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Erschienen in: Journal of Materials Engineering and Performance 4-5/2011

01.07.2011

Rapid Obtaining of Nano-Hydroxyapatite Bioactive Films on NiTi Shape Memory Alloy by Electrodeposition Process

verfasst von: A. O. Lobo, J. Otubo, J. T. Matsushima, E. J. Corat

Erschienen in: Journal of Materials Engineering and Performance | Ausgabe 4-5/2011

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Abstract

Nano-hydroxyapatite (n-HA) crystalline films have been developed in this study by electrodeposition method on NiTi shape memory alloy (SMA). The electrodeposition of the n-HA films was carried out using 0.042 mol/L Ca(NO3)2 · 4H2O + 0.025 mol/L (NH4) · 2HPO4 electrolytes by applying a constant potential of −2.0 V for 120 min and keeping the solution temperature at 70 °C. The characterization of n-HA films is of special importance since bioactive properties related to n-HA have been directly identified with its specific composition and crystalline structure. AFM, XRD, EDX, FEG-SEM and Raman spectroscopy shows a homogeneous film, with high crystallinity, special composition, and bioactivity properties (Ca/P = 1.93) of n-HA on NiTi SMA surfaces. The n-HA coating with special structure would benefit the use of NiTi alloy in orthopedic applications.

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Metadaten
Titel
Rapid Obtaining of Nano-Hydroxyapatite Bioactive Films on NiTi Shape Memory Alloy by Electrodeposition Process
verfasst von
A. O. Lobo
J. Otubo
J. T. Matsushima
E. J. Corat
Publikationsdatum
01.07.2011
Verlag
Springer US
Erschienen in
Journal of Materials Engineering and Performance / Ausgabe 4-5/2011
Print ISSN: 1059-9495
Elektronische ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-010-9751-9

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