductile Iron, Mater. Sci. Technol., 1998, 14, p 452-460CrossRef
29.
Zurück zum Zitat C. Yang, X.X. Cui, Z.B. Zhao, G. Hua, and C. Liu, Role of Bulky Retained Austenite in Austempered Ductile Iron, Adv. Mater. Res., 2016, 1142, p 19-22CrossRef C. Yang, X.X. Cui, Z.B. Zhao, G. Hua, and C. Liu, Role of Bulky Retained Austenite in Austempered Ductile Iron, Adv. Mater. Res., 2016, 1142, p 19-22CrossRef
30.
Zurück zum Zitat S.M.C. van Bohemen, Bainite and Martensite Start Temperature Calculated with Exponential Carbon Dependence, Mater. Sci. Technol., 2012, 28, p 487-495CrossRef S.M.C. van Bohemen, Bainite and Martensite Start Temperature Calculated with Exponential Carbon Dependence, Mater. Sci. Technol., 2012, 28, p 487-495CrossRef
31.
Zurück zum Zitat Y.F. Shen, L.N. Qiu, X. Sun, L. Zuo, P.K. Liaw, and D. Raabe, Effects of Retained Austenite Volume Fraction, Morphology, and Carbon Content on Strength and Ductility of Nanostructured TRIP-assisted Steels, Mater. Sci. Eng. A, 2015, 636, p 551-564CrossRef Y.F. Shen, L.N. Qiu, X. Sun, L. Zuo, P.K. Liaw, and D. Raabe, Effects of Retained Austenite Volume Fraction, Morphology, and Carbon Content on Strength and Ductility of Nanostructured TRIP-assisted Steels, Mater. Sci. Eng. A, 2015, 636, p 551-564CrossRef
32.
Zurück zum Zitat S.K. Putatunda and P.K. Gadicherla, Effect of Austempering Time on Mechanical Properties of a Low Manganese Austempered Ductile Iron, J. Mater. Eng. Perform., 2000, 9, p 193-203CrossRef S.K. Putatunda and P.K. Gadicherla, Effect of Austempering Time on Mechanical Properties of a Low Manganese Austempered Ductile Iron, J. Mater. Eng. Perform., 2000, 9, p 193-203CrossRef
33.
Zurück zum Zitat W.S. Li, H.Y. Gao, Z.Y. Li, H. Nakashima, S. Hata, and W.H. Tian, Effect of Lower Bainite/Martensite/Retained Austenite Triplex Microstructure on the Mechanical Properties of a Low-carbon Steel with Quenching and Partitioning Process, Int. J. Min. Met. Mater., 2016, 23, p 303CrossRef W.S. Li, H.Y. Gao, Z.Y. Li, H. Nakashima, S. Hata, and W.H. Tian, Effect of Lower Bainite/Martensite/Retained Austenite Triplex Microstructure on the Mechanical Properties of a Low-carbon Steel with Quenching and Partitioning Process, Int. J. Min. Met. Mater., 2016, 23, p 303CrossRef
34.
Zurück zum Zitat K. Abbaszadeh, H. Saghafian, and S. Kheirandish, Effect of Bainite Morphology on Mechanical Properties of the Mixed Bainite-martensite Microstructure in D6AC Steel, J. Mater. Sci. Technol., 2012, 28, p 336-342CrossRef K. Abbaszadeh, H. Saghafian, and S. Kheirandish, Effect of Bainite Morphology on Mechanical Properties of the Mixed Bainite-martensite Microstructure in D6AC Steel, J. Mater. Sci. Technol., 2012, 28, p 336-342CrossRef
35.
Zurück zum Zitat K.K. Wang, Z.L. Tan, G.H. Gao, and X.L. Gui, R.DK. Misra and B.Z. Bai, Ultrahigh Strength-toughness Combination in Bainitic Rail Steel: The Determining Role of Austenite Stability during Tempering, Mater. Sci. Eng. A, 2016, 662, p 162-168CrossRef K.K. Wang, Z.L. Tan, G.H. Gao, and X.L. Gui, R.DK. Misra and B.Z. Bai, Ultrahigh Strength-toughness Combination in Bainitic Rail Steel: The Determining Role of Austenite Stability during Tempering, Mater. Sci. Eng. A, 2016, 662, p 162-168CrossRef
Metadaten
Titel
Multiphase Microstructure in a Metastability-Assisted Medium Carbon Alloy Steel
verfasst von
Cheng Liu
Xixi Cui
Chen Yang
Publikationsdatum
17.05.2018
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 7/2018
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-018-3378-7

Weitere Artikel der Ausgabe 7/2018

Journal of Materials Engineering and Performance 7/2018 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.