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Journal of Materials Science
Erschienen in: Journal of Materials Science 2/2015

01.01.2015 | Original Paper

A mechanochemical approach to manufacturing bamboo cellulose nanocrystals

verfasst von: Qilin Lu, Wenyi Lin, Lirong Tang, Siqun Wang, Xuerong Chen, Biao Huang

Erschienen in: Journal of Materials Science | Ausgabe 2/2015

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Abstract

Bamboo cellulose nanocrystals (BCNC) were manufactured via a mechanochemical approach with the dissolving action of phosphoric acid on cellulose. The effects of phosphoric acid concentration, reaction time, reaction temperature, and ultrasonication time on the yield of BCNC were investigated. Micromorphology and microstructure of BCNC were studied using scanning electron microscopy and transmission electron microscopy. Results showed that BCNC were short rod-like particles with 100–200 nm in length and 15–30 nm in width, forming an interconnected network structure. X-ray diffraction results indicated that the crystalline structure of BCNC transformed from cellulose I to cellulose II, compared to cellulose pulp, with the crystallinity index declining from 66.44 to 59.62 %. The thermal properties of BCNC were investigated by thermogravimetric analysis and revealed that BCNC exhibited lower thermal stability compared to cellulose pulp. This research work provides a low-cost approach and mild operating conditions to manufacturing BCNC.
Vorheriger Artikel Gold-functionalized graphene as conductive filler in UV-curable epoxy resin
Nächster Artikel Structural, magnetic, and magnetocaloric studies of La0.67Ba0.22Sr0.11Mn1−x Co x O3 manganites

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Metadaten
Titel
A mechanochemical approach to manufacturing bamboo cellulose nanocrystals
verfasst von
Qilin Lu
Wenyi Lin
Lirong Tang
Siqun Wang
Xuerong Chen
Biao Huang
Publikationsdatum
01.01.2015
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 2/2015
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-014-8620-6

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