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Journal of Nanoparticle Research

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01.10.2020 | Research paper

Synthesis of early transition metal oxide nanomaterials and their conversion to nitrides

verfasst von: Anastasia M. Kastl, Andrew P. Purdy, Raymond J. Butcher

Erschienen in: Journal of Nanoparticle Research | Ausgabe 10/2020

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Abstract

The synthesis of nanorods and nanowires of early transition metal oxides by hydrothermal methods and the conversion of some bulk oxides to nitrides in NH₃ flow are both well established. However, the conversion of such oxide nanostructures to nitrides is not as well explored but could be a valuable method of producing nanowires, nanorods, and other asymmetric or high aspect ratio nanoparticles of the highly conductive metal nitrides. In this work, nanostructures of TiO₂, V₂O₅, MoO₃, and WO₃ and mixtures thereof were synthesized by hydrothermal reactions, and conversion into nitride was attempted by heating the oxide material under NH₃ flow with or without N₂ flow. It was found that slow heating produces the best shape retention, but the nitridized products are porous in even the most favorable cases. The products were characterized by X-ray powder diffraction and scanning electron microscopy. Two-point conductivity measurements were done on the nitride materials, and optical measurements to characterize the plasmon absorption were done in favorable cases.

Vorheriger Artikel Fabrication and characterization of supercapacitor electrodes using chemically synthesized CuO nanostructure and activated charcoal (AC) based nanocomposite

Nächster Artikel Synthesis of tetrahedral patchy nanoparticles with controlled patch size

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Titel: Synthesis of early transition metal oxide nanomaterials and their conversion to nitrides
verfasst von: Anastasia M. Kastl
Andrew P. Purdy
Raymond J. Butcher
Publikationsdatum: 01.10.2020
Verlag: Springer Netherlands
Erschienen in: Journal of Nanoparticle Research / Ausgabe 10/2020
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-020-05038-8

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