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Journal of Materials Science
Erschienen in: Journal of Materials Science 19/2019

27.06.2019 | Chemical routes to materials

Preparation of oxygen-deficient 2D WO3−x nanoplates and their adsorption behaviors for organic pollutants: equilibrium and kinetics modeling

verfasst von: Wenjie Pu, Zhilong Song, Jia Yan, Hui Xu, Haiyan Ji, Shouqi Yuan, Huaming Li

Erschienen in: Journal of Materials Science | Ausgabe 19/2019

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Abstract

A novel oxygen defect-rich WO3−x nanoplates were synthesized using a solvothermal method followed by an annealing treatment under Ar–H2 gas mixture atmosphere. WO3−x nanoplates possess large numbers of oxygen defects systematically demonstrated by the elemental analysis, X-ray diffraction, Fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy, respectively. The adsorption capacity of defect-rich 2D WO3−x nanoplates was evaluated by removal of methyl orange (MO) and the adsorption capacity could reach to 63.7 µg mg−1 with good stability and reusability after. Their adsorption performance at the temperature of 298 K, 308 K and 318 K is carried out and proved to fit Langmuir isotherm model very well, suggestive of a monolayer adsorption on the materials surface sites. In addition, adsorption kinetics studies show that the adsorption process conforms to the pseudo-second-order equation model very well demonstrating a chemical process for MO adsorption. Compared to pure WO3 with annealing treatment at N2 and air atmospheres, the one treated under Ar–H2 gas mixture atmosphere (WO3−x) shows higher adsorption capacity and fast adsorption kinetics toward MO, which was attributed to deprivation of lattice oxygen of WO3 at the reducing atmosphere. Meanwhile, the 2D defect-rich WO3−x nanoplates also exhibit excellent adsorption properties toward methylene blue and rhodamine B, and they can be made into thin film by vacuum suction filtration for dynamically removing the organic pollutants. Our study shows that the as-synthesized defect-rich 2D WO3−x nanoplates have potential applications in real-time wastewater treatment.
Vorheriger Artikel A novel two-stage synthesis for 3C–SiC nanowires by carbothermic reduction and their photoluminescence properties
Nächster Artikel Conversion of residue biomass into value added carbon materials: utilisation of sugarcane bagasse and ionic liquids

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Metadaten
Titel
Preparation of oxygen-deficient 2D WO3−x nanoplates and their adsorption behaviors for organic pollutants: equilibrium and kinetics modeling
verfasst von
Wenjie Pu
Zhilong Song
Jia Yan
Hui Xu
Haiyan Ji
Shouqi Yuan
Huaming Li
Publikationsdatum
27.06.2019
Verlag
Springer US
Erschienen in
Journal of Materials Science / Ausgabe 19/2019
Print ISSN: 0022-2461
Elektronische ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-019-03780-6

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