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Journal of Materials Science
Erschienen in: Journal of Materials Science 19/2018

24.04.2018 | Mechanochemical Synthesis

On the influence of water on the mechanochemical synthesis of low F-doped Al-hydroxide fluorides

verfasst von: V. Scalise, G. Scholz, E. Kemnitz

Erschienen in: Journal of Materials Science | Ausgabe 19/2018

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Abstract

The significant role played by water in the mechanochemical synthesis of highly distorted aluminum hydroxide fluorides is on the main focus of this research paper. The importance of water in the synthesis was evaluated considering separately combinations of O/OH sources (Al(OH)3, Al2O3) and fluorine sources with or without structural water (β-AlF3.3H2O, α-AlF3). Each system was studied by typical bulk and surface characterization techniques (XRD, MAS NMR, DTA-TG, NH3-TPD) and compared to each other in order to gain a more comprehensive insight of the importance of including water in the synthesis of amorphous aluminum hydroxide fluorides.
Vorheriger Artikel Mechanochemical preparation of nanocrystalline metal halide phosphors
Nächster Artikel F anion dynamics in cation-mixed nanocrystalline LaF3: SrF2

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Metadaten
Titel
On the influence of water on the mechanochemical synthesis of low F-doped Al-hydroxide fluorides
verfasst von
V. Scalise
G. Scholz
E. Kemnitz
Publikationsdatum
24.04.2018
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 19/2018
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-018-2347-8

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